JP7372636B2 - ポリオールの製造プロセス - Google Patents

ポリオールの製造プロセス Download PDF

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Publication number
JP7372636B2
JP7372636B2 JP2020514574A JP2020514574A JP7372636B2 JP 7372636 B2 JP7372636 B2 JP 7372636B2 JP 2020514574 A JP2020514574 A JP 2020514574A JP 2020514574 A JP2020514574 A JP 2020514574A JP 7372636 B2 JP7372636 B2 JP 7372636B2
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Japan
Prior art keywords
catalyst
molecular weight
lewis acid
fluoroalkyl
polyether polyol
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JP2020514574A
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Japanese (ja)
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JP2020534391A (ja
Inventor
ラグラマン、アルジュン
エイチ． ヒース、ウィリアム
ムコーパデャイ、スクリット
エイ． スピニ―、ヒーサー
アール． ウィルソン、デイビット
エム． ノートスタイン、ジャスティン
ティー． グエン、ソンビン
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Dow Global Technologies LLC
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Dow Global Technologies LLC
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    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C08G65/2603—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing oxygen
    • C08G65/2606—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing oxygen containing hydroxyl groups
    • C08G65/2609—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing oxygen containing hydroxyl groups containing aliphatic hydroxyl groups
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C08G65/2642—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the catalyst used
    • C08G65/2645—Metals or compounds thereof, e.g. salts
    • C08G65/2654—Aluminium or boron; Compounds thereof
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/02—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides
    • B01J31/0272—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides containing elements other than those covered by B01J31/0201 - B01J31/0255
    • B01J31/0275—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides containing elements other than those covered by B01J31/0201 - B01J31/0255 also containing elements or functional groups covered by B01J31/0201 - B01J31/0269
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/02—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides
    • B01J31/12—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides containing organo-metallic compounds or metal hydrides
    • B01J31/14—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides containing organo-metallic compounds or metal hydrides of aluminium or boron
    • B01J31/143—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides containing organo-metallic compounds or metal hydrides of aluminium or boron of aluminium
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/40—High-molecular-weight compounds
    • C08G18/48—Polyethers
    • C08G18/4833—Polyethers containing oxyethylene units
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/40—High-molecular-weight compounds
    • C08G18/48—Polyethers
    • C08G18/4833—Polyethers containing oxyethylene units
    • C08G18/4837—Polyethers containing oxyethylene units and other oxyalkylene units
    • C08G18/4841—Polyethers containing oxyethylene units and other oxyalkylene units containing oxyethylene end groups
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C08G65/2642—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the catalyst used
    • C08G65/2645—Metals or compounds thereof, e.g. salts
    • C08G65/266—Metallic elements not covered by group C08G65/2648 - C08G65/2645, or compounds thereof
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C08G65/2642—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the catalyst used
    • C08G65/2669—Non-metals or compounds thereof
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C08G65/2642—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the catalyst used
    • C08G65/2669—Non-metals or compounds thereof
    • C08G65/2684—Halogens or compounds thereof
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2231/00—Catalytic reactions performed with catalysts classified in B01J31/00
    • B01J2231/20—Olefin oligomerisation or telomerisation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2531/00—Additional information regarding catalytic systems classified in B01J31/00
    • B01J2531/001—General concepts, e.g. reviews, relating to catalyst systems and methods of making them, the concept being defined by a common material or method/theory
    • B01J2531/002—Materials
    • B01J2531/004—Ligands
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C41/00—Preparation of ethers; Preparation of compounds having groups, groups or groups
    • C07C41/01—Preparation of ethers
    • C07C41/02—Preparation of ethers from oxiranes
    • C07C41/03—Preparation of ethers from oxiranes by reaction of oxirane rings with hydroxy groups

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Polyethers (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Polyurethanes Or Polyureas (AREA)
  • Catalysts (AREA)
  • Emergency Medicine (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
JP2020514574A 2017-09-14 2018-09-14 ポリオールの製造プロセス Active JP7372636B2 (ja)

Applications Claiming Priority (7)

Application Number Priority Date Filing Date Title
US201762558409P 2017-09-14 2017-09-14
US201762558422P 2017-09-14 2017-09-14
US62/558,409 2017-09-14
US62/558,422 2017-09-14
US201862635631P 2018-02-27 2018-02-27
US62/635,631 2018-02-27
PCT/US2018/050991 WO2019055731A1 (en) 2017-09-14 2018-09-14 PROCESS FOR PRODUCING POLYOLS

Publications (2)

Publication Number Publication Date
JP2020534391A JP2020534391A (ja) 2020-11-26
JP7372636B2 true JP7372636B2 (ja) 2023-11-01

Family

ID=63714126

Family Applications (2)

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JP2020514574A Active JP7372636B2 (ja) 2017-09-14 2018-09-14 ポリオールの製造プロセス
JP2020514509A Active JP7263323B2 (ja) 2017-09-14 2018-09-14 ポリオールの製造プロセス

Family Applications After (1)

Application Number Title Priority Date Filing Date
JP2020514509A Active JP7263323B2 (ja) 2017-09-14 2018-09-14 ポリオールの製造プロセス

Country Status (10)

Country Link
US (3) US11186683B2 (enExample)
EP (3) EP3681926B1 (enExample)
JP (2) JP7372636B2 (enExample)
KR (2) KR102603166B1 (enExample)
CN (3) CN111225937B (enExample)
ES (2) ES2982459T3 (enExample)
HU (2) HUE067017T2 (enExample)
PL (2) PL3681927T3 (enExample)
SG (2) SG11202002126WA (enExample)
WO (3) WO2019055725A1 (enExample)

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HUE067017T2 (hu) * 2017-09-14 2024-09-28 Univ Northwestern Eljárás poliolok gyártására
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EP4172241B1 (en) * 2020-06-24 2024-02-28 Dow Silicones Corporation Composition and method for reacting an organosilicon compound and a silyl hydride catalyzed by a fluorinated arylborane lewis acid
US12473404B2 (en) * 2020-06-24 2025-11-18 Dow Global Technologies Llc Composition and method for silyl hydride reaction catalyzed by fluorinated arylborane Lewis acids
EP4232493A1 (en) 2020-10-23 2023-08-30 Dow Global Technologies LLC Polyurethane composition
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JP2025501491A (ja) 2021-12-21 2025-01-22 ダウ グローバル テクノロジーズ エルエルシー ルイス酸触媒を使用するセミバッチアルキレンオキシド重合プロセス
JP2025512331A (ja) 2022-04-13 2025-04-17 ダウ グローバル テクノロジーズ エルエルシー ポリエーテル官能性有機ケイ素化合物の製造
EP4634263A1 (en) 2022-12-13 2025-10-22 Basf Se New ether-amine compositions and the use thereof as curing agents for epoxy resins
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Publication number Publication date
JP2020534391A (ja) 2020-11-26
EP3681926B1 (en) 2024-05-15
ES2981205T3 (es) 2024-10-07
KR102603117B1 (ko) 2023-11-17
CN111344331B (zh) 2023-02-21
CN111212866A (zh) 2020-05-29
PL3681927T3 (pl) 2024-07-15
US20200199294A1 (en) 2020-06-25
KR20200055739A (ko) 2020-05-21
KR102603166B1 (ko) 2023-11-16
WO2019055731A1 (en) 2019-03-21
US20200231738A1 (en) 2020-07-23
CN111225937A (zh) 2020-06-02
BR112020004916A2 (pt) 2020-09-15
CN111212866B (zh) 2023-02-21
EP3681929A1 (en) 2020-07-22
PL3681929T3 (pl) 2024-08-05
JP7263323B2 (ja) 2023-04-24
EP3681929B1 (en) 2024-05-08
WO2019055725A1 (en) 2019-03-21
CN111225937B (zh) 2023-02-21
JP2020534390A (ja) 2020-11-26
HUE067017T2 (hu) 2024-09-28
KR20200055742A (ko) 2020-05-21
CN111344331A (zh) 2020-06-26
SG11202002124VA (en) 2020-04-29
ES2982459T3 (es) 2024-10-16
EP3681926A1 (en) 2020-07-22
SG11202002126WA (en) 2020-04-29
EP3681927B1 (en) 2024-05-22
WO2019055741A1 (en) 2019-03-21
EP3681927A1 (en) 2020-07-22
HUE068772T2 (hu) 2025-01-28
US20210070920A1 (en) 2021-03-11
BR112020004888A2 (pt) 2020-09-15
US11479642B2 (en) 2022-10-25
US11186683B2 (en) 2021-11-30
US11198760B2 (en) 2021-12-14

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