JP7004646B2 - Na3V2(PO4)2F3粒子状物質の製造方法 - Google Patents

Na3V2(PO4)2F3粒子状物質の製造方法 Download PDF

Info

Publication number
JP7004646B2
JP7004646B2 JP2018519448A JP2018519448A JP7004646B2 JP 7004646 B2 JP7004646 B2 JP 7004646B2 JP 2018519448 A JP2018519448 A JP 2018519448A JP 2018519448 A JP2018519448 A JP 2018519448A JP 7004646 B2 JP7004646 B2 JP 7004646B2
Authority
JP
Japan
Prior art keywords
substance
present
carbon
atmosphere
primary particles
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
JP2018519448A
Other languages
English (en)
Japanese (ja)
Other versions
JP2018531871A5 (enExample
JP2018531871A (ja
Inventor
ハル,ニキータ
ブリノー,シルヴァン
クロガネック,ローレンス
ロノワ,セバスティアン
マスクリエ,クリスティアン
シモニン,ロイク
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Universite de Picardie Jules Verne
Commissariat a lEnergie Atomique et aux Energies Alternatives CEA
Original Assignee
Universite de Picardie Jules Verne
Commissariat a lEnergie Atomique et aux Energies Alternatives CEA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Universite de Picardie Jules Verne, Commissariat a lEnergie Atomique et aux Energies Alternatives CEA filed Critical Universite de Picardie Jules Verne
Publication of JP2018531871A publication Critical patent/JP2018531871A/ja
Publication of JP2018531871A5 publication Critical patent/JP2018531871A5/ja
Priority to JP2021133042A priority Critical patent/JP7301101B2/ja
Application granted granted Critical
Publication of JP7004646B2 publication Critical patent/JP7004646B2/ja
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Classifications

    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01BNON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B25/00Phosphorus; Compounds thereof
    • C01B25/16Oxyacids of phosphorus; Salts thereof
    • C01B25/26Phosphates
    • C01B25/455Phosphates containing halogen
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M4/36Selection of substances as active materials, active masses, active liquids
    • H01M4/58Selection of substances as active materials, active masses, active liquids of inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy; of polyanionic structures, e.g. phosphates, silicates or borates
    • H01M4/5825Oxygenated metallic salts or polyanionic structures, e.g. borates, phosphates, silicates, olivines
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2002/00Crystal-structural characteristics
    • C01P2002/20Two-dimensional structures
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/60Particles characterised by their size
    • C01P2004/61Micrometer sized, i.e. from 1-100 micrometer
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2004/00Particle morphology
    • C01P2004/60Particles characterised by their size
    • C01P2004/62Submicrometer sized, i.e. from 0.1-1 micrometer
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/12Surface area
    • CCHEMISTRY; METALLURGY
    • C01INORGANIC CHEMISTRY
    • C01PINDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
    • C01P2006/00Physical properties of inorganic compounds
    • C01P2006/40Electric properties
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M10/00Secondary cells; Manufacture thereof
    • H01M10/05Accumulators with non-aqueous electrolyte
    • H01M10/054Accumulators with insertion or intercalation of metals other than lithium, e.g. with magnesium or aluminium
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01MPROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
    • H01M4/00Electrodes
    • H01M4/02Electrodes composed of, or comprising, active material
    • H01M2004/026Electrodes composed of, or comprising, active material characterised by the polarity
    • H01M2004/028Positive electrodes
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02EREDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
    • Y02E60/00Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
    • Y02E60/10Energy storage using batteries

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • General Chemical & Material Sciences (AREA)
  • Electrochemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Materials Engineering (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Manufacturing & Machinery (AREA)
  • Battery Electrode And Active Subsutance (AREA)
  • Secondary Cells (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
JP2018519448A 2015-10-13 2016-10-13 Na3V2(PO4)2F3粒子状物質の製造方法 Active JP7004646B2 (ja)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP2021133042A JP7301101B2 (ja) 2015-10-13 2021-08-17 Na3V2(PO4)2F3粒子状物質の製造方法

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
FR1559709A FR3042313B1 (fr) 2015-10-13 2015-10-13 Procede de preparation d'un materiau particulaire na3v2(po4)2f3
FR1559709 2015-10-13
PCT/EP2016/074597 WO2017064189A1 (fr) 2015-10-13 2016-10-13 Procede de preparation d'un materiau particulaire na3v2(po4)2f3

Related Child Applications (1)

Application Number Title Priority Date Filing Date
JP2021133042A Division JP7301101B2 (ja) 2015-10-13 2021-08-17 Na3V2(PO4)2F3粒子状物質の製造方法

Publications (3)

Publication Number Publication Date
JP2018531871A JP2018531871A (ja) 2018-11-01
JP2018531871A5 JP2018531871A5 (enExample) 2020-04-02
JP7004646B2 true JP7004646B2 (ja) 2022-02-04

Family

ID=55589932

Family Applications (2)

Application Number Title Priority Date Filing Date
JP2018519448A Active JP7004646B2 (ja) 2015-10-13 2016-10-13 Na3V2(PO4)2F3粒子状物質の製造方法
JP2021133042A Active JP7301101B2 (ja) 2015-10-13 2021-08-17 Na3V2(PO4)2F3粒子状物質の製造方法

Family Applications After (1)

Application Number Title Priority Date Filing Date
JP2021133042A Active JP7301101B2 (ja) 2015-10-13 2021-08-17 Na3V2(PO4)2F3粒子状物質の製造方法

Country Status (9)

Country Link
US (1) US11040881B2 (enExample)
EP (1) EP3484814B1 (enExample)
JP (2) JP7004646B2 (enExample)
KR (1) KR102743837B1 (enExample)
CN (1) CN108349738B (enExample)
FR (1) FR3042313B1 (enExample)
HU (1) HUE047790T2 (enExample)
PL (1) PL3484814T3 (enExample)
WO (1) WO2017064189A1 (enExample)

Families Citing this family (18)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR3062384B1 (fr) * 2017-02-01 2021-02-12 Centre Nat Rech Scient Procede de preparation d'un materiau composite phosphate de vanadium-carbone par voie liquide
FR3067709B1 (fr) * 2017-06-16 2020-06-19 Rhodia Operations Procede de preparation d'un phosphate de vanadium
CN116598479A (zh) * 2018-06-27 2023-08-15 宁德时代新能源科技股份有限公司 正极活性材料、正极极片及钠离子二次电池
CN112512966B (zh) * 2018-07-30 2024-02-20 罗地亚经营管理公司 正极组合物
CN110092366B (zh) * 2019-04-25 2023-03-31 西北工业大学 一种复相磷酸钒钠电极材料及其制备方法
CN112216823B (zh) * 2019-07-10 2022-03-08 上海交通大学 氟磷酸钒钠包覆正极材料、钠离子电池及其制备方法和应用
CN112864358B (zh) * 2019-11-27 2023-11-07 中国科学院大连化学物理研究所 一种一步法制备的钒基聚阴离子型化合物及应用
CN111606314B (zh) * 2020-06-04 2023-05-26 哈尔滨工业大学 一种钠离子电池正极材料三氟磷酸钒钠的制备方法
CN111943161B (zh) * 2020-08-24 2022-05-17 西北大学 一种氟磷酸钒钠和碳复合的二次电池正极材料的制备方法及其应用
CN114538400A (zh) * 2020-11-24 2022-05-27 天津理工大学 多元阳离子取代磷酸盐电极材料及其制备方法
CN113293459A (zh) * 2021-05-24 2021-08-24 中南大学 一种介孔纳米纤维氟磷酸钒钠正极材料及其制备方法
CN113764662A (zh) * 2021-07-29 2021-12-07 武汉理工大学 一种碳包覆磷酸钒钛锰钠微米球及其制备方法与应用
CN114572957B (zh) * 2022-02-22 2023-03-28 鞍钢集团北京研究院有限公司 一种磷酸钒钠材料的制备方法
CN114572958B (zh) * 2022-03-04 2023-03-21 湖南大学 一种含氟聚阴离子型正极材料的制备方法及含氟聚阴离子型正极材料
CN114933293B (zh) * 2022-04-29 2024-06-14 广州鹏辉能源科技股份有限公司 氟磷酸钒钠的制备和在钠离子电池中的应用
CN118281179B (zh) * 2022-12-29 2025-11-11 比亚迪股份有限公司 钠电池用正极材料及其制备方法、正极极片、钠电池
WO2025003375A1 (en) 2023-06-30 2025-01-02 Specialty Operations France Positive electrode composition
CN119008903A (zh) * 2024-08-19 2024-11-22 湖北万润新能源科技股份有限公司 一种碳包覆氟磷酸钒钠正极材料及其制备方法、正极极片和二次电池

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2004533706A (ja) 2001-04-06 2004-11-04 ヴァレンス テクノロジー インコーポレーテッド ナトリウムイオンバッテリ
JP2014179317A (ja) 2013-02-18 2014-09-25 Semiconductor Energy Lab Co Ltd 蓄電池用電極

Family Cites Families (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20070160519A1 (en) * 2005-03-28 2007-07-12 Jeremy Barker Method Of Making Active Materials For Use In Secondary Electrochemical Cells
CN101369661A (zh) * 2008-10-17 2009-02-18 吉林大学 一种钠基锂离子二次电池正极材料及其制备方法
WO2010080519A1 (en) * 2008-12-19 2010-07-15 Conocophillips Company Process for making fluorinated lithium vanadium polyanion powders for batteries
CN102306771A (zh) * 2011-08-17 2012-01-04 中南大学 一种混合离子电池氟磷酸钒钠正极材料的制备方法
JP2013089391A (ja) * 2011-10-14 2013-05-13 Kyushu Univ ナトリウムイオン二次電池用の電極活物質
CN102509789A (zh) * 2011-10-17 2012-06-20 中南大学 一种制备含钠锂离子电池正极材料掺氟磷酸钒钠的方法
CN103022490A (zh) * 2012-12-31 2013-04-03 广西地博矿业集团股份有限公司 钠离子电池正极材料氟磷酸钒钠的制备方法
WO2015067316A1 (en) * 2013-11-08 2015-05-14 MAX-PLANCK-Gesellschaft zur Förderung der Wissenschaften e.V. Method of manufacturing an electrode material, electrode material and vehicle comprising a battery including such an electrode material
US9564656B1 (en) * 2015-09-14 2017-02-07 Nanotek Instruments, Inc. Process for producing alkali metal or alkali-ion batteries having high volumetric and gravimetric energy densities

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2004533706A (ja) 2001-04-06 2004-11-04 ヴァレンス テクノロジー インコーポレーテッド ナトリウムイオンバッテリ
JP2014179317A (ja) 2013-02-18 2014-09-25 Semiconductor Energy Lab Co Ltd 蓄電池用電極

Also Published As

Publication number Publication date
FR3042313A1 (fr) 2017-04-14
HUE047790T2 (hu) 2020-05-28
CN108349738A (zh) 2018-07-31
JP7301101B2 (ja) 2023-06-30
WO2017064189A1 (fr) 2017-04-20
EP3484814A1 (fr) 2019-05-22
CN108349738B (zh) 2023-02-21
US11040881B2 (en) 2021-06-22
KR102743837B1 (ko) 2024-12-17
FR3042313B1 (fr) 2020-04-03
JP2021185125A (ja) 2021-12-09
JP2018531871A (ja) 2018-11-01
PL3484814T3 (pl) 2020-06-01
US20180297847A1 (en) 2018-10-18
EP3484814B1 (fr) 2019-11-20
KR20180072708A (ko) 2018-06-29

Similar Documents

Publication Publication Date Title
JP7301101B2 (ja) Na3V2(PO4)2F3粒子状物質の製造方法
Javed et al. The emergence of 2D MXenes based Zn‐ion batteries: recent development and prospects
Liu et al. Carbon-coated Na 3 V 2 (PO 4) 2 F 3 nanoparticles embedded in a mesoporous carbon matrix as a potential cathode material for sodium-ion batteries with superior rate capability and long-term cycle life
Kashale et al. Biosynthesized Co-doped TiO2 nanoparticles based anode for lithium-ion battery application and investigating the influence of dopant concentrations on its performance
JP6228142B2 (ja) 電極物質として使用する硫酸塩
US8623549B2 (en) Iron oxyfluoride electrodes for electrochemical energy storage
EP3371104B1 (en) Direct synthesis of carbon doped tio2-bronze nanostructures as anode materials for high performance lithium batteries
JP6288257B2 (ja) ナノシリコン材料とその製造方法及び二次電池の負極
WO2010089931A1 (ja) リチウムシリケート系化合物の製造方法
US8951668B2 (en) Iron oxyfluoride electrodes for electrochemical energy storage
US20140099560A1 (en) Mesoporous metal oxide microsphere electrode compositions and their methods of making
JP6176510B2 (ja) シリコン材料及び二次電池の負極
Yan et al. Multicore closely packed ultrathin-MnO 2@ N-doped carbon-gear yolk–shell micro-nanostructures as highly efficient sulfur hosts for Li–S batteries
KR20140023858A (ko) 리튬이차전지용 실리콘 복합재 음극활물질, 이의 제조방법 및 이를 포함하는 리튬이차전지
JP6042512B2 (ja) 二次電池用正極活物質及びその製造方法
KR102075929B1 (ko) 리튬 이차전지용 TiO2 기반 산화물 복합체 및 이의 제조방법
Zhao et al. Influence of phase variation of ZnMn2O4/carbon electrodes on cycling performances of Li-ion batteries
Lokeswararao et al. Enabling high-rate capability by combining sol-gel synthesis and solid-state reaction with PTFE of 4.2 V cathode material LiVPO4F/C
JP6176511B2 (ja) シリコン材料及び二次電池の負極
Grishanova et al. Evaluation of Ti3C2Tx MXene-supported germanium sulfide as sodium-ion battery anodes: A comparison with reduced graphene oxide supports
La et al. Biphasic interactions between Na4Fe3 (PO4) 2P2O7 and Na3V2 (PO4) 3 to achieve ultra-long lifespan cathode material for sodium-ion batteries
Xiong et al. A 3D interconnected NH 4 Fe 0.6 V 2.4 O 7.4@ C nanocomposite with superior sodium storage properties
Wang et al. Nanoporous ZnGa2O4-modified separator as a multifunctional polysulphide barrier for advanced lithium-sulfur batteries
WO2014155408A1 (ja) 水素含有リチウムシリケート系化合物及びその製造方法、並びに非水電解質二次電池用正極活物質、非水電解質二次電池用正極、及び非水電解質二次電池

Legal Events

Date Code Title Description
A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20190913

A621 Written request for application examination

Free format text: JAPANESE INTERMEDIATE CODE: A621

Effective date: 20190913

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20200220

A977 Report on retrieval

Free format text: JAPANESE INTERMEDIATE CODE: A971007

Effective date: 20200630

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20200729

A601 Written request for extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A601

Effective date: 20201027

A601 Written request for extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A601

Effective date: 20201228

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20210128

A02 Decision of refusal

Free format text: JAPANESE INTERMEDIATE CODE: A02

Effective date: 20210419

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20210817

C60 Trial request (containing other claim documents, opposition documents)

Free format text: JAPANESE INTERMEDIATE CODE: C60

Effective date: 20210817

C11 Written invitation by the commissioner to file amendments

Free format text: JAPANESE INTERMEDIATE CODE: C11

Effective date: 20210903

A911 Transfer to examiner for re-examination before appeal (zenchi)

Free format text: JAPANESE INTERMEDIATE CODE: A911

Effective date: 20211001

C21 Notice of transfer of a case for reconsideration by examiners before appeal proceedings

Free format text: JAPANESE INTERMEDIATE CODE: C21

Effective date: 20211011

TRDD Decision of grant or rejection written
A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

Effective date: 20211206

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20220104

R150 Certificate of patent or registration of utility model

Ref document number: 7004646

Country of ref document: JP

Free format text: JAPANESE INTERMEDIATE CODE: R150

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250