JP6001768B2 - NU型及びPI型のバナジウム補償型SISiC単結晶及びその結晶成長方法 - Google Patents
NU型及びPI型のバナジウム補償型SISiC単結晶及びその結晶成長方法 Download PDFInfo
- Publication number
- JP6001768B2 JP6001768B2 JP2015514213A JP2015514213A JP6001768B2 JP 6001768 B2 JP6001768 B2 JP 6001768B2 JP 2015514213 A JP2015514213 A JP 2015514213A JP 2015514213 A JP2015514213 A JP 2015514213A JP 6001768 B2 JP6001768 B2 JP 6001768B2
- Authority
- JP
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- Prior art keywords
- growth
- sic
- single crystal
- crystal
- vanadium
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 0 *C1CCCCC1 Chemical compound *C1CCCCC1 0.000 description 1
- AWYMFBJJKFTCFO-UHFFFAOYSA-N C(C1)C2C1CCC2 Chemical compound C(C1)C2C1CCC2 AWYMFBJJKFTCFO-UHFFFAOYSA-N 0.000 description 1
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B23/00—Single-crystal growth by condensing evaporated or sublimed materials
- C30B23/002—Controlling or regulating
-
- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B29/00—Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape
- C30B29/10—Inorganic compounds or compositions
- C30B29/36—Carbides
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01B—CABLES; CONDUCTORS; INSULATORS; SELECTION OF MATERIALS FOR THEIR CONDUCTIVE, INSULATING OR DIELECTRIC PROPERTIES
- H01B3/00—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties
- H01B3/02—Insulators or insulating bodies characterised by the insulating materials; Selection of materials for their insulating or dielectric properties mainly consisting of inorganic substances
- H01B3/025—Other inorganic material
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Crystallography & Structural Chemistry (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Crystals, And After-Treatments Of Crystals (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201261651143P | 2012-05-24 | 2012-05-24 | |
| US61/651,143 | 2012-05-24 | ||
| PCT/US2013/042604 WO2013177496A1 (en) | 2012-05-24 | 2013-05-24 | Vanadium compensated, si sic single crystals of nu and pi type and the crystal growth process thereof |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2015517451A JP2015517451A (ja) | 2015-06-22 |
| JP2015517451A5 JP2015517451A5 (https=) | 2016-09-01 |
| JP6001768B2 true JP6001768B2 (ja) | 2016-10-05 |
Family
ID=49624371
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2015514213A Expired - Fee Related JP6001768B2 (ja) | 2012-05-24 | 2013-05-24 | NU型及びPI型のバナジウム補償型SISiC単結晶及びその結晶成長方法 |
Country Status (6)
| Country | Link |
|---|---|
| US (2) | US9090989B2 (https=) |
| EP (1) | EP2855741B1 (https=) |
| JP (1) | JP6001768B2 (https=) |
| KR (1) | KR101661053B1 (https=) |
| CN (1) | CN104364428B (https=) |
| WO (1) | WO2013177496A1 (https=) |
Families Citing this family (24)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US9090989B2 (en) | 2012-05-24 | 2015-07-28 | Ii-Vi Incorporated | Vanadium compensated, SI SiC single crystals of NU and PI type and the crystal growth process thereof |
| CN105734672B (zh) * | 2014-12-10 | 2018-11-30 | 北京天科合达半导体股份有限公司 | 一种在含氧气氛下生长高质量碳化硅晶体的方法 |
| US20170321345A1 (en) | 2016-05-06 | 2017-11-09 | Ii-Vi Incorporated | Large Diameter Silicon Carbide Single Crystals and Apparatus and Method of Manufacture Thereof |
| CN109666971B (zh) * | 2017-10-16 | 2020-11-10 | 北京北方华创微电子装备有限公司 | 生长炉 |
| CN107955969A (zh) * | 2017-12-28 | 2018-04-24 | 河北同光晶体有限公司 | 一种持续供料的SiC单晶生长系统 |
| CN108118394B (zh) * | 2017-12-28 | 2020-07-17 | 河北同光晶体有限公司 | 一种降低碳化硅单晶中氮杂质含量的方法 |
| JP7268299B2 (ja) * | 2018-08-08 | 2023-05-08 | 株式会社レゾナック | 遮蔽部材及び単結晶成長装置 |
| CN110055588A (zh) * | 2019-06-05 | 2019-07-26 | 华北电力大学 | 一种碳化硅单晶生长用固气界面可控的坩埚 |
| JP6806270B1 (ja) * | 2019-06-20 | 2021-01-06 | 三菱電機株式会社 | 炭化ケイ素単結晶、半導体素子 |
| CN110408998B (zh) * | 2019-07-29 | 2020-12-22 | 江苏星特亮科技有限公司 | 一种碳化硅单晶连续生长装置及其生长方法 |
| CN110565167A (zh) * | 2019-08-19 | 2019-12-13 | 河北同光晶体有限公司 | 一种用于PVT法生长SiC单晶的装料装置及装料方法 |
| WO2021085587A1 (ja) * | 2019-10-31 | 2021-05-06 | 京セラ株式会社 | 配線基板、電子装置及び電子モジュール |
| US12006591B2 (en) * | 2020-03-02 | 2024-06-11 | Ii-Vi Advanced Materials, Llc | Method for preparing an aluminum doped silicon carbide crystal by providing a compound including aluminum and oxygen in a capsule comprised of a first and second material |
| CN111534854B (zh) * | 2020-06-12 | 2021-07-13 | 北京北方华创微电子装备有限公司 | 晶体生长炉 |
| TWI865578B (zh) | 2020-06-18 | 2024-12-11 | 盛新材料科技股份有限公司 | 半絕緣單晶碳化矽塊材以及粉末 |
| JP2021195301A (ja) | 2020-06-18 | 2021-12-27 | 盛新材料科技股▲ふん▼有限公司Taisic Materials Corp. | 半絶縁性単結晶炭化ケイ素粉末の製造方法 |
| US12297561B2 (en) | 2020-06-18 | 2025-05-13 | Taisic Materials Corp. | Semi-insulating single-crystal silicon carbide bulk material and powder |
| CN113981536B (zh) | 2020-07-27 | 2024-07-09 | 环球晶圆股份有限公司 | 碳化硅晶碇及其制备方法 |
| CN111793821A (zh) * | 2020-08-21 | 2020-10-20 | 哈尔滨科友半导体产业装备与技术研究院有限公司 | 一种精确控制pvt法晶体生长气体压力的系统及方法 |
| CN112853491A (zh) * | 2020-12-31 | 2021-05-28 | 山西烁科晶体有限公司 | 一种掺杂碳化硅单晶及其制备方法 |
| CN113249792B (zh) * | 2021-06-22 | 2021-09-28 | 苏州优晶光电科技有限公司 | 一种调节组分平衡的碳化硅晶体生长方法及设备 |
| CN114000198B (zh) | 2021-11-15 | 2023-03-10 | 苏州优晶光电科技有限公司 | 一种多坩埚碳化硅晶体同步生长方法及设备 |
| JP7534809B2 (ja) | 2021-11-15 | 2024-08-15 | スーチョウ ユーキング セミコンダクター テクノロジー カンパニー リミテッド | 複数の坩堝における炭化ケイ素結晶の同期成長方法及び装置 |
| WO2023157514A1 (ja) * | 2022-02-17 | 2023-08-24 | 住友電気工業株式会社 | 炭化珪素基板、炭化珪素基板の製造方法および炭化珪素基板の製造装置 |
Family Cites Families (21)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE4325804C3 (de) | 1993-07-31 | 2001-08-09 | Daimler Chrysler Ag | Verfahren zum Herstellen von hochohmigem Siliziumkarbid |
| US5611955A (en) | 1993-10-18 | 1997-03-18 | Northrop Grumman Corp. | High resistivity silicon carbide substrates for high power microwave devices |
| US6562130B2 (en) * | 1997-01-22 | 2003-05-13 | The Fox Group, Inc. | Low defect axially grown single crystal silicon carbide |
| US6410433B1 (en) | 1999-04-27 | 2002-06-25 | Tokyo Electron Limited | Thermal CVD of TaN films from tantalum halide precursors |
| US6218680B1 (en) * | 1999-05-18 | 2001-04-17 | Cree, Inc. | Semi-insulating silicon carbide without vanadium domination |
| US6396080B2 (en) * | 1999-05-18 | 2002-05-28 | Cree, Inc | Semi-insulating silicon carbide without vanadium domination |
| US6507046B2 (en) | 2001-05-11 | 2003-01-14 | Cree, Inc. | High-resistivity silicon carbide substrate for semiconductor devices with high break down voltage |
| SE520968C2 (sv) | 2001-10-29 | 2003-09-16 | Okmetic Oyj | Högresistiv monokristallin kiselkarbid och metod för dess framställning |
| US7063741B2 (en) * | 2002-03-27 | 2006-06-20 | General Electric Company | High pressure high temperature growth of crystalline group III metal nitrides |
| WO2006017074A2 (en) * | 2004-07-07 | 2006-02-16 | Ii-Vi Incorporated | Low-doped semi-insulating sic crystals and method |
| US7276117B2 (en) * | 2005-02-09 | 2007-10-02 | Cree Dulles, Inc. | Method of forming semi-insulating silicon carbide single crystal |
| US7608524B2 (en) | 2005-04-19 | 2009-10-27 | Ii-Vi Incorporated | Method of and system for forming SiC crystals having spatially uniform doping impurities |
| US8858709B1 (en) * | 2006-04-11 | 2014-10-14 | Ii-Vi Incorporated | Silicon carbide with low nitrogen content and method for preparation |
| US8361227B2 (en) * | 2006-09-26 | 2013-01-29 | Ii-Vi Incorporated | Silicon carbide single crystals with low boron content |
| WO2008039914A2 (en) * | 2006-09-27 | 2008-04-03 | Ii-Vi Incorporated | Sic single crystals with reduced dislocation density grown by step-wise periodic perturbation technique |
| DE102008063129B4 (de) * | 2008-12-24 | 2013-05-16 | Sicrystal Ag | Herstellungsverfahren für einen codotierten SiC-Volumeneinkristall und hochohmiges SiC-Substrat |
| JP5779171B2 (ja) * | 2009-03-26 | 2015-09-16 | トゥー‐シックス・インコーポレイテッド | SiC単結晶の昇華成長方法及び装置 |
| EP2477944A4 (en) * | 2009-09-15 | 2013-08-28 | Ii Vi Inc | SUBLIMATION BREEDING OF SIC INDIVIDUAL CRYSTALS |
| WO2012029952A1 (ja) * | 2010-09-02 | 2012-03-08 | 株式会社ブリヂストン | 炭化ケイ素単結晶の製造方法、炭化ケイ素単結晶、及び炭化ケイ素単結晶基板 |
| CN102560671B (zh) * | 2010-12-31 | 2015-05-27 | 中国科学院物理研究所 | 半绝缘碳化硅单晶 |
| US9090989B2 (en) | 2012-05-24 | 2015-07-28 | Ii-Vi Incorporated | Vanadium compensated, SI SiC single crystals of NU and PI type and the crystal growth process thereof |
-
2013
- 2013-05-24 US US13/902,016 patent/US9090989B2/en not_active Ceased
- 2013-05-24 KR KR1020147033938A patent/KR101661053B1/ko not_active Expired - Fee Related
- 2013-05-24 CN CN201380027241.9A patent/CN104364428B/zh active Active
- 2013-05-24 JP JP2015514213A patent/JP6001768B2/ja not_active Expired - Fee Related
- 2013-05-24 EP EP13794286.8A patent/EP2855741B1/en active Active
- 2013-05-24 WO PCT/US2013/042604 patent/WO2013177496A1/en not_active Ceased
-
2017
- 2017-05-01 US US15/583,538 patent/USRE48378E1/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| EP2855741B1 (en) | 2022-04-27 |
| US20130320275A1 (en) | 2013-12-05 |
| US9090989B2 (en) | 2015-07-28 |
| KR20150013233A (ko) | 2015-02-04 |
| JP2015517451A (ja) | 2015-06-22 |
| WO2013177496A1 (en) | 2013-11-28 |
| CN104364428A (zh) | 2015-02-18 |
| EP2855741A1 (en) | 2015-04-08 |
| EP2855741A4 (en) | 2016-01-06 |
| KR101661053B1 (ko) | 2016-09-28 |
| CN104364428B (zh) | 2017-09-05 |
| USRE48378E1 (en) | 2021-01-05 |
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