JP6076742B2 - 高繰返周波数の超高速パルスレーザ溶発による、有機化合物のナノ粒子の液中生成方法 - Google Patents

高繰返周波数の超高速パルスレーザ溶発による、有機化合物のナノ粒子の液中生成方法 Download PDF

Info

Publication number
JP6076742B2
JP6076742B2 JP2012552906A JP2012552906A JP6076742B2 JP 6076742 B2 JP6076742 B2 JP 6076742B2 JP 2012552906 A JP2012552906 A JP 2012552906A JP 2012552906 A JP2012552906 A JP 2012552906A JP 6076742 B2 JP6076742 B2 JP 6076742B2
Authority
JP
Japan
Prior art keywords
target
liquid
laser beam
nanoparticles
pulse
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
JP2012552906A
Other languages
English (en)
Japanese (ja)
Other versions
JP2013519671A (ja
JP2013519671A5 (https=
Inventor
ジェンドン ホゥ、
ジェンドン ホゥ、
ヨン チェ、
ヨン チェ、
Original Assignee
イムラ アメリカ インコーポレイテッド
イムラ アメリカ インコーポレイテッド
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by イムラ アメリカ インコーポレイテッド, イムラ アメリカ インコーポレイテッド filed Critical イムラ アメリカ インコーポレイテッド
Publication of JP2013519671A publication Critical patent/JP2013519671A/ja
Publication of JP2013519671A5 publication Critical patent/JP2013519671A5/ja
Application granted granted Critical
Publication of JP6076742B2 publication Critical patent/JP6076742B2/ja
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Classifications

    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K9/00—Medicinal preparations characterised by special physical form
    • A61K9/10—Dispersions; Emulsions
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J13/00—Colloid chemistry, e.g. the production of colloidal materials or their solutions, not otherwise provided for; Making microcapsules or microballoons
    • B01J13/0086—Preparation of sols by physical processes
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K31/00—Medicinal preparations containing organic active ingredients
    • A61K31/12—Ketones
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K9/00—Medicinal preparations characterised by special physical form
    • A61K9/14—Particulate form, e.g. powders, Processes for size reducing of pure drugs or the resulting products, Pure drug nanoparticles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B23—MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
    • B23K—SOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
    • B23K26/00—Working by laser beam, e.g. welding, cutting or boring
    • B23K26/02—Positioning or observing the workpiece, e.g. with respect to the point of impact; Aligning, aiming or focusing the laser beam
    • B23K26/06—Shaping the laser beam, e.g. by masks or multi-focusing
    • B23K26/062—Shaping the laser beam, e.g. by masks or multi-focusing by direct control of the laser beam
    • B23K26/0622—Shaping the laser beam, e.g. by masks or multi-focusing by direct control of the laser beam by shaping pulses
    • B23K26/0624—Shaping the laser beam, e.g. by masks or multi-focusing by direct control of the laser beam by shaping pulses using ultrashort pulses, i.e. pulses of 1 ns or less
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B23—MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
    • B23K—SOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
    • B23K26/00—Working by laser beam, e.g. welding, cutting or boring
    • B23K26/14—Working by laser beam, e.g. welding, cutting or boring using a fluid stream, e.g. a jet of gas, in conjunction with the laser beam; Nozzles therefor
    • B23K26/144—Working by laser beam, e.g. welding, cutting or boring using a fluid stream, e.g. a jet of gas, in conjunction with the laser beam; Nozzles therefor the fluid stream containing particles, e.g. powder
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B23—MACHINE TOOLS; METAL-WORKING NOT OTHERWISE PROVIDED FOR
    • B23K—SOLDERING OR UNSOLDERING; WELDING; CLADDING OR PLATING BY SOLDERING OR WELDING; CUTTING BY APPLYING HEAT LOCALLY, e.g. FLAME CUTTING; WORKING BY LASER BEAM
    • B23K26/00—Working by laser beam, e.g. welding, cutting or boring
    • B23K26/14—Working by laser beam, e.g. welding, cutting or boring using a fluid stream, e.g. a jet of gas, in conjunction with the laser beam; Nozzles therefor
    • B23K26/146—Working by laser beam, e.g. welding, cutting or boring using a fluid stream, e.g. a jet of gas, in conjunction with the laser beam; Nozzles therefor the fluid stream containing a liquid
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y40/00—Manufacture or treatment of nanostructures
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S977/00—Nanotechnology
    • Y10S977/84—Manufacture, treatment, or detection of nanostructure
    • Y10S977/888—Shaping or removal of materials, e.g. etching
    • Y10S977/889—Shaping or removal of materials, e.g. etching by laser ablation
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S977/00—Nanotechnology
    • Y10S977/84—Manufacture, treatment, or detection of nanostructure
    • Y10S977/901—Manufacture, treatment, or detection of nanostructure having step or means utilizing electromagnetic property, e.g. optical, x-ray, electron beamm

Landscapes

  • Engineering & Computer Science (AREA)
  • Physics & Mathematics (AREA)
  • Chemical & Material Sciences (AREA)
  • Optics & Photonics (AREA)
  • Health & Medical Sciences (AREA)
  • Mechanical Engineering (AREA)
  • Plasma & Fusion (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Public Health (AREA)
  • Animal Behavior & Ethology (AREA)
  • Epidemiology (AREA)
  • Pharmacology & Pharmacy (AREA)
  • Medicinal Chemistry (AREA)
  • Organic Chemistry (AREA)
  • Nanotechnology (AREA)
  • Dispersion Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • General Physics & Mathematics (AREA)
  • Manufacturing & Machinery (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)
  • Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
JP2012552906A 2010-02-10 2011-02-03 高繰返周波数の超高速パルスレーザ溶発による、有機化合物のナノ粒子の液中生成方法 Expired - Fee Related JP6076742B2 (ja)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
US30298410P 2010-02-10 2010-02-10
US61/302,984 2010-02-10
US12/951,496 US8992815B2 (en) 2010-02-10 2010-11-22 Production of organic compound nanoparticles with high repetition rate ultrafast pulsed laser ablation in liquids
US12/951,496 2010-11-22
PCT/US2011/023530 WO2011100154A1 (en) 2010-02-10 2011-02-03 Production of organic compound nanoparticles with high repetition rate ultrafast pulsed laser ablation in liquids

Publications (3)

Publication Number Publication Date
JP2013519671A JP2013519671A (ja) 2013-05-30
JP2013519671A5 JP2013519671A5 (https=) 2015-08-20
JP6076742B2 true JP6076742B2 (ja) 2017-02-08

Family

ID=44354201

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2012552906A Expired - Fee Related JP6076742B2 (ja) 2010-02-10 2011-02-03 高繰返周波数の超高速パルスレーザ溶発による、有機化合物のナノ粒子の液中生成方法

Country Status (5)

Country Link
US (2) US8992815B2 (https=)
JP (1) JP6076742B2 (https=)
CN (1) CN102802934A (https=)
DE (1) DE112011100502T5 (https=)
WO (1) WO2011100154A1 (https=)

Families Citing this family (27)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20110192450A1 (en) * 2010-02-10 2011-08-11 Bing Liu Method for producing nanoparticle solutions based on pulsed laser ablation for fabrication of thin film solar cells
US8540173B2 (en) * 2010-02-10 2013-09-24 Imra America, Inc. Production of fine particles of functional ceramic by using pulsed laser
US8685293B1 (en) * 2010-03-19 2014-04-01 Nicholas V. Coppa Control of particle formation at the nanoscale
US8802234B2 (en) * 2011-01-03 2014-08-12 Imra America, Inc. Composite nanoparticles and methods for making the same
JP5671724B2 (ja) * 2011-02-21 2015-02-18 株式会社奈良機械製作所 液相レーザーアブレーション方法及び装置
US9849512B2 (en) 2011-07-01 2017-12-26 Attostat, Inc. Method and apparatus for production of uniformly sized nanoparticles
US9463243B2 (en) 2012-02-13 2016-10-11 Imra America, Inc. Amorphous medicinal fine particles produced by pulsed laser ablation in liquid and the production method thereof
CN102701270B (zh) * 2012-06-12 2014-05-14 天津大学 胶体硫化锡空心纳米颗粒的制备方法
US9646729B2 (en) * 2013-01-18 2017-05-09 Westinghouse Electric Company Llc Laser sintering systems and methods for remote manufacture of high density pellets containing highly radioactive elements
WO2015077867A1 (en) * 2013-11-26 2015-06-04 National Research Council Of Canada Method and apparatus for fast quantitative analysis of a material by laser induced breakdown spectroscopy (libs)
US20160236296A1 (en) * 2015-02-13 2016-08-18 Gold Nanotech Inc Nanoparticle Manufacturing System
WO2016161348A1 (en) 2015-04-01 2016-10-06 Attostat, Inc. Nanoparticle compositions and methods for treating or preventing tissue infections and diseases
WO2016168346A1 (en) 2015-04-13 2016-10-20 Attostat, Inc. Anti-corrosion nanoparticle compositions
US11473202B2 (en) 2015-04-13 2022-10-18 Attostat, Inc. Anti-corrosion nanoparticle compositions
DE102015211280B4 (de) * 2015-06-18 2018-01-04 Fraunhofer-Gesellschaft zur Förderung der angewandten Forschung e.V. Dispergierung von agglomerierten Nanopartikeln
US10201571B2 (en) 2016-01-25 2019-02-12 Attostat, Inc. Nanoparticle compositions and methods for treating onychomychosis
TWI593134B (zh) * 2016-05-19 2017-07-21 Method and structure for manufacturing graphene quantum dot on light-emitting diode
CN106496605B (zh) * 2016-12-23 2019-10-11 广东工业大学 一种制备高分子磁性微球的装置与方法
US11018376B2 (en) 2017-11-28 2021-05-25 Attostat, Inc. Nanoparticle compositions and methods for enhancing lead-acid batteries
US11646453B2 (en) 2017-11-28 2023-05-09 Attostat, Inc. Nanoparticle compositions and methods for enhancing lead-acid batteries
CN108875264B (zh) * 2018-07-06 2021-06-15 厦门大学 一种用于飞秒激光烧蚀仿真的激光源模型的建立方法
DE102018216824A1 (de) * 2018-10-01 2020-04-02 Universität Duisburg-Essen Kompakte Vorrichtung und Verfahren zur Herstellung von Nanopartikeln in Suspension
WO2020165220A1 (de) * 2019-02-12 2020-08-20 Trumpf Laser- Und Systemtechnik Gmbh Verfahren und vorrichtung zum bearbeiten von partikeln sowie nanopartikel eines pharmazeutischen wirkstoffs
CN109868462A (zh) * 2019-03-28 2019-06-11 北京理工大学 一种实现在纳米尺度下激光辅助金离子化学还原的方法
US12115250B2 (en) 2019-07-12 2024-10-15 Evoq Nano, Inc. Use of nanoparticles for treating respiratory infections associated with cystic fibrosis
ES3057406T3 (en) * 2020-10-01 2026-03-02 Univ South Africa Method of producing a nanofluid using laser ablation, and laser ablation system for manufacturing nanofluids
US12456759B2 (en) 2021-03-30 2025-10-28 Evoq Nano, Inc. Nanoparticle-enhanced lead-acid electrode paste and improved lead-acid batteries made therefrom

Family Cites Families (29)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5390864A (en) * 1990-03-13 1995-02-21 The Board Of Regents Of The University Of Nebraska Apparatus for forming fine particles
US5585020A (en) * 1994-11-03 1996-12-17 Becker; Michael F. Process for the production of nanoparticles
US6653226B1 (en) * 2001-01-09 2003-11-25 Novellus Systems, Inc. Method for electrochemical planarization of metal surfaces
FR2802308B1 (fr) * 1999-12-09 2002-03-08 Gc Comm Procede et dispositif d'usinage par laser de guides de lumiere, guides de lumiere obtenus et ecrans retro-elaires incorporant ces guides
JP4763957B2 (ja) * 2000-05-10 2011-08-31 オバン・エナジー・リミテッド メディアミリング
US6741345B2 (en) * 2001-02-08 2004-05-25 National Research Council Of Canada Method and apparatus for in-process liquid analysis by laser induced plasma spectroscopy
JP2003306319A (ja) * 2002-04-10 2003-10-28 Japan Atom Energy Res Inst 金属酸化物ナノ微粒子の製造方法
JP4116404B2 (ja) 2002-11-18 2008-07-09 浜松ホトニクス株式会社 ナノ粒子化処理に用いるレーザ光照射条件の決定方法及び決定装置並びにナノ粒子の製造方法
JP4344153B2 (ja) 2003-03-07 2009-10-14 浜松ホトニクス株式会社 微粒子の製造方法及び製造装置、並びに注射剤の製造方法
JP4398182B2 (ja) 2003-06-16 2010-01-13 浜松ホトニクス株式会社 微粒子の製造方法、並びに注射剤の製造方法
JP4643155B2 (ja) 2004-02-24 2011-03-02 株式会社ＡＢｓｉｚｅ 薬効成分の超微粒子の製造方法
US7529011B2 (en) * 2004-04-12 2009-05-05 Ricoh Company, Ltd. Deflector mirror with regions of different flexural rigidity
US7133188B2 (en) * 2004-06-07 2006-11-07 Electro Scientific Industries, Inc. AOM modulation techniques employing an upstream Bragg adjustment device
US7527824B2 (en) * 2004-06-25 2009-05-05 Becker Michael F Methods for producing coated nanoparticles from microparticles
US8512436B2 (en) * 2004-09-15 2013-08-20 Kyoto University Metal fine particles and manufacturing method therefor
JP2006152032A (ja) * 2004-11-25 2006-06-15 Matsushita Electric Works Ltd 蛍光体ナノ粒子の製造方法
CN100467118C (zh) * 2005-08-08 2009-03-11 鸿富锦精密工业（深圳）有限公司 纳米粒子制备装置
US7718432B2 (en) * 2006-03-22 2010-05-18 The University Of Southern Mississippi Non-immunogenic, hydrophilic/cationic block copolymers and uses thereof
JP2007301534A (ja) 2006-05-15 2007-11-22 Ebara Corp 微細化装置
JP2007306950A (ja) * 2006-05-15 2007-11-29 Osaka Univ 薬効成分ナノ粒子分散液の製造方法
US20080006524A1 (en) * 2006-07-05 2008-01-10 Imra America, Inc. Method for producing and depositing nanoparticles
GB0712287D0 (en) * 2007-06-22 2007-08-01 Ucl Business Plc Antimicrobial Conjugates
US7729031B2 (en) * 2006-09-07 2010-06-01 Ricoh Company, Ltd. Light-source device, optical scanning device, and image forming apparatus
WO2008073558A2 (en) * 2006-10-05 2008-06-19 The Johns Hopkins University Water-dispersible oral, parenteral, and topical formulations for poorly water soluble drugs using smart polymeric nanoparticles
EP2252426A4 (en) * 2008-03-21 2014-08-06 Imra America Inc METHOD AND SYSTEMS FOR PROCESSING A LASER BASED MATERIAL
US20090246530A1 (en) * 2008-03-27 2009-10-01 Imra America, Inc. Method For Fabricating Thin Films
JP5589168B2 (ja) * 2008-06-11 2014-09-17 独立行政法人産業技術総合研究所 金ナノ粒子およびその分散液、金ナノ粒子の製造方法、ナノ粒子製造システム
US20110190399A1 (en) * 2008-07-31 2011-08-04 Santosh Kumar Kar Curcumin nanoparticles and methods of producing the same
US8246714B2 (en) * 2009-01-30 2012-08-21 Imra America, Inc. Production of metal and metal-alloy nanoparticles with high repetition rate ultrafast pulsed laser ablation in liquids

Also Published As

Publication number Publication date
US20110196044A1 (en) 2011-08-11
JP2013519671A (ja) 2013-05-30
DE112011100502T5 (de) 2013-03-28
US20150258631A1 (en) 2015-09-17
CN102802934A (zh) 2012-11-28
WO2011100154A1 (en) 2011-08-18
US8992815B2 (en) 2015-03-31

Similar Documents

Publication Publication Date Title
JP6076742B2 (ja) 高繰返周波数の超高速パルスレーザ溶発による、有機化合物のナノ粒子の液中生成方法
JP5589168B2 (ja) 金ナノ粒子およびその分散液、金ナノ粒子の製造方法、ナノ粒子製造システム
Wagener et al. Pulsed laser ablation of zinc in tetrahydrofuran: bypassing the cavitation bubble
US8246714B2 (en) Production of metal and metal-alloy nanoparticles with high repetition rate ultrafast pulsed laser ablation in liquids
JP2013519671A5 (https=)
JP4643155B2 (ja) 薬効成分の超微粒子の製造方法
JP2014129608A5 (https=)
Lasemi et al. The influence of the fluid nature on femtosecond laser ablation properties of a SiO 2/Si target and synthesis of ultrafine-grained Si nanoparticles
Serkov et al. Laser-induced agglomeration of gold and silver nanoparticles dispersed in liquid
Altakroury et al. Size control of nanoparticles synthesized by pulsed laser ablation in liquids using donut-shaped beams
Watanabe et al. Fabrication of FeCoNi medium-entropy alloy nanoparticles by high-repetition-rate UV picosecond laser ablation in water
Al-Azawi et al. The effects of the ambient liquid medium on the ablation efficiency, size and stability of silver nanoparticles prepared by pulse laser ablation in liquid technique
CN103341635B (zh) 一种通过激光生成水合电子来制备纳米金颗粒的方法
JP6912553B2 (ja) レーザアブレーションによる金属ナノコロイド生成方法
Ali Preparation of gold nanoparticles by pulsed laser ablation in NaOH solution
CN114632481A (zh) 一种制备均分散金属纳米颗粒胶体的方法
JP2018040033A (ja) レーザアブレーションによる金属ナノコロイド生成方法
Ghalot et al. Obtaining Nanoparticles by Underwater Laser Ablation–A Brief Review
Nancy et al. Ultrafast Laser Ablation–A Peerless Synthesis Strategy for Functional Nanomaterials
Al-Nassar et al. Study the effect of liquid layer level on the formation of zinc oxide nanoparticles synthesized by liquid-phase pulsed laser ablation
Lin et al. Synthesis and characterization of FeCo nanoparticle colloid by pulsed laser ablation in distilled water
Bertocco Optimization of polyynes production by Pulsed Laser Ablation in Liquid through a recirculation system
WO2023082023A1 (en) Tunable nanostructure formation methods and techniques exploiting ablation
de Oliveira et al. Green synthesis of sub-10 nm gold nanoparticles by two-step laser irradiation
JP2009119340A (ja) 液中レーザーアブレーションシステム

Legal Events

Date Code Title Description
A621 Written request for application examination

Free format text: JAPANESE INTERMEDIATE CODE: A621

Effective date: 20131204

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20141015

A601 Written request for extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A601

Effective date: 20150106

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20150316

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20150407

A524 Written submission of copy of amendment under article 19 pct

Free format text: JAPANESE INTERMEDIATE CODE: A524

Effective date: 20150702

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20160126

A601 Written request for extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A601

Effective date: 20160425

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20160519

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20161101

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20161116

TRDD Decision of grant or rejection written
A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

Effective date: 20161213

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20170111

R150 Certificate of patent or registration of utility model

Ref document number: 6076742

Country of ref document: JP

Free format text: JAPANESE INTERMEDIATE CODE: R150

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

LAPS Cancellation because of no payment of annual fees