FR3042313B1 - Procede de preparation d'un materiau particulaire na3v2(po4)2f3 - Google Patents
Procede de preparation d'un materiau particulaire na3v2(po4)2f3 Download PDFInfo
- Publication number
- FR3042313B1 FR3042313B1 FR1559709A FR1559709A FR3042313B1 FR 3042313 B1 FR3042313 B1 FR 3042313B1 FR 1559709 A FR1559709 A FR 1559709A FR 1559709 A FR1559709 A FR 1559709A FR 3042313 B1 FR3042313 B1 FR 3042313B1
- Authority
- FR
- France
- Prior art keywords
- na3v2
- preparation
- vpo4
- mixture
- under
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 229910001373 Na3V2(PO4)2F3 Inorganic materials 0.000 title abstract 3
- 238000000034 method Methods 0.000 title abstract 2
- 238000002360 preparation method Methods 0.000 title abstract 2
- 239000011236 particulate material Substances 0.000 title 1
- PUZPDOWCWNUUKD-UHFFFAOYSA-M sodium fluoride Chemical compound [F-].[Na+] PUZPDOWCWNUUKD-UHFFFAOYSA-M 0.000 abstract 4
- 239000000463 material Substances 0.000 abstract 3
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 abstract 2
- 229910052799 carbon Inorganic materials 0.000 abstract 2
- 150000001875 compounds Chemical class 0.000 abstract 2
- 239000000203 mixture Substances 0.000 abstract 2
- 235000013024 sodium fluoride Nutrition 0.000 abstract 2
- 239000011775 sodium fluoride Substances 0.000 abstract 2
- 239000004215 Carbon black (E152) Substances 0.000 abstract 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical group C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 abstract 1
- 229910019142 PO4 Inorganic materials 0.000 abstract 1
- XHCLAFWTIXFWPH-UHFFFAOYSA-N [O-2].[O-2].[O-2].[O-2].[O-2].[V+5].[V+5] Chemical compound [O-2].[O-2].[O-2].[O-2].[O-2].[V+5].[V+5] XHCLAFWTIXFWPH-UHFFFAOYSA-N 0.000 abstract 1
- GLMOMDXKLRBTDY-UHFFFAOYSA-A [V+5].[V+5].[V+5].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O Chemical compound [V+5].[V+5].[V+5].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O GLMOMDXKLRBTDY-UHFFFAOYSA-A 0.000 abstract 1
- 238000001354 calcination Methods 0.000 abstract 1
- 239000007772 electrode material Substances 0.000 abstract 1
- 229930195733 hydrocarbon Natural products 0.000 abstract 1
- 150000002430 hydrocarbons Chemical class 0.000 abstract 1
- 239000010452 phosphate Substances 0.000 abstract 1
- -1 phosphate anion Chemical class 0.000 abstract 1
- 239000002243 precursor Substances 0.000 abstract 1
- 229910052708 sodium Inorganic materials 0.000 abstract 1
- 239000011734 sodium Substances 0.000 abstract 1
- 229910001935 vanadium oxide Inorganic materials 0.000 abstract 1
- 239000012002 vanadium phosphate Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B25/00—Phosphorus; Compounds thereof
- C01B25/16—Oxyacids of phosphorus; Salts thereof
- C01B25/26—Phosphates
- C01B25/455—Phosphates containing halogen
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M10/00—Secondary cells; Manufacture thereof
- H01M10/05—Accumulators with non-aqueous electrolyte
- H01M10/054—Accumulators with insertion or intercalation of metals other than lithium, e.g. with magnesium or aluminium
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/36—Selection of substances as active materials, active masses, active liquids
- H01M4/58—Selection of substances as active materials, active masses, active liquids of inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy; of polyanionic structures, e.g. phosphates, silicates or borates
- H01M4/5825—Oxygenated metallic salts or polyanionic structures, e.g. borates, phosphates, silicates, olivines
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2002/00—Crystal-structural characteristics
- C01P2002/20—Two-dimensional structures
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/60—Particles characterised by their size
- C01P2004/61—Micrometer sized, i.e. from 1-100 micrometer
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/60—Particles characterised by their size
- C01P2004/62—Submicrometer sized, i.e. from 0.1-1 micrometer
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/12—Surface area
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/40—Electric properties
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M2004/026—Electrodes composed of, or comprising, active material characterised by the polarity
- H01M2004/028—Positive electrodes
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/10—Energy storage using batteries
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- General Chemical & Material Sciences (AREA)
- Electrochemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Materials Engineering (AREA)
- Crystallography & Structural Chemistry (AREA)
- Manufacturing & Machinery (AREA)
- Battery Electrode And Active Subsutance (AREA)
- Secondary Cells (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
Priority Applications (10)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR1559709A FR3042313B1 (fr) | 2015-10-13 | 2015-10-13 | Procede de preparation d'un materiau particulaire na3v2(po4)2f3 |
| PL16781440T PL3484814T3 (pl) | 2015-10-13 | 2016-10-13 | Sposób wytwarzania materiału w postaci cząstek Na<sub>3</sub>V<sub>2</sub>(PO<sub>4</sub>)<sub>2</sub>F<sub>3</sub> |
| EP16781440.9A EP3484814B1 (fr) | 2015-10-13 | 2016-10-13 | Procede de preparation d'un materiau particulaire na3v2(po4)2f3 |
| CN201680060268.1A CN108349738B (zh) | 2015-10-13 | 2016-10-13 | 制备Na3V2(PO4)2F3颗粒材料的方法 |
| KR1020187011926A KR102743837B1 (ko) | 2015-10-13 | 2016-10-13 | Na3V2(PO4)2F3 미립자 물질의 제조 방법 |
| HUE16781440A HUE047790T2 (hu) | 2015-10-13 | 2016-10-13 | Eljárás Na3V2(PO4)2F3 szemcsés anyag elõállítására |
| PCT/EP2016/074597 WO2017064189A1 (fr) | 2015-10-13 | 2016-10-13 | Procede de preparation d'un materiau particulaire na3v2(po4)2f3 |
| US15/767,472 US11040881B2 (en) | 2015-10-13 | 2016-10-13 | Method for preparing a NA3V2(PO4)2F3 particulate material |
| JP2018519448A JP7004646B2 (ja) | 2015-10-13 | 2016-10-13 | Ｎａ３Ｖ２（ＰＯ４）２Ｆ３粒子状物質の製造方法 |
| JP2021133042A JP7301101B2 (ja) | 2015-10-13 | 2021-08-17 | Ｎａ３Ｖ２（ＰＯ４）２Ｆ３粒子状物質の製造方法 |
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| FR1559709A FR3042313B1 (fr) | 2015-10-13 | 2015-10-13 | Procede de preparation d'un materiau particulaire na3v2(po4)2f3 |
| FR1559709 | 2015-10-13 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| FR3042313A1 FR3042313A1 (fr) | 2017-04-14 |
| FR3042313B1 true FR3042313B1 (fr) | 2020-04-03 |
Family
ID=55589932
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| FR1559709A Expired - Fee Related FR3042313B1 (fr) | 2015-10-13 | 2015-10-13 | Procede de preparation d'un materiau particulaire na3v2(po4)2f3 |
Country Status (9)
| Country | Link |
|---|---|
| US (1) | US11040881B2 (enExample) |
| EP (1) | EP3484814B1 (enExample) |
| JP (2) | JP7004646B2 (enExample) |
| KR (1) | KR102743837B1 (enExample) |
| CN (1) | CN108349738B (enExample) |
| FR (1) | FR3042313B1 (enExample) |
| HU (1) | HUE047790T2 (enExample) |
| PL (1) | PL3484814T3 (enExample) |
| WO (1) | WO2017064189A1 (enExample) |
Families Citing this family (18)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR3062384B1 (fr) * | 2017-02-01 | 2021-02-12 | Centre Nat Rech Scient | Procede de preparation d'un materiau composite phosphate de vanadium-carbone par voie liquide |
| FR3067709B1 (fr) * | 2017-06-16 | 2020-06-19 | Rhodia Operations | Procede de preparation d'un phosphate de vanadium |
| CN116598479A (zh) * | 2018-06-27 | 2023-08-15 | 宁德时代新能源科技股份有限公司 | 正极活性材料、正极极片及钠离子二次电池 |
| CN112512966B (zh) * | 2018-07-30 | 2024-02-20 | 罗地亚经营管理公司 | 正极组合物 |
| CN110092366B (zh) * | 2019-04-25 | 2023-03-31 | 西北工业大学 | 一种复相磷酸钒钠电极材料及其制备方法 |
| CN112216823B (zh) * | 2019-07-10 | 2022-03-08 | 上海交通大学 | 氟磷酸钒钠包覆正极材料、钠离子电池及其制备方法和应用 |
| CN112864358B (zh) * | 2019-11-27 | 2023-11-07 | 中国科学院大连化学物理研究所 | 一种一步法制备的钒基聚阴离子型化合物及应用 |
| CN111606314B (zh) * | 2020-06-04 | 2023-05-26 | 哈尔滨工业大学 | 一种钠离子电池正极材料三氟磷酸钒钠的制备方法 |
| CN111943161B (zh) * | 2020-08-24 | 2022-05-17 | 西北大学 | 一种氟磷酸钒钠和碳复合的二次电池正极材料的制备方法及其应用 |
| CN114538400A (zh) * | 2020-11-24 | 2022-05-27 | 天津理工大学 | 多元阳离子取代磷酸盐电极材料及其制备方法 |
| CN113293459A (zh) * | 2021-05-24 | 2021-08-24 | 中南大学 | 一种介孔纳米纤维氟磷酸钒钠正极材料及其制备方法 |
| CN113764662A (zh) * | 2021-07-29 | 2021-12-07 | 武汉理工大学 | 一种碳包覆磷酸钒钛锰钠微米球及其制备方法与应用 |
| CN114572957B (zh) * | 2022-02-22 | 2023-03-28 | 鞍钢集团北京研究院有限公司 | 一种磷酸钒钠材料的制备方法 |
| CN114572958B (zh) * | 2022-03-04 | 2023-03-21 | 湖南大学 | 一种含氟聚阴离子型正极材料的制备方法及含氟聚阴离子型正极材料 |
| CN114933293B (zh) * | 2022-04-29 | 2024-06-14 | 广州鹏辉能源科技股份有限公司 | 氟磷酸钒钠的制备和在钠离子电池中的应用 |
| CN118281179B (zh) * | 2022-12-29 | 2025-11-11 | 比亚迪股份有限公司 | 钠电池用正极材料及其制备方法、正极极片、钠电池 |
| WO2025003375A1 (en) | 2023-06-30 | 2025-01-02 | Specialty Operations France | Positive electrode composition |
| CN119008903A (zh) * | 2024-08-19 | 2024-11-22 | 湖北万润新能源科技股份有限公司 | 一种碳包覆氟磷酸钒钠正极材料及其制备方法、正极极片和二次电池 |
Family Cites Families (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR100814540B1 (ko) * | 2001-04-06 | 2008-03-17 | 발렌스 테크놀로지, 인코포레이티드 | 나트륨 이온 배터리 |
| US20070160519A1 (en) * | 2005-03-28 | 2007-07-12 | Jeremy Barker | Method Of Making Active Materials For Use In Secondary Electrochemical Cells |
| CN101369661A (zh) * | 2008-10-17 | 2009-02-18 | 吉林大学 | 一种钠基锂离子二次电池正极材料及其制备方法 |
| WO2010080519A1 (en) * | 2008-12-19 | 2010-07-15 | Conocophillips Company | Process for making fluorinated lithium vanadium polyanion powders for batteries |
| CN102306771A (zh) * | 2011-08-17 | 2012-01-04 | 中南大学 | 一种混合离子电池氟磷酸钒钠正极材料的制备方法 |
| JP2013089391A (ja) * | 2011-10-14 | 2013-05-13 | Kyushu Univ | ナトリウムイオン二次電池用の電極活物質 |
| CN102509789A (zh) * | 2011-10-17 | 2012-06-20 | 中南大学 | 一种制备含钠锂离子电池正极材料掺氟磷酸钒钠的方法 |
| CN103022490A (zh) * | 2012-12-31 | 2013-04-03 | 广西地博矿业集团股份有限公司 | 钠离子电池正极材料氟磷酸钒钠的制备方法 |
| US9673454B2 (en) | 2013-02-18 | 2017-06-06 | Semiconductor Energy Laboratory Co., Ltd. | Sodium-ion secondary battery |
| WO2015067316A1 (en) * | 2013-11-08 | 2015-05-14 | MAX-PLANCK-Gesellschaft zur Förderung der Wissenschaften e.V. | Method of manufacturing an electrode material, electrode material and vehicle comprising a battery including such an electrode material |
| US9564656B1 (en) * | 2015-09-14 | 2017-02-07 | Nanotek Instruments, Inc. | Process for producing alkali metal or alkali-ion batteries having high volumetric and gravimetric energy densities |
-
2015
- 2015-10-13 FR FR1559709A patent/FR3042313B1/fr not_active Expired - Fee Related
-
2016
- 2016-10-13 EP EP16781440.9A patent/EP3484814B1/fr active Active
- 2016-10-13 KR KR1020187011926A patent/KR102743837B1/ko active Active
- 2016-10-13 US US15/767,472 patent/US11040881B2/en active Active
- 2016-10-13 HU HUE16781440A patent/HUE047790T2/hu unknown
- 2016-10-13 CN CN201680060268.1A patent/CN108349738B/zh active Active
- 2016-10-13 JP JP2018519448A patent/JP7004646B2/ja active Active
- 2016-10-13 WO PCT/EP2016/074597 patent/WO2017064189A1/fr not_active Ceased
- 2016-10-13 PL PL16781440T patent/PL3484814T3/pl unknown
-
2021
- 2021-08-17 JP JP2021133042A patent/JP7301101B2/ja active Active
Also Published As
| Publication number | Publication date |
|---|---|
| FR3042313A1 (fr) | 2017-04-14 |
| HUE047790T2 (hu) | 2020-05-28 |
| CN108349738A (zh) | 2018-07-31 |
| JP7301101B2 (ja) | 2023-06-30 |
| WO2017064189A1 (fr) | 2017-04-20 |
| EP3484814A1 (fr) | 2019-05-22 |
| CN108349738B (zh) | 2023-02-21 |
| US11040881B2 (en) | 2021-06-22 |
| KR102743837B1 (ko) | 2024-12-17 |
| JP7004646B2 (ja) | 2022-02-04 |
| JP2021185125A (ja) | 2021-12-09 |
| JP2018531871A (ja) | 2018-11-01 |
| PL3484814T3 (pl) | 2020-06-01 |
| US20180297847A1 (en) | 2018-10-18 |
| EP3484814B1 (fr) | 2019-11-20 |
| KR20180072708A (ko) | 2018-06-29 |
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