JPH0193404A - ガーネット構造を持つ化合物の原料粉末の製造方法 - Google Patents
ガーネット構造を持つ化合物の原料粉末の製造方法Info
- Publication number
- JPH0193404A JPH0193404A JP62248957A JP24895787A JPH0193404A JP H0193404 A JPH0193404 A JP H0193404A JP 62248957 A JP62248957 A JP 62248957A JP 24895787 A JP24895787 A JP 24895787A JP H0193404 A JPH0193404 A JP H0193404A
- Authority
- JP
- Japan
- Prior art keywords
- compound
- metals
- garnet structure
- raw material
- precipitates
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 150000001875 compounds Chemical class 0.000 title claims abstract description 25
- 239000000843 powder Substances 0.000 title claims abstract description 23
- 239000002223 garnet Substances 0.000 title claims abstract description 22
- 239000002994 raw material Substances 0.000 title claims abstract description 16
- 238000004519 manufacturing process Methods 0.000 title claims description 10
- 239000002244 precipitate Substances 0.000 claims abstract description 28
- 229910052751 metal Inorganic materials 0.000 claims abstract description 15
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 claims abstract description 14
- 239000004202 carbamide Substances 0.000 claims abstract description 14
- 239000002184 metal Substances 0.000 claims abstract description 13
- 150000002739 metals Chemical class 0.000 claims abstract description 12
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims abstract description 8
- 239000001301 oxygen Substances 0.000 claims abstract description 8
- 229910052760 oxygen Inorganic materials 0.000 claims abstract description 8
- 238000001354 calcination Methods 0.000 claims abstract description 7
- 238000001035 drying Methods 0.000 claims abstract description 3
- 239000000243 solution Substances 0.000 abstract description 7
- 239000007864 aqueous solution Substances 0.000 abstract description 6
- 239000002253 acid Substances 0.000 abstract description 5
- 230000002378 acidificating effect Effects 0.000 abstract description 4
- 230000009257 reactivity Effects 0.000 abstract description 4
- 238000010438 heat treatment Methods 0.000 abstract description 2
- 229910052746 lanthanum Inorganic materials 0.000 abstract description 2
- 239000000126 substance Substances 0.000 abstract description 2
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 abstract 1
- 238000000034 method Methods 0.000 description 16
- 239000006227 byproduct Substances 0.000 description 7
- 238000000354 decomposition reaction Methods 0.000 description 7
- 150000003839 salts Chemical class 0.000 description 5
- 239000000470 constituent Substances 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- 239000012071 phase Substances 0.000 description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- 230000000694 effects Effects 0.000 description 3
- 239000007789 gas Substances 0.000 description 3
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 description 2
- VSCWAEJMTAWNJL-UHFFFAOYSA-K aluminium trichloride Chemical compound Cl[Al](Cl)Cl VSCWAEJMTAWNJL-UHFFFAOYSA-K 0.000 description 2
- 235000011114 ammonium hydroxide Nutrition 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 150000001805 chlorine compounds Chemical class 0.000 description 2
- 230000000052 comparative effect Effects 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- 239000011164 primary particle Substances 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- BNGXYYYYKUGPPF-UHFFFAOYSA-M (3-methylphenyl)methyl-triphenylphosphanium;chloride Chemical compound [Cl-].CC1=CC=CC(C[P+](C=2C=CC=CC=2)(C=2C=CC=CC=2)C=2C=CC=CC=2)=C1 BNGXYYYYKUGPPF-UHFFFAOYSA-M 0.000 description 1
- OBOSXEWFRARQPU-UHFFFAOYSA-N 2-n,2-n-dimethylpyridine-2,5-diamine Chemical compound CN(C)C1=CC=C(N)C=N1 OBOSXEWFRARQPU-UHFFFAOYSA-N 0.000 description 1
- NGDQQLAVJWUYSF-UHFFFAOYSA-N 4-methyl-2-phenyl-1,3-thiazole-5-sulfonyl chloride Chemical compound S1C(S(Cl)(=O)=O)=C(C)N=C1C1=CC=CC=C1 NGDQQLAVJWUYSF-UHFFFAOYSA-N 0.000 description 1
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonia chloride Chemical compound [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 description 1
- 239000003929 acidic solution Substances 0.000 description 1
- QGZKDVFQNNGYKY-UHFFFAOYSA-N ammonia Natural products N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 1
- 150000001450 anions Chemical class 0.000 description 1
- 239000008280 blood Substances 0.000 description 1
- 210000004369 blood Anatomy 0.000 description 1
- 150000001768 cations Chemical class 0.000 description 1
- 238000005119 centrifugation Methods 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 238000000975 co-precipitation Methods 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 238000010908 decantation Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 230000018044 dehydration Effects 0.000 description 1
- 238000006297 dehydration reaction Methods 0.000 description 1
- 229910010272 inorganic material Inorganic materials 0.000 description 1
- 239000011147 inorganic material Substances 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- 150000002823 nitrates Chemical class 0.000 description 1
- WHOPEPSOPUIRQQ-UHFFFAOYSA-N oxoaluminum Chemical compound O1[Al]O[Al]1 WHOPEPSOPUIRQQ-UHFFFAOYSA-N 0.000 description 1
- UZLYXNNZYFBAQO-UHFFFAOYSA-N oxygen(2-);ytterbium(3+) Chemical compound [O-2].[O-2].[O-2].[Yb+3].[Yb+3] UZLYXNNZYFBAQO-UHFFFAOYSA-N 0.000 description 1
- 238000000634 powder X-ray diffraction Methods 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 229910052761 rare earth metal Inorganic materials 0.000 description 1
- 238000010532 solid phase synthesis reaction Methods 0.000 description 1
- 150000003467 sulfuric acid derivatives Chemical class 0.000 description 1
- 238000005979 thermal decomposition reaction Methods 0.000 description 1
- 229910003454 ytterbium oxide Inorganic materials 0.000 description 1
- 229940075624 ytterbium oxide Drugs 0.000 description 1
- 229910052727 yttrium Inorganic materials 0.000 description 1
Landscapes
- Oxygen, Ozone, And Oxides In General (AREA)
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP62248957A JPH0193404A (ja) | 1987-10-01 | 1987-10-01 | ガーネット構造を持つ化合物の原料粉末の製造方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP62248957A JPH0193404A (ja) | 1987-10-01 | 1987-10-01 | ガーネット構造を持つ化合物の原料粉末の製造方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPH0193404A true JPH0193404A (ja) | 1989-04-12 |
| JPH0446884B2 JPH0446884B2 (enrdf_load_stackoverflow) | 1992-07-31 |
Family
ID=17185918
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP62248957A Granted JPH0193404A (ja) | 1987-10-01 | 1987-10-01 | ガーネット構造を持つ化合物の原料粉末の製造方法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPH0193404A (enrdf_load_stackoverflow) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO1995004701A1 (fr) * | 1993-08-11 | 1995-02-16 | Sumitomo Chemical Company, Limited | Poudre d'oxyde metallique composite et procede de production |
| JP2001158620A (ja) * | 1999-09-20 | 2001-06-12 | Shin Etsu Chem Co Ltd | 希土類・アルミニウム・ガーネット微粉末、その製造方法および該粉末を用いた焼結体 |
| EP1338556A3 (en) * | 2002-02-26 | 2004-01-07 | Sumitomo Chemical Company, Limited | Process for producing particles of a metal compound |
| US7691765B2 (en) | 2005-03-31 | 2010-04-06 | Fujifilm Corporation | Translucent material and manufacturing method of the same |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5696727A (en) * | 1979-11-09 | 1981-08-05 | Rhone Poulenc Ind | Manufacture of polycrystalline garnet and corresponding single crystal |
| JPS5696728A (en) * | 1979-11-09 | 1981-08-05 | Rhone Poulenc Ind | Manufacture of polycrystalline garnet containing at least one element selected from groups comprising aluminum and*or gallium and*or indium* rare earth element and yttrium and corresponding single cry |
-
1987
- 1987-10-01 JP JP62248957A patent/JPH0193404A/ja active Granted
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5696727A (en) * | 1979-11-09 | 1981-08-05 | Rhone Poulenc Ind | Manufacture of polycrystalline garnet and corresponding single crystal |
| JPS5696728A (en) * | 1979-11-09 | 1981-08-05 | Rhone Poulenc Ind | Manufacture of polycrystalline garnet containing at least one element selected from groups comprising aluminum and*or gallium and*or indium* rare earth element and yttrium and corresponding single cry |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO1995004701A1 (fr) * | 1993-08-11 | 1995-02-16 | Sumitomo Chemical Company, Limited | Poudre d'oxyde metallique composite et procede de production |
| JP2001158620A (ja) * | 1999-09-20 | 2001-06-12 | Shin Etsu Chem Co Ltd | 希土類・アルミニウム・ガーネット微粉末、その製造方法および該粉末を用いた焼結体 |
| EP1338556A3 (en) * | 2002-02-26 | 2004-01-07 | Sumitomo Chemical Company, Limited | Process for producing particles of a metal compound |
| US7691765B2 (en) | 2005-03-31 | 2010-04-06 | Fujifilm Corporation | Translucent material and manufacturing method of the same |
Also Published As
| Publication number | Publication date |
|---|---|
| JPH0446884B2 (enrdf_load_stackoverflow) | 1992-07-31 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| EXPY | Cancellation because of completion of term |