JPS59184192A - 含硫オルガノ珪素化合物の製法 - Google Patents
含硫オルガノ珪素化合物の製法Info
- Publication number
- JPS59184192A JPS59184192A JP59057519A JP5751984A JPS59184192A JP S59184192 A JPS59184192 A JP S59184192A JP 59057519 A JP59057519 A JP 59057519A JP 5751984 A JP5751984 A JP 5751984A JP S59184192 A JPS59184192 A JP S59184192A
- Authority
- JP
- Japan
- Prior art keywords
- group
- formula
- atoms
- sulfur
- hydrogen sulfide
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 title claims abstract description 12
- 239000011593 sulfur Substances 0.000 title claims abstract description 11
- 229910052717 sulfur Inorganic materials 0.000 title claims abstract description 11
- 150000003961 organosilicon compounds Chemical class 0.000 title abstract description 8
- 238000004519 manufacturing process Methods 0.000 title abstract description 6
- 238000000034 method Methods 0.000 claims abstract description 18
- 229910052783 alkali metal Inorganic materials 0.000 claims abstract description 11
- 150000001340 alkali metals Chemical class 0.000 claims abstract description 11
- RWSOTUBLDIXVET-UHFFFAOYSA-N Dihydrogen sulfide Chemical compound S RWSOTUBLDIXVET-UHFFFAOYSA-N 0.000 claims abstract description 10
- 229910000037 hydrogen sulfide Inorganic materials 0.000 claims abstract description 10
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 15
- 125000004429 atom Chemical group 0.000 claims description 7
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 6
- 150000001875 compounds Chemical class 0.000 claims description 6
- 239000003960 organic solvent Substances 0.000 claims description 6
- 229910052708 sodium Inorganic materials 0.000 claims description 6
- 239000011734 sodium Substances 0.000 claims description 6
- 125000004432 carbon atom Chemical group C* 0.000 claims description 5
- 150000004820 halides Chemical class 0.000 claims description 5
- -1 aromatic hydroxyl compound Chemical class 0.000 claims description 4
- 229910052801 chlorine Chemical group 0.000 claims description 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 claims description 2
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical group [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims description 2
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims description 2
- 125000003545 alkoxy group Chemical group 0.000 claims description 2
- 125000000217 alkyl group Chemical group 0.000 claims description 2
- 125000001797 benzyl group Chemical group [H]C1=C([H])C([H])=C(C([H])=C1[H])C([H])([H])* 0.000 claims description 2
- 125000000051 benzyloxy group Chemical group [H]C1=C([H])C([H])=C(C([H])=C1[H])C([H])([H])O* 0.000 claims description 2
- 239000000460 chlorine Chemical group 0.000 claims description 2
- 125000000000 cycloalkoxy group Chemical group 0.000 claims description 2
- 125000000753 cycloalkyl group Chemical group 0.000 claims description 2
- 239000006185 dispersion Substances 0.000 claims description 2
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 claims description 2
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 claims description 2
- 229910052700 potassium Inorganic materials 0.000 claims description 2
- 239000011591 potassium Substances 0.000 claims description 2
- 229930195734 saturated hydrocarbon Natural products 0.000 claims description 2
- 239000002904 solvent Substances 0.000 claims description 2
- WKBOTKDWSSQWDR-UHFFFAOYSA-N Bromine atom Chemical group [Br] WKBOTKDWSSQWDR-UHFFFAOYSA-N 0.000 claims 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 claims 1
- 125000001309 chloro group Chemical group Cl* 0.000 claims 1
- 125000001183 hydrocarbyl group Chemical group 0.000 claims 1
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims 1
- 125000000951 phenoxy group Chemical group [H]C1=C([H])C([H])=C(O*)C([H])=C1[H] 0.000 claims 1
- 229910052725 zinc Inorganic materials 0.000 claims 1
- 239000011701 zinc Substances 0.000 claims 1
- 238000006243 chemical reaction Methods 0.000 abstract description 13
- 235000019441 ethanol Nutrition 0.000 description 9
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 6
- 238000010992 reflux Methods 0.000 description 5
- 230000015572 biosynthetic process Effects 0.000 description 4
- 239000000047 product Substances 0.000 description 4
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 3
- HIVLDXAAFGCOFU-UHFFFAOYSA-N ammonium hydrosulfide Chemical compound [NH4+].[SH-] HIVLDXAAFGCOFU-UHFFFAOYSA-N 0.000 description 3
- 239000007789 gas Substances 0.000 description 3
- 239000001257 hydrogen Substances 0.000 description 3
- 229910052739 hydrogen Inorganic materials 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- HYHCSLBZRBJJCH-UHFFFAOYSA-M sodium hydrosulfide Chemical compound [Na+].[SH-] HYHCSLBZRBJJCH-UHFFFAOYSA-M 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 150000001298 alcohols Chemical class 0.000 description 2
- 239000006227 byproduct Substances 0.000 description 2
- 238000004821 distillation Methods 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 125000004430 oxygen atom Chemical group O* 0.000 description 2
- BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 description 2
- 150000003839 salts Chemical class 0.000 description 2
- 239000007858 starting material Substances 0.000 description 2
- VXNZUUAINFGPBY-UHFFFAOYSA-N 1-Butene Chemical group CCC=C VXNZUUAINFGPBY-UHFFFAOYSA-N 0.000 description 1
- 125000004826 2,3-dimethylpropylene group Chemical group [H]C([H])([H])C([H])([*:2])C([H])(C([H])([H])[H])C([H])([H])[*:1] 0.000 description 1
- KSCAZPYHLGGNPZ-UHFFFAOYSA-N 3-chloropropyl(triethoxy)silane Chemical compound CCO[Si](OCC)(OCC)CCCCl KSCAZPYHLGGNPZ-UHFFFAOYSA-N 0.000 description 1
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 description 1
- 239000005977 Ethylene Substances 0.000 description 1
- 238000004566 IR spectroscopy Methods 0.000 description 1
- AMQJEAYHLZJPGS-UHFFFAOYSA-N N-Pentanol Chemical compound CCCCCO AMQJEAYHLZJPGS-UHFFFAOYSA-N 0.000 description 1
- BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 description 1
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 230000001476 alcoholic effect Effects 0.000 description 1
- 125000005370 alkoxysilyl group Chemical group 0.000 description 1
- 235000019445 benzyl alcohol Nutrition 0.000 description 1
- 150000003938 benzyl alcohols Chemical class 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- LBVNUQQORDPZCR-UHFFFAOYSA-N calcium;sulfane Chemical compound S.[Ca] LBVNUQQORDPZCR-UHFFFAOYSA-N 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 125000000118 dimethyl group Chemical group [H]C([H])([H])* 0.000 description 1
- 229920001971 elastomer Polymers 0.000 description 1
- 230000007717 exclusion Effects 0.000 description 1
- 239000000945 filler Substances 0.000 description 1
- 239000000706 filtrate Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 150000002430 hydrocarbons Chemical group 0.000 description 1
- 125000001570 methylene group Chemical group [H]C([H])([*:1])[*:2] 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 150000002989 phenols Chemical class 0.000 description 1
- ZOCLAPYLSUCOGI-UHFFFAOYSA-M potassium hydrosulfide Chemical compound [SH-].[K+] ZOCLAPYLSUCOGI-UHFFFAOYSA-M 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 230000001681 protective effect Effects 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 239000012758 reinforcing additive Substances 0.000 description 1
- 229910000077 silane Inorganic materials 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000005809 transesterification reaction Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
- C07F7/02—Silicon compounds
- C07F7/08—Compounds having one or more C—Si linkages
- C07F7/18—Compounds having one or more C—Si linkages as well as one or more C—O—Si linkages
- C07F7/1804—Compounds having Si-O-C linkages
- C07F7/1872—Preparation; Treatments not provided for in C07F7/20
- C07F7/1892—Preparation; Treatments not provided for in C07F7/20 by reactions not provided for in C07F7/1876 - C07F7/1888
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F7/00—Compounds containing elements of Groups 4 or 14 of the Periodic Table
- C07F7/02—Silicon compounds
- C07F7/08—Compounds having one or more C—Si linkages
- C07F7/18—Compounds having one or more C—Si linkages as well as one or more C—O—Si linkages
- C07F7/1804—Compounds having Si-O-C linkages
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE19833311340 DE3311340A1 (de) | 1983-03-29 | 1983-03-29 | Verfahren zur herstellung von schwefelhaltigen organosiliciumverbindungen |
DE3311340.8 | 1983-03-29 |
Publications (2)
Publication Number | Publication Date |
---|---|
JPS59184192A true JPS59184192A (ja) | 1984-10-19 |
JPH0463879B2 JPH0463879B2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1992-10-13 |
Family
ID=6194944
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP59057519A Granted JPS59184192A (ja) | 1983-03-29 | 1984-03-27 | 含硫オルガノ珪素化合物の製法 |
Country Status (6)
Cited By (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH02142798A (ja) * | 1988-07-13 | 1990-05-31 | Univ Brigham Young | イオウ含有炭化水素化合物及び所望イオンの当該化合物溶液からの回収,濃縮化時に当該化合物を使用する方法 |
JPH07228588A (ja) * | 1994-02-16 | 1995-08-29 | Shin Etsu Chem Co Ltd | 含硫黄有機珪素化合物の製造方法 |
JPH0853473A (ja) * | 1994-07-08 | 1996-02-27 | Goodyear Tire & Rubber Co:The | 硫黄含有有機ケイ素化合物の製造方法 |
JPH11116585A (ja) * | 1997-08-08 | 1999-04-27 | Degussa Ag | 高純度オルガノシリコンジスルファンの製造方法 |
JP2000103794A (ja) * | 1998-04-10 | 2000-04-11 | Daiso Co Ltd | 含硫黄有機珪素化合物の製造方法およびその合成中間体の製造方法 |
JP2000159932A (ja) * | 1998-11-27 | 2000-06-13 | Bridgestone Corp | ゴム組成物および空気入りタイヤ |
JP2005511700A (ja) * | 2001-12-06 | 2005-04-28 | ロディア・シミ | ポリスルフィドモノオルガノオキシシランの製造法 |
JP4352282B1 (ja) * | 2008-10-24 | 2009-10-28 | 住友ベークライト株式会社 | 半導体用接着剤組成物およびそれを用いて製造した半導体装置 |
JP2011073405A (ja) * | 2009-10-01 | 2011-04-14 | Sumitomo Bakelite Co Ltd | 積層構造体の製造方法 |
JP2018065954A (ja) * | 2016-10-20 | 2018-04-26 | 住友ゴム工業株式会社 | タイヤ用ゴム組成物及び空気入りタイヤ |
JPWO2021153396A1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) * | 2020-01-30 | 2021-08-05 |
Families Citing this family (37)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE3346910C1 (de) * | 1983-12-24 | 1985-05-02 | Dynamit Nobel Ag, 5210 Troisdorf | Verfahren zur Herstellung von Mercaptoalkylsilanen |
DE3543567A1 (de) * | 1985-12-10 | 1987-06-11 | Degussa | Verfahren zur herstellung von sulfensaeurechloriden und sulfensaeureestern |
DD299589A7 (de) * | 1990-07-13 | 1992-04-30 | Nuenchritz Chemie | Verfahren zur herstellung von oligo[4-(2-organo-organooxysilylalkyl)-cyclohexan-1,2-diyl]-bis-oligosulfiden |
DE4409140A1 (de) * | 1994-03-17 | 1995-09-21 | Degussa | Wäßrige Lösungen von Organopolysiloxan-Ammoniumverbindungen, ihre Herstellung und Verwendung |
US5399739A (en) * | 1994-04-18 | 1995-03-21 | Wright Chemical Corporation | Method of making sulfur-containing organosilanes |
US5405985A (en) * | 1994-07-08 | 1995-04-11 | The Goodyear Tire & Rubber Company | Preparation of sulfur-containing organosilicon compounds |
US5489701A (en) * | 1994-09-28 | 1996-02-06 | Osi Specialties, Inc. | Process for the preparation of silane polysulfides |
US5466848A (en) * | 1994-09-28 | 1995-11-14 | Osi Specialties, Inc. | Process for the preparation of silane polysulfides |
US5440064A (en) * | 1994-12-23 | 1995-08-08 | The Goodyear Tire & Rubber Company | Process for the preparation of organosilicon disulfide compounds |
US5596116A (en) * | 1995-09-11 | 1997-01-21 | Osi Specialties, Inc. | Process for the preparation of silane polysulfides |
US5583245A (en) * | 1996-03-06 | 1996-12-10 | The Goodyear Tire & Rubber Company | Preparation of sulfur-containing organosilicon compounds |
US5663396A (en) * | 1996-10-31 | 1997-09-02 | The Goodyear Tire & Rubber Company | Preparation of sulfur-containing organosilicon compounds |
DE19732725A1 (de) * | 1997-07-30 | 1999-02-04 | Degussa | Mischungen, bestehend aus Bis(silylorganyl)polysulfanen und Silylorganylthiocyanaten, ihre Herstellung und Verwendung |
JP3498559B2 (ja) * | 1997-12-01 | 2004-02-16 | 信越化学工業株式会社 | 短鎖ポリスルフィドシラン混合物の製造方法 |
DE19819373A1 (de) * | 1998-04-30 | 1999-11-04 | Degussa | Verfahren zur Herstellung von Gemischen von Organosiliciumoligosulfanen mit einem hohen Anteil an Organanosiliciumdisulfanen |
JPH11349594A (ja) * | 1998-06-08 | 1999-12-21 | Shin Etsu Chem Co Ltd | 短鎖ポリスルフィドシラン混合物の製造方法 |
US6452034B2 (en) | 2000-01-04 | 2002-09-17 | Crompton Corporation | Low-sulfur polysulfide silanes and process for preparation |
US6518335B2 (en) | 2000-01-05 | 2003-02-11 | Crompton Corporation | Sulfur-containing silane coupling agents |
US6359046B1 (en) | 2000-09-08 | 2002-03-19 | Crompton Corporation | Hydrocarbon core polysulfide silane coupling agents for filled elastomer compositions |
FR2830014B1 (fr) * | 2001-09-21 | 2005-02-18 | Rhodia Chimie Sa | Procede d'obtention de monoorganoxysilanes halogenes utilisables notamment en tant qu'intermediaires de synthese |
FR2830013B1 (fr) * | 2001-09-21 | 2005-02-25 | Rhodia Chimie Sa | Procede d'obtention de monoorganoxysilanes halogenes utilisables notamment en tant qu'intermediaires de synthese |
JP2003261580A (ja) * | 2002-03-08 | 2003-09-19 | Shin Etsu Chem Co Ltd | スルフィド鎖含有有機珪素化合物の製造方法 |
FR2841244B1 (fr) * | 2002-06-21 | 2007-10-05 | Rhodia Chimie Sa | Procede de preparation d'organo dialkylalcoxysilane |
US8592506B2 (en) | 2006-12-28 | 2013-11-26 | Continental Ag | Tire compositions and components containing blocked mercaptosilane coupling agent |
US7968633B2 (en) | 2006-12-28 | 2011-06-28 | Continental Ag | Tire compositions and components containing free-flowing filler compositions |
US7960460B2 (en) | 2006-12-28 | 2011-06-14 | Momentive Performance Materials, Inc. | Free-flowing filler composition and rubber composition containing same |
US7968635B2 (en) | 2006-12-28 | 2011-06-28 | Continental Ag | Tire compositions and components containing free-flowing filler compositions |
US7968636B2 (en) | 2006-12-28 | 2011-06-28 | Continental Ag | Tire compositions and components containing silated cyclic core polysulfides |
US7696269B2 (en) | 2006-12-28 | 2010-04-13 | Momentive Performance Materials Inc. | Silated core polysulfides, their preparation and use in filled elastomer compositions |
US7687558B2 (en) | 2006-12-28 | 2010-03-30 | Momentive Performance Materials Inc. | Silated cyclic core polysulfides, their preparation and use in filled elastomer compositions |
US7968634B2 (en) | 2006-12-28 | 2011-06-28 | Continental Ag | Tire compositions and components containing silated core polysulfides |
US7781606B2 (en) | 2006-12-28 | 2010-08-24 | Momentive Performance Materials Inc. | Blocked mercaptosilane coupling agents, process for making and uses in rubber |
US7737202B2 (en) | 2006-12-28 | 2010-06-15 | Momentive Performance Materials Inc. | Free-flowing filler composition and rubber composition containing same |
US9127167B2 (en) | 2011-04-29 | 2015-09-08 | Korea Institute Of Science And Technology | Functional reinforcing fillers modified with alkenylalkoxysilane and preparing method of the same |
KR101250300B1 (ko) | 2011-04-29 | 2013-04-03 | 한국과학기술연구원 | 알케닐알콕시실란을 이용한 기능성 보강 충전제 및 이의 제조 방법 |
CN103342717A (zh) * | 2013-07-18 | 2013-10-09 | 招远市金鹏橡胶助剂有限公司 | 一种双-[丙基三乙氧基硅烷]-二硫化物硅烷偶联剂合成方法 |
CN114394992A (zh) * | 2021-11-12 | 2022-04-26 | 安徽沸点新材料有限公司 | 一种氢硫基硅烷偶联剂及其制备方法 |
Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS5253819A (en) * | 1975-09-24 | 1977-04-30 | Degussa | Process for manufacturing sulfuric aciddcontaining organo silicon compounds |
Family Cites Families (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3284466A (en) * | 1963-07-12 | 1966-11-08 | Thiokol Chemical Corp | Preparation of monomeric disulfides |
US3530160A (en) * | 1968-02-09 | 1970-09-22 | Exxon Research Engineering Co | (organo- or hydrolyzable group substituted)3silyl (unsubstituted chloro- or sulfenyl chloride substituted hydrocarbylene) sulfenyl chlorides |
DE2141159C3 (de) * | 1971-08-17 | 1983-11-24 | Degussa Ag, 6000 Frankfurt | Schwefel enthaltende Organosiliciumverbindungen |
US3873489A (en) * | 1971-08-17 | 1975-03-25 | Degussa | Rubber compositions containing silica and an organosilane |
DE2141160C3 (de) * | 1971-08-17 | 1982-01-21 | Degussa Ag, 6000 Frankfurt | Schwefel enthaltende Organosiliciumverbindungen |
BE787691A (fr) * | 1971-08-17 | 1973-02-19 | Degussa | Composes organosiliciques contenant du soufre |
SU580840A3 (ru) * | 1974-02-07 | 1977-11-15 | Дегусса (Фирма) | Способ получени серосодержащих кремнийорганических соединений |
US4125552A (en) * | 1975-12-29 | 1978-11-14 | Dow Corning Corporation | Preparation of alkyl polysulfides |
DE2712866C3 (de) * | 1977-03-24 | 1980-04-30 | Deutsche Gold- Und Silber-Scheideanstalt Vormals Roessler, 6000 Frankfurt | Verfahren zum Herstellen von schwefelhaltigen Organosiliciumverbindungen |
DE2856229A1 (de) * | 1978-12-27 | 1980-07-03 | Degussa | Bis-(silylaethyl)-oligosulfide und verfahren zur herstellung derselben |
-
1983
- 1983-03-29 DE DE19833311340 patent/DE3311340A1/de active Granted
- 1983-12-23 AT AT83113063T patent/ATE29258T1/de not_active IP Right Cessation
- 1983-12-23 EP EP83113063A patent/EP0124654B1/de not_active Expired
- 1983-12-23 DE DE8383113063T patent/DE3373308D1/de not_active Expired
-
1984
- 1984-03-26 US US06/593,308 patent/US4507490A/en not_active Expired - Fee Related
- 1984-03-27 JP JP59057519A patent/JPS59184192A/ja active Granted
- 1984-03-28 CA CA000450787A patent/CA1234136A/en not_active Expired
Patent Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS5253819A (en) * | 1975-09-24 | 1977-04-30 | Degussa | Process for manufacturing sulfuric aciddcontaining organo silicon compounds |
Cited By (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH02142798A (ja) * | 1988-07-13 | 1990-05-31 | Univ Brigham Young | イオウ含有炭化水素化合物及び所望イオンの当該化合物溶液からの回収,濃縮化時に当該化合物を使用する方法 |
JPH07228588A (ja) * | 1994-02-16 | 1995-08-29 | Shin Etsu Chem Co Ltd | 含硫黄有機珪素化合物の製造方法 |
JPH0853473A (ja) * | 1994-07-08 | 1996-02-27 | Goodyear Tire & Rubber Co:The | 硫黄含有有機ケイ素化合物の製造方法 |
JPH11116585A (ja) * | 1997-08-08 | 1999-04-27 | Degussa Ag | 高純度オルガノシリコンジスルファンの製造方法 |
JP2000103794A (ja) * | 1998-04-10 | 2000-04-11 | Daiso Co Ltd | 含硫黄有機珪素化合物の製造方法およびその合成中間体の製造方法 |
JP2000159932A (ja) * | 1998-11-27 | 2000-06-13 | Bridgestone Corp | ゴム組成物および空気入りタイヤ |
JP2005511700A (ja) * | 2001-12-06 | 2005-04-28 | ロディア・シミ | ポリスルフィドモノオルガノオキシシランの製造法 |
JP4352282B1 (ja) * | 2008-10-24 | 2009-10-28 | 住友ベークライト株式会社 | 半導体用接着剤組成物およびそれを用いて製造した半導体装置 |
JP2011073405A (ja) * | 2009-10-01 | 2011-04-14 | Sumitomo Bakelite Co Ltd | 積層構造体の製造方法 |
JP2018065954A (ja) * | 2016-10-20 | 2018-04-26 | 住友ゴム工業株式会社 | タイヤ用ゴム組成物及び空気入りタイヤ |
JPWO2021153396A1 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) * | 2020-01-30 | 2021-08-05 |
Also Published As
Publication number | Publication date |
---|---|
DE3373308D1 (en) | 1987-10-08 |
DE3311340A1 (de) | 1984-10-11 |
US4507490A (en) | 1985-03-26 |
EP0124654A1 (de) | 1984-11-14 |
JPH0463879B2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1992-10-13 |
EP0124654B1 (de) | 1987-09-02 |
CA1234136A (en) | 1988-03-15 |
ATE29258T1 (de) | 1987-09-15 |
DE3311340C2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1987-06-25 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
JPS59184192A (ja) | 含硫オルガノ珪素化合物の製法 | |
US5892085A (en) | Process for the preparation of high-purity organosilicon disulphanes | |
EP0949263B1 (en) | Process for producing sulfur-containing organosilicon compounds | |
JPH10175981A (ja) | ビス(シリルオルガニル)−ポリスルファンの製造方法 | |
JP4669139B2 (ja) | オルガノシリルアルキルポリスルファンの製法 | |
JPS6225650B2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | ||
US4379766A (en) | Silyl esters of carboxylic acids by phase transfer catalysts | |
JP2002155092A (ja) | オルガノシリルアルキルポリスルファンの製法 | |
US1945183A (en) | Manufacture of alkoxy derivatives of phosphorous acid chlorides | |
US4412078A (en) | Hydantoinylsilanes | |
SU529808A3 (ru) | Способ получени кремнийорганических производных ацетилена | |
JPS647998B2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | ||
US4539418A (en) | Method for the preparation of pentamethylcyclotrisiloxane | |
JP3840810B2 (ja) | β−ケトアルデヒアルカリ塩の製造方法 | |
JP2011001305A (ja) | アザボラシクロペンテン化合物の製造方法 | |
JPS61218555A (ja) | トリフルオロジクロロエチル基により置換された酸類の製法および亜鉛化合物類 | |
Yoshida et al. | SYNTHESIS AND CHARACTERIZATION OF CATIONIC DIAMINOCYCLOPROPENYLIDENE MERCURY COMPLEX | |
US3565935A (en) | Method of forming mercaptoalkyl substituted organosilicon compounds | |
JPH0474189A (ja) | メルカプト基を有するシラン | |
JPS62132893A (ja) | テトラオルガノホスホニウムテトラアリ−ルボレ−トの製造法 | |
JPS6067485A (ja) | 置換フエニルウレイドプロピルトリアルコキシシラン | |
JPS6141898B2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | ||
JPS607977B2 (ja) | P−アミノベンズアルデヒドの製造方法 | |
JPH0421646A (ja) | クロルエチルエーテルの製造方法 | |
JPS61257977A (ja) | 含フツ素複素環化合物 |