JP6459132B2 - SiCエピタキシャルウェハ及びその製造方法、並びに、欠陥識別方法 - Google Patents
SiCエピタキシャルウェハ及びその製造方法、並びに、欠陥識別方法 Download PDFInfo
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- JP6459132B2 JP6459132B2 JP2016186062A JP2016186062A JP6459132B2 JP 6459132 B2 JP6459132 B2 JP 6459132B2 JP 2016186062 A JP2016186062 A JP 2016186062A JP 2016186062 A JP2016186062 A JP 2016186062A JP 6459132 B2 JP6459132 B2 JP 6459132B2
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- 230000007547 defect Effects 0.000 title claims description 285
- 238000000034 method Methods 0.000 title claims description 45
- 238000004519 manufacturing process Methods 0.000 title claims description 40
- 239000000758 substrate Substances 0.000 claims description 224
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims description 134
- 229910052799 carbon Inorganic materials 0.000 claims description 133
- 239000013078 crystal Substances 0.000 claims description 102
- 230000003287 optical effect Effects 0.000 claims description 14
- 238000005424 photoluminescence Methods 0.000 claims description 10
- 230000008569 process Effects 0.000 claims description 3
- 229910010271 silicon carbide Inorganic materials 0.000 description 216
- HBMJWWWQQXIZIP-UHFFFAOYSA-N silicon carbide Chemical compound [Si+]#[C-] HBMJWWWQQXIZIP-UHFFFAOYSA-N 0.000 description 203
- 235000012431 wafers Nutrition 0.000 description 73
- 238000006243 chemical reaction Methods 0.000 description 57
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- ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical compound CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 description 4
- 239000007789 gas Substances 0.000 description 4
- 241000239290 Araneae Species 0.000 description 3
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 3
- 238000005229 chemical vapour deposition Methods 0.000 description 3
- 230000003247 decreasing effect Effects 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 229910052710 silicon Inorganic materials 0.000 description 3
- 238000000859 sublimation Methods 0.000 description 3
- 230000008022 sublimation Effects 0.000 description 3
- 244000000626 Daucus carota Species 0.000 description 2
- 235000002767 Daucus carota Nutrition 0.000 description 2
- BLRPTPMANUNPDV-UHFFFAOYSA-N Silane Chemical compound [SiH4] BLRPTPMANUNPDV-UHFFFAOYSA-N 0.000 description 2
- 239000012159 carrier gas Substances 0.000 description 2
- 230000006866 deterioration Effects 0.000 description 2
- 229910002804 graphite Inorganic materials 0.000 description 2
- 239000010439 graphite Substances 0.000 description 2
- 239000001257 hydrogen Substances 0.000 description 2
- 229910052739 hydrogen Inorganic materials 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 238000007689 inspection Methods 0.000 description 2
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- 238000005259 measurement Methods 0.000 description 2
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- 239000001294 propane Substances 0.000 description 2
- 239000004065 semiconductor Substances 0.000 description 2
- 229910000077 silane Inorganic materials 0.000 description 2
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 1
- 230000004888 barrier function Effects 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 229910003460 diamond Inorganic materials 0.000 description 1
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- 238000001953 recrystallisation Methods 0.000 description 1
- 238000011160 research Methods 0.000 description 1
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- 239000007787 solid Substances 0.000 description 1
- 241000894007 species Species 0.000 description 1
- 238000001228 spectrum Methods 0.000 description 1
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Classifications
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- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B29/00—Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape
- C30B29/10—Inorganic compounds or compositions
- C30B29/36—Carbides
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- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C16/00—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes
- C23C16/22—Chemical coating by decomposition of gaseous compounds, without leaving reaction products of surface material in the coating, i.e. chemical vapour deposition [CVD] processes characterised by the deposition of inorganic material, other than metallic material
- C23C16/30—Deposition of compounds, mixtures or solid solutions, e.g. borides, carbides, nitrides
- C23C16/32—Carbides
- C23C16/325—Silicon carbide
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- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B25/00—Single-crystal growth by chemical reaction of reactive gases, e.g. chemical vapour-deposition growth
- C30B25/02—Epitaxial-layer growth
- C30B25/16—Controlling or regulating
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- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B25/00—Single-crystal growth by chemical reaction of reactive gases, e.g. chemical vapour-deposition growth
- C30B25/02—Epitaxial-layer growth
- C30B25/18—Epitaxial-layer growth characterised by the substrate
- C30B25/20—Epitaxial-layer growth characterised by the substrate the substrate being of the same materials as the epitaxial layer
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- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/84—Systems specially adapted for particular applications
- G01N21/88—Investigating the presence of flaws or contamination
- G01N21/95—Investigating the presence of flaws or contamination characterised by the material or shape of the object to be examined
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01L—SEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
- H01L21/00—Processes or apparatus adapted for the manufacture or treatment of semiconductor or solid state devices or of parts thereof
- H01L21/02—Manufacture or treatment of semiconductor devices or of parts thereof
- H01L21/02104—Forming layers
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- H01L21/02—Manufacture or treatment of semiconductor devices or of parts thereof
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- H01L21/02433—Crystal orientation
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- H01L21/02—Manufacture or treatment of semiconductor devices or of parts thereof
- H01L21/02104—Forming layers
- H01L21/02365—Forming inorganic semiconducting materials on a substrate
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- H01L21/02447—Silicon carbide
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- H—ELECTRICITY
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- H01L—SEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
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- H01L21/02518—Deposited layers
- H01L21/02521—Materials
- H01L21/02524—Group 14 semiconducting materials
- H01L21/02529—Silicon carbide
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- H—ELECTRICITY
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- H01L—SEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
- H01L21/00—Processes or apparatus adapted for the manufacture or treatment of semiconductor or solid state devices or of parts thereof
- H01L21/02—Manufacture or treatment of semiconductor devices or of parts thereof
- H01L21/02104—Forming layers
- H01L21/02365—Forming inorganic semiconducting materials on a substrate
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- H01L21/02365—Forming inorganic semiconducting materials on a substrate
- H01L21/02612—Formation types
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- H01L21/02634—Homoepitaxy
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- H—ELECTRICITY
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- H01L22/00—Testing or measuring during manufacture or treatment; Reliability measurements, i.e. testing of parts without further processing to modify the parts as such; Structural arrangements therefor
- H01L22/10—Measuring as part of the manufacturing process
- H01L22/12—Measuring as part of the manufacturing process for structural parameters, e.g. thickness, line width, refractive index, temperature, warp, bond strength, defects, optical inspection, electrical measurement of structural dimensions, metallurgic measurement of diffusions
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01L—SEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
- H01L29/00—Semiconductor devices specially adapted for rectifying, amplifying, oscillating or switching and having potential barriers; Capacitors or resistors having potential barriers, e.g. a PN-junction depletion layer or carrier concentration layer; Details of semiconductor bodies or of electrodes thereof ; Multistep manufacturing processes therefor
- H01L29/02—Semiconductor bodies ; Multistep manufacturing processes therefor
- H01L29/12—Semiconductor bodies ; Multistep manufacturing processes therefor characterised by the materials of which they are formed
- H01L29/16—Semiconductor bodies ; Multistep manufacturing processes therefor characterised by the materials of which they are formed including, apart from doping materials or other impurities, only elements of Group IV of the Periodic Table
- H01L29/1608—Silicon carbide
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- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01L—SEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
- H01L29/00—Semiconductor devices specially adapted for rectifying, amplifying, oscillating or switching and having potential barriers; Capacitors or resistors having potential barriers, e.g. a PN-junction depletion layer or carrier concentration layer; Details of semiconductor bodies or of electrodes thereof ; Multistep manufacturing processes therefor
- H01L29/02—Semiconductor bodies ; Multistep manufacturing processes therefor
- H01L29/30—Semiconductor bodies ; Multistep manufacturing processes therefor characterised by physical imperfections; having polished or roughened surface
- H01L29/32—Semiconductor bodies ; Multistep manufacturing processes therefor characterised by physical imperfections; having polished or roughened surface the imperfections being within the semiconductor body
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- Engineering & Computer Science (AREA)
- Chemical & Material Sciences (AREA)
- Microelectronics & Electronic Packaging (AREA)
- Power Engineering (AREA)
- Physics & Mathematics (AREA)
- General Physics & Mathematics (AREA)
- Computer Hardware Design (AREA)
- Manufacturing & Machinery (AREA)
- Condensed Matter Physics & Semiconductors (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Crystallography & Structural Chemistry (AREA)
- Metallurgy (AREA)
- General Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Ceramic Engineering (AREA)
- Pathology (AREA)
- Theoretical Computer Science (AREA)
- Immunology (AREA)
- Analytical Chemistry (AREA)
- Quality & Reliability (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Biochemistry (AREA)
- Health & Medical Sciences (AREA)
- Computer Vision & Pattern Recognition (AREA)
- Mechanical Engineering (AREA)
- Crystals, And After-Treatments Of Crystals (AREA)
- Recrystallisation Techniques (AREA)
- Chemical Vapour Deposition (AREA)
- Testing Or Measuring Of Semiconductors Or The Like (AREA)
Priority Applications (6)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201780051959.XA CN109642342B (zh) | 2016-08-31 | 2017-08-21 | SiC外延晶片及其制造方法、以及缺陷识别方法 |
TW106128221A TWI630292B (zh) | 2016-08-31 | 2017-08-21 | SiC磊晶晶圓及其製造方法、以及缺陷識別方法 |
US16/325,281 US11293115B2 (en) | 2016-08-31 | 2017-08-21 | Method for producing a SiC epitaxial wafer containing a total density of large pit defects and triangular defects of 0.01 defects/cm2 or more and 0.6 defects/cm2 or less |
DE112017004297.6T DE112017004297B4 (de) | 2016-08-31 | 2017-08-21 | Herstellungsverfahren für einen SiC-Epitaxiewafer |
PCT/JP2017/029740 WO2018043171A1 (ja) | 2016-08-31 | 2017-08-21 | SiCエピタキシャルウェハ及びその製造方法、並びに、欠陥識別方法 |
US17/683,176 US11961736B2 (en) | 2016-08-31 | 2022-02-28 | SiC epitaxial wafer, production method therefor, and defect identification method |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2016170194 | 2016-08-31 | ||
JP2016170194 | 2016-08-31 |
Publications (2)
Publication Number | Publication Date |
---|---|
JP2018041942A JP2018041942A (ja) | 2018-03-15 |
JP6459132B2 true JP6459132B2 (ja) | 2019-01-30 |
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JP2016186062A Active JP6459132B2 (ja) | 2016-08-31 | 2016-09-23 | SiCエピタキシャルウェハ及びその製造方法、並びに、欠陥識別方法 |
Country Status (4)
Country | Link |
---|---|
JP (1) | JP6459132B2 (de) |
CN (1) | CN109642342B (de) |
DE (1) | DE112017004297B4 (de) |
TW (1) | TWI630292B (de) |
Families Citing this family (12)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP6493690B2 (ja) * | 2016-08-31 | 2019-04-03 | 昭和電工株式会社 | SiCエピタキシャルウェハ及びその製造方法、並びに、ラージピット欠陥検出方法、欠陥識別方法 |
US11293115B2 (en) | 2016-08-31 | 2022-04-05 | Showa Denko K.K. | Method for producing a SiC epitaxial wafer containing a total density of large pit defects and triangular defects of 0.01 defects/cm2 or more and 0.6 defects/cm2 or less |
US11320388B2 (en) | 2016-08-31 | 2022-05-03 | Showa Denko K.K. | SiC epitaxial wafer containing large pit defects with a surface density of 0.5 defects/CM2 or less, and production method therefor |
JP7204436B2 (ja) * | 2018-11-16 | 2023-01-16 | 昭和電工株式会社 | 欠陥除去方法及びSiCエピタキシャルウェハの製造方法 |
JP7063259B2 (ja) * | 2018-12-27 | 2022-05-09 | 株式会社Sumco | シリコンエピタキシャルウェーハの製造方法 |
JP7148427B2 (ja) * | 2019-02-06 | 2022-10-05 | 昭和電工株式会社 | SiCエピタキシャルウェハ及びその製造方法 |
JP7179219B1 (ja) | 2019-02-06 | 2022-11-28 | 昭和電工株式会社 | SiCデバイス及びその製造方法 |
JP7363110B2 (ja) * | 2019-06-10 | 2023-10-18 | 株式会社レゾナック | SiCエピタキシャルウェハ、SiC基板及びSiCエピタキシャルウェハの評価方法、及びSiCデバイスの製造方法 |
JP7363423B2 (ja) * | 2019-12-02 | 2023-10-18 | 株式会社デンソー | 炭化珪素単結晶の製造方法 |
CN113295616A (zh) * | 2021-03-30 | 2021-08-24 | 浙江大学杭州国际科创中心 | 一种SiC晶圆及其外延层结构的综合测试方法 |
WO2023282001A1 (ja) * | 2021-07-08 | 2023-01-12 | 住友電気工業株式会社 | 炭化珪素エピタキシャル基板、炭化珪素エピタキシャル基板の製造方法および炭化珪素半導体装置の製造方法 |
CN114717639B (zh) * | 2022-06-07 | 2022-09-16 | 浙江大学杭州国际科创中心 | 基于光电化学腐蚀工艺定位氧化镓晶片表面缺陷的方法 |
Family Cites Families (12)
Publication number | Priority date | Publication date | Assignee | Title |
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EP2264223A3 (de) * | 2006-09-14 | 2011-10-26 | Cree, Inc. | Mikroröhrchen-freies Siliciumcarbid und Verfahren zu seiner Herstellung |
JP4887418B2 (ja) * | 2009-12-14 | 2012-02-29 | 昭和電工株式会社 | SiCエピタキシャルウェハの製造方法 |
JP5897834B2 (ja) * | 2011-07-19 | 2016-03-30 | 昭和電工株式会社 | SiCエピタキシャルウェハの製造方法 |
JP6226959B2 (ja) * | 2012-04-20 | 2017-11-08 | トゥー‐シックス・インコーポレイテッド | 大口径高品質SiC単結晶、方法、及び装置 |
JP6037671B2 (ja) * | 2012-06-19 | 2016-12-07 | 昭和電工株式会社 | SiCエピタキシャルウェハ及びその製造方法 |
JP2014024703A (ja) * | 2012-07-26 | 2014-02-06 | Sumitomo Electric Ind Ltd | 炭化珪素単結晶の製造方法 |
JP6078330B2 (ja) * | 2012-12-21 | 2017-02-08 | 昭和電工株式会社 | 炭化珪素単結晶製造用坩堝、炭化珪素単結晶製造装置及び炭化珪素単結晶の製造方法 |
KR101989255B1 (ko) * | 2013-06-04 | 2019-06-13 | 쇼와 덴코 가부시키가이샤 | 에피택셜 탄화규소 웨이퍼용 탄화규소 단결정 기판의 제조 방법 |
JP6347188B2 (ja) | 2014-09-08 | 2018-06-27 | 富士電機株式会社 | 炭化珪素半導体装置の製造方法および炭化珪素半導体装置 |
JP2016170194A (ja) | 2015-03-11 | 2016-09-23 | セイコーエプソン株式会社 | 吸音体、吸音構造 |
JP5861794B1 (ja) | 2015-03-27 | 2016-02-16 | 東洋インキScホールディングス株式会社 | 再剥離型粘着剤 |
JP6493690B2 (ja) * | 2016-08-31 | 2019-04-03 | 昭和電工株式会社 | SiCエピタキシャルウェハ及びその製造方法、並びに、ラージピット欠陥検出方法、欠陥識別方法 |
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2016
- 2016-09-23 JP JP2016186062A patent/JP6459132B2/ja active Active
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2017
- 2017-08-21 CN CN201780051959.XA patent/CN109642342B/zh active Active
- 2017-08-21 DE DE112017004297.6T patent/DE112017004297B4/de active Active
- 2017-08-21 TW TW106128221A patent/TWI630292B/zh active
Also Published As
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TWI630292B (zh) | 2018-07-21 |
CN109642342A (zh) | 2019-04-16 |
JP2018041942A (ja) | 2018-03-15 |
DE112017004297B4 (de) | 2024-04-25 |
TW201812124A (zh) | 2018-04-01 |
CN109642342B (zh) | 2021-10-26 |
DE112017004297T5 (de) | 2019-05-23 |
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