JPS6096521A - ケ−キ状含水珪酸の製法 - Google Patents
ケ−キ状含水珪酸の製法Info
- Publication number
- JPS6096521A JPS6096521A JP20125483A JP20125483A JPS6096521A JP S6096521 A JPS6096521 A JP S6096521A JP 20125483 A JP20125483 A JP 20125483A JP 20125483 A JP20125483 A JP 20125483A JP S6096521 A JPS6096521 A JP S6096521A
- Authority
- JP
- Japan
- Prior art keywords
- silicic acid
- reaction
- acid
- alkali silicate
- stirring
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 235000012239 silicon dioxide Nutrition 0.000 title abstract description 30
- RMAQACBXLXPBSY-UHFFFAOYSA-N silicic acid Chemical compound O[Si](O)(O)O RMAQACBXLXPBSY-UHFFFAOYSA-N 0.000 title abstract description 29
- 229910052910 alkali metal silicate Inorganic materials 0.000 claims abstract description 17
- 150000003863 ammonium salts Chemical class 0.000 claims abstract description 13
- 238000000354 decomposition reaction Methods 0.000 claims abstract description 7
- 239000011259 mixed solution Substances 0.000 claims abstract description 3
- 238000004519 manufacturing process Methods 0.000 claims description 9
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims description 3
- 229910052710 silicon Inorganic materials 0.000 claims description 3
- 239000010703 silicon Substances 0.000 claims description 3
- 238000000034 method Methods 0.000 abstract description 20
- 239000000243 solution Substances 0.000 abstract description 19
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 abstract description 18
- 238000006243 chemical reaction Methods 0.000 abstract description 18
- 239000007864 aqueous solution Substances 0.000 abstract description 15
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 abstract description 14
- 238000003756 stirring Methods 0.000 abstract description 14
- 150000007522 mineralic acids Chemical class 0.000 abstract description 11
- BFNBIHQBYMNNAN-UHFFFAOYSA-N ammonium sulfate Chemical compound N.N.OS(O)(=O)=O BFNBIHQBYMNNAN-UHFFFAOYSA-N 0.000 abstract description 9
- 229910052921 ammonium sulfate Inorganic materials 0.000 abstract description 9
- 235000011130 ammonium sulphate Nutrition 0.000 abstract description 9
- 229910021529 ammonia Inorganic materials 0.000 abstract description 7
- 239000007787 solid Substances 0.000 abstract description 7
- 239000004115 Sodium Silicate Substances 0.000 abstract description 6
- 229910052911 sodium silicate Inorganic materials 0.000 abstract description 6
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 abstract description 6
- 238000001035 drying Methods 0.000 abstract description 4
- 239000000203 mixture Substances 0.000 abstract description 4
- 239000007788 liquid Substances 0.000 abstract description 2
- -1 ammonium sulfate Chemical class 0.000 abstract 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 11
- 238000001879 gelation Methods 0.000 description 8
- 239000002245 particle Substances 0.000 description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 8
- 239000000047 product Substances 0.000 description 5
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonia chloride Chemical compound [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 description 4
- 230000000052 comparative effect Effects 0.000 description 4
- 238000007639 printing Methods 0.000 description 4
- 239000000377 silicon dioxide Substances 0.000 description 4
- 239000002002 slurry Substances 0.000 description 4
- 239000000945 filler Substances 0.000 description 3
- 230000007935 neutral effect Effects 0.000 description 3
- 238000005191 phase separation Methods 0.000 description 3
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 2
- 230000032683 aging Effects 0.000 description 2
- 235000019270 ammonium chloride Nutrition 0.000 description 2
- 230000018044 dehydration Effects 0.000 description 2
- 238000006297 dehydration reaction Methods 0.000 description 2
- 239000010419 fine particle Substances 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 238000006386 neutralization reaction Methods 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 230000005070 ripening Effects 0.000 description 2
- 238000000926 separation method Methods 0.000 description 2
- 239000011734 sodium Substances 0.000 description 2
- 229910052708 sodium Inorganic materials 0.000 description 2
- PAWQVTBBRAZDMG-UHFFFAOYSA-N 2-(3-bromo-2-fluorophenyl)acetic acid Chemical compound OC(=O)CC1=CC=CC(Br)=C1F PAWQVTBBRAZDMG-UHFFFAOYSA-N 0.000 description 1
- 241000252233 Cyprinus carpio Species 0.000 description 1
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 1
- BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 description 1
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 1
- 238000005299 abrasion Methods 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000004480 active ingredient Substances 0.000 description 1
- 239000000853 adhesive Substances 0.000 description 1
- 230000001070 adhesive effect Effects 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- LFVGISIMTYGQHF-UHFFFAOYSA-N ammonium dihydrogen phosphate Chemical compound [NH4+].OP(O)([O-])=O LFVGISIMTYGQHF-UHFFFAOYSA-N 0.000 description 1
- 229910000387 ammonium dihydrogen phosphate Inorganic materials 0.000 description 1
- 239000002585 base Substances 0.000 description 1
- 238000009924 canning Methods 0.000 description 1
- 239000001569 carbon dioxide Substances 0.000 description 1
- 229910002092 carbon dioxide Inorganic materials 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000006482 condensation reaction Methods 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 238000004132 cross linking Methods 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 230000003247 decreasing effect Effects 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 238000007865 diluting Methods 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 229920001971 elastomer Polymers 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000003337 fertilizer Substances 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 150000002357 guanidines Chemical class 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 238000007644 letterpress printing Methods 0.000 description 1
- 229910003002 lithium salt Inorganic materials 0.000 description 1
- 159000000002 lithium salts Chemical class 0.000 description 1
- 235000019837 monoammonium phosphate Nutrition 0.000 description 1
- 239000006012 monoammonium phosphate Substances 0.000 description 1
- 229910017604 nitric acid Inorganic materials 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 239000011574 phosphorus Substances 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- 159000000001 potassium salts Chemical class 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 239000010453 quartz Substances 0.000 description 1
- 230000000630 rising effect Effects 0.000 description 1
- 239000005060 rubber Substances 0.000 description 1
- 238000000967 suction filtration Methods 0.000 description 1
- 229910052717 sulfur Inorganic materials 0.000 description 1
- 239000011593 sulfur Substances 0.000 description 1
- 238000010998 test method Methods 0.000 description 1
- POWFTOSLLWLEBN-UHFFFAOYSA-N tetrasodium;silicate Chemical class [Na+].[Na+].[Na+].[Na+].[O-][Si]([O-])([O-])[O-] POWFTOSLLWLEBN-UHFFFAOYSA-N 0.000 description 1
- 239000002562 thickening agent Substances 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
Landscapes
- Silicon Compounds (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP20125483A JPS6096521A (ja) | 1983-10-26 | 1983-10-26 | ケ−キ状含水珪酸の製法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP20125483A JPS6096521A (ja) | 1983-10-26 | 1983-10-26 | ケ−キ状含水珪酸の製法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS6096521A true JPS6096521A (ja) | 1985-05-30 |
| JPH059367B2 JPH059367B2 (https=) | 1993-02-04 |
Family
ID=16437889
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP20125483A Granted JPS6096521A (ja) | 1983-10-26 | 1983-10-26 | ケ−キ状含水珪酸の製法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS6096521A (https=) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1047148C (zh) * | 1994-09-26 | 1999-12-08 | 日本制纸株式会社 | 硅酸水合物的制备方法 |
| CN103274422A (zh) * | 2013-05-31 | 2013-09-04 | 肇庆市金三江化工有限公司 | 核壳型沉淀二氧化硅、制备方法及含有该二氧化硅的牙膏 |
| JP2018118867A (ja) * | 2017-01-24 | 2018-08-02 | 太平洋セメント株式会社 | 精製シリカの製造方法 |
| CN110330022A (zh) * | 2019-07-08 | 2019-10-15 | 福建远翔新材料股份有限公司 | 一种发泡硅橡胶海绵用高分散二氧化硅的制备方法 |
| CN110562988A (zh) * | 2019-09-12 | 2019-12-13 | 青岛美高集团有限公司 | 一种隔热保温材料及其生产方法 |
-
1983
- 1983-10-26 JP JP20125483A patent/JPS6096521A/ja active Granted
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1047148C (zh) * | 1994-09-26 | 1999-12-08 | 日本制纸株式会社 | 硅酸水合物的制备方法 |
| CN103274422A (zh) * | 2013-05-31 | 2013-09-04 | 肇庆市金三江化工有限公司 | 核壳型沉淀二氧化硅、制备方法及含有该二氧化硅的牙膏 |
| CN103274422B (zh) * | 2013-05-31 | 2016-03-30 | 肇庆金三江硅材料有限公司 | 核壳型沉淀二氧化硅、制备方法及含有该二氧化硅的牙膏 |
| JP2018118867A (ja) * | 2017-01-24 | 2018-08-02 | 太平洋セメント株式会社 | 精製シリカの製造方法 |
| CN110330022A (zh) * | 2019-07-08 | 2019-10-15 | 福建远翔新材料股份有限公司 | 一种发泡硅橡胶海绵用高分散二氧化硅的制备方法 |
| CN110562988A (zh) * | 2019-09-12 | 2019-12-13 | 青岛美高集团有限公司 | 一种隔热保温材料及其生产方法 |
| CN110562988B (zh) * | 2019-09-12 | 2023-10-31 | 青岛美高集团有限公司 | 一种隔热保温材料及其生产方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| JPH059367B2 (https=) | 1993-02-04 |
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