JPH07500077A - 窒化ニオビウムの調製方法 - Google Patents
窒化ニオビウムの調製方法Info
- Publication number
- JPH07500077A JPH07500077A JP5501633A JP50163393A JPH07500077A JP H07500077 A JPH07500077 A JP H07500077A JP 5501633 A JP5501633 A JP 5501633A JP 50163393 A JP50163393 A JP 50163393A JP H07500077 A JPH07500077 A JP H07500077A
- Authority
- JP
- Japan
- Prior art keywords
- nitride
- iron
- niobium
- alloy
- alloys
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/06—Binary compounds of nitrogen with metals, with silicon, or with boron, or with carbon, i.e. nitrides; Compounds of nitrogen with more than one metal, silicon or boron
- C01B21/0602—Binary compounds of nitrogen with metals, with silicon, or with boron, or with carbon, i.e. nitrides; Compounds of nitrogen with more than one metal, silicon or boron with two or more other elements chosen from metals, silicon or boron
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/06—Binary compounds of nitrogen with metals, with silicon, or with boron, or with carbon, i.e. nitrides; Compounds of nitrogen with more than one metal, silicon or boron
- C01B21/0615—Binary compounds of nitrogen with metals, with silicon, or with boron, or with carbon, i.e. nitrides; Compounds of nitrogen with more than one metal, silicon or boron with transition metals other than titanium, zirconium or hafnium
- C01B21/0617—Binary compounds of nitrogen with metals, with silicon, or with boron, or with carbon, i.e. nitrides; Compounds of nitrogen with more than one metal, silicon or boron with transition metals other than titanium, zirconium or hafnium with vanadium, niobium or tantalum
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B6/00—Hydrides of metals including fully or partially hydrided metals, alloys or intermetallic compounds ; Compounds containing at least one metal-hydrogen bond, e.g. (GeH3)2S, SiH GeH; Monoborane or diborane; Addition complexes thereof
- C01B6/02—Hydrides of transition elements; Addition complexes thereof
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/01—Particle morphology depicted by an image
- C01P2004/03—Particle morphology depicted by an image obtained by SEM
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/10—Particle morphology extending in one dimension, e.g. needle-like
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Crystallography & Structural Chemistry (AREA)
- Manufacture And Refinement Of Metals (AREA)
Abstract
Description
Claims (10)
- 1.窒化金属を調製する方法であって、該窒化物を形成するための金属は鉄合金 及びニッケル合金からなるグループから選択された合金に含まれていて、 a)充分な温度で、1平方インチ当り約15ポンドの最大圧力で、充分な時間を かけて、上記合金を酸素を含まない水素含有ガスと反応させ、砕け易い水素化合 生成物を形成し、b)充分高い温度及び圧力で、充分長い時間をかけて、工程a )による水素化合生成物を酵素を含まない窒素含有ガスにおいて反応させ、窒化 鉄又は窒化ニツケル及び窒化合金の化合物を形成し、c)形成された窒化金属組 成から、形成された窒化鉄組成を分離し、窒化金属を回収することからなる方法 。
- 2.鉄金属合金における鉄含有量が約20〜約40重量%である請求項1記載の 方法。
- 3.窒素含有ガスとの反応の前に水素化合合金が約140メッシュ以下の粒子サ イズに細分化される請求項1記載の方法。
- 4.合金が、鉄ニオビウム合金、鉄タンタル合金、鉄バナジウム合金及び鉄シリ コン合金からなるグループから選択される請求項1記載の方法。
- 5.窒化反応が約500℃〜約1400℃の温度で充分な時間行われ、混合され た窒化生成物を強磁性にする請求項4記載の方法。
- 6.窒化鉄を酸性浸出液に溶解することによって、窒化鉄をその他の窒化物から 分離させる請求項4記載の方法。
- 7.酸浸出のための酸が塩酸及び硫酸からなるグループから選択される請求項4 記載の方法。
- 8.酸浸出にフッ化イオンが含まれる請求項7記載の方法。
- 9.窒化反応の生成物が充分な時間、充分高い温度に維持され、形成された窒化 物の拡散による分離を促進する請求項4記載の方法。
- 10.鉄ニオビウムから窒化ニオビウムを調製する方法であって、a)充分高い 温度で、1平方インチ当り約15ポンドの最大圧力で、充分長い時間をかけて、 鉄ニオビウム合金を酸素を含まない水素含有ガスと反応させ、鉄ニオビウム合金 から砕け易い水素化合生成物を形成し、 b)充分高い温度及び圧力で、充分長い時間をかけて、工程a)による水素化合 生成物を酸素を含まない窒素含有ガスにおいて反応させ、窒化鉄及び窒化ニオビ ウムの化合物を形成し、c)形成された窒化ニオビウム化合物から、形成された 窒化鉄化合物を分離し、窒化ニオビウムを回収することからなる方法。
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US72188791A | 1991-06-27 | 1991-06-27 | |
US721,887 | 1991-06-27 | ||
PCT/US1992/005323 WO1993000293A1 (en) | 1991-06-27 | 1992-06-26 | Method for the preparation of niobium nitride |
Publications (2)
Publication Number | Publication Date |
---|---|
JPH07500077A true JPH07500077A (ja) | 1995-01-05 |
JP3379957B2 JP3379957B2 (ja) | 2003-02-24 |
Family
ID=24899725
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP50163393A Expired - Lifetime JP3379957B2 (ja) | 1991-06-27 | 1992-06-26 | 窒化ニオビウムの調製方法 |
Country Status (6)
Country | Link |
---|---|
US (1) | US5284639A (ja) |
EP (1) | EP0591390A4 (ja) |
JP (1) | JP3379957B2 (ja) |
AU (1) | AU2254392A (ja) |
BR (1) | BR9206197A (ja) |
WO (1) | WO1993000293A1 (ja) |
Families Citing this family (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US6007597A (en) * | 1997-02-28 | 1999-12-28 | Teledyne Industries, Inc. | Electron-beam melt refining of ferroniobium |
DE19907616A1 (de) * | 1999-02-23 | 2000-08-24 | Dmc2 Degussa Metals Catalysts | Tantal(V)-nitrid-Pigmente, Verfahren zu deren Herstellung und deren Verwendung |
US6960237B2 (en) | 1999-07-15 | 2005-11-01 | Showa Denko Kabushiki Kaisha | Niobium powder, sintered body thereof and capacitor using the same |
US6600646B1 (en) * | 1999-08-11 | 2003-07-29 | Showa Denko Kabushiki Kaisha | Niobium powder, sintered body thereof and capacitor using same |
CN107857240B (zh) * | 2017-11-30 | 2021-03-30 | 株洲硬质合金集团有限公司 | 氮化铌粉末的生产方法 |
KR102449895B1 (ko) | 2018-05-18 | 2022-09-30 | 삼성전자주식회사 | 반도체 장치와 그 제조 방법 |
CN111017889A (zh) * | 2019-11-20 | 2020-04-17 | 中色(宁夏)东方集团有限公司 | 一种氮化铌的制备方法 |
CN112125287A (zh) * | 2020-09-11 | 2020-12-25 | 昆明理工大学 | 一种难熔金属纳米氮化物及其制备方法 |
Family Cites Families (46)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CA554840A (en) * | 1958-03-25 | Von Bichowsky Foord | Process for the manufacture of particulate metallic niobium | |
CA541516A (en) * | 1957-05-28 | F. Yntema Leonard | Tantalum and columbium recovery | |
DE1068683B (de) * | 1959-11-12 | Deutsche Gold- und Silfoer-Scheideanstalt vormals Roessler, Frankfurt/M | Verfahren zur Herstellung von reinem Zirkontetrachlorid durch Sublimation | |
CA541517A (en) * | 1957-05-28 | Fansteel Metallurgical Corporation | Tantalum and columbium recovery | |
CA470022A (en) * | 1950-12-12 | Electro Metallurgical Company Of Canada | Methods of treating materials containing columbium and tantalum | |
GB485021A (en) * | 1936-12-12 | 1938-05-13 | Metallurg De Hoboken Soc Gen | Improvements in or relating to the production of tantalum and/or niobium carbides |
US2164198A (en) * | 1938-05-05 | 1939-06-27 | Gen Motors Corp | Method of making powdered iron |
US2553444A (en) * | 1947-07-19 | 1951-05-15 | Vanadium Corp Of America | Preparation of pure metallic carbides |
US2474021A (en) * | 1948-01-17 | 1949-06-21 | Du Pont | Production of metal compounds |
GB660397A (en) * | 1948-06-21 | 1951-11-07 | Johnson & Co A | Method of producing pure zirconium halides |
US2682445A (en) * | 1951-07-23 | 1954-06-29 | Schweizerhall Saeurefab | Process for the production of purified anhydrous zirconium tetrahalide |
DE903034C (de) * | 1951-08-09 | 1954-02-01 | Heraeus Gmbh W C | Verfahren zur Herstellung von metallischem Niob oder Tantal |
US2849275A (en) * | 1954-01-21 | 1958-08-26 | Allegheny Ludlum Steel | Production of refractory metal carbides |
GB771144A (en) * | 1954-04-16 | 1957-03-27 | Nat Lead Co | Improvements in or relating to the purification of zirconium tetrachloride |
US2886616A (en) * | 1955-08-24 | 1959-05-12 | Phillips Petroleum Co | Control of polymerization processes |
GB866771A (en) * | 1956-05-18 | 1961-05-03 | Laporte Titanium Ltd | Process for the purification of titanium tetrachloride or zirconium tetrachloride |
US3053620A (en) * | 1958-02-12 | 1962-09-11 | Nat Distillers Chem Corp | Purification method for metal halides |
DE1082240B (de) * | 1959-06-04 | 1960-05-25 | Degussa | Verfahren zur Herstellung von reinem Zirkontetrachlorid durch Sublimation |
NL294900A (ja) * | 1962-07-04 | |||
FR1335556A (fr) * | 1962-07-04 | 1963-08-23 | Commissariat Energie Atomique | Perfectionnements apportés aux procédés et appareils pour la préparation de nitrures métalliques susceptibles d'être frittés ultérieurement, notamment ceux de l'uanium |
US3230077A (en) * | 1962-11-05 | 1966-01-18 | Du Pont | Production of refractory metals |
US3300297A (en) * | 1964-05-26 | 1967-01-24 | Kawecki Chemical Company | Beneficiation of tantalum- and columbium-bearing tin slags |
US3461190A (en) * | 1964-08-20 | 1969-08-12 | Westinghouse Electric Corp | Method of and apparatus for establishing and maintaining an atmosphere controlled as to pressure,temperature,gas content and rate of gas flow,and closed and semi-closed arc heater loop apparatus for use therein |
US3425826A (en) * | 1966-03-21 | 1969-02-04 | Atomic Energy Commission | Purification of vanadium and columbium (niobium) |
US3356513A (en) * | 1966-12-20 | 1967-12-05 | Norton Co | Production of silicon oxynitride |
US3573000A (en) * | 1966-12-23 | 1971-03-30 | Nat Lead Co | Apparatus for generating gaseous metal halides |
FR1536970A (fr) * | 1967-05-02 | 1968-08-23 | Machine à creuser les tranchées à régulation hydraulique et automatique | |
US3539165A (en) * | 1969-06-16 | 1970-11-10 | Glenn R Ingels | Apparatus for treating metallic and nonmetallic materials |
US3639101A (en) * | 1970-06-29 | 1972-02-01 | Norton Co | Process for producing silicon oxynitride |
US3854882A (en) * | 1973-01-17 | 1974-12-17 | Norton Co | Control system in an apparatus for reacting silicon with nitrogen |
US3999981A (en) * | 1974-08-05 | 1976-12-28 | Ontario Research Foundation | Production and recovery of metallic carbides from ores and concentrates |
US4029740A (en) * | 1975-11-24 | 1977-06-14 | Rockwell International Corporation | Method of producing metal nitrides |
LU78341A1 (ja) * | 1977-10-19 | 1979-02-02 | ||
US4318897A (en) * | 1980-08-18 | 1982-03-09 | Uop Inc. | Process for preparing hydrided iron-vanadium alloys |
US4425318A (en) * | 1981-11-12 | 1984-01-10 | Allied Corporation | Hydriding body-centered cubic phase alloys at room temperature |
IL66552A (en) * | 1982-08-15 | 1985-12-31 | Technion Res & Dev Foundation | Method for preparing improved porous metal hydride compacts and apparatus therefor |
US4440737A (en) * | 1982-09-20 | 1984-04-03 | Allied Corporation | Room temperature reaction of vanadium-based alloys with hydrogen |
JPS61276975A (ja) * | 1985-06-03 | 1986-12-06 | Toyo Soda Mfg Co Ltd | 超高純度金属ニオブの製造法 |
LU86090A1 (fr) * | 1985-09-23 | 1987-04-02 | Metallurgie Hoboken | Procede pour preparer du tantale ou du niobium affins |
US4812301A (en) * | 1986-04-24 | 1989-03-14 | The United States Of America As Represented By The Secretary Of The Interior | Production of titanium nitride, carbide, and carbonitride powders |
US4741894A (en) * | 1986-06-03 | 1988-05-03 | Morton Thiokol, Inc. | Method of producing halide-free metal and hydroxides |
US4728507A (en) * | 1987-01-09 | 1988-03-01 | Westinghouse Electric Corp. | Preparation of reactive metal hydrides |
US4913778A (en) * | 1989-01-02 | 1990-04-03 | Westinghouse Electric Corp. | Molten salt scrubbing of zirconium or hafnium tetrachloride |
JPH0339426A (ja) * | 1989-07-05 | 1991-02-20 | Nkk Corp | 金属ニオブの製造方法 |
JPH03249144A (ja) * | 1990-02-27 | 1991-11-07 | Nkk Corp | ハロゲン化ニオブ、酸化ニオブ、窒化ニオブ、炭化ニオブ及び金属ニオブの製造方法 |
AU2269192A (en) * | 1991-06-27 | 1993-01-25 | Teledyne Industries, Inc. | System for controlled nitriding |
-
1992
- 1992-06-26 JP JP50163393A patent/JP3379957B2/ja not_active Expired - Lifetime
- 1992-06-26 AU AU22543/92A patent/AU2254392A/en not_active Abandoned
- 1992-06-26 BR BR9206197A patent/BR9206197A/pt not_active IP Right Cessation
- 1992-06-26 WO PCT/US1992/005323 patent/WO1993000293A1/en not_active Application Discontinuation
- 1992-06-26 EP EP9292914280A patent/EP0591390A4/en not_active Withdrawn
- 1992-07-06 US US07/908,797 patent/US5284639A/en not_active Expired - Lifetime
Also Published As
Publication number | Publication date |
---|---|
BR9206197A (pt) | 1994-12-13 |
EP0591390A1 (en) | 1994-04-13 |
JP3379957B2 (ja) | 2003-02-24 |
US5284639A (en) | 1994-02-08 |
EP0591390A4 (en) | 1994-08-24 |
AU2254392A (en) | 1993-01-25 |
WO1993000293A1 (en) | 1993-01-07 |
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