JP5925182B2 - 撮像のための試料調製方法 - Google Patents

撮像のための試料調製方法 Download PDF

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Publication number
JP5925182B2
JP5925182B2 JP2013268368A JP2013268368A JP5925182B2 JP 5925182 B2 JP5925182 B2 JP 5925182B2 JP 2013268368 A JP2013268368 A JP 2013268368A JP 2013268368 A JP2013268368 A JP 2013268368A JP 5925182 B2 JP5925182 B2 JP 5925182B2
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sample
workpiece
ion beam
guiding
deposited
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JP2014130145A (ja
JP2014130145A5 (enExample
Inventor
シュミット マイケル
シュミット マイケル
ブラックウッド ジェフ
ブラックウッド ジェフ
ストーン ステイシー
ストーン ステイシー
フーン リー サン
フーン リー サン
ケリー ロナルド
ケリー ロナルド
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FEI Co
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FEI Co
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Priority claimed from US14/081,947 external-priority patent/US8912490B2/en
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/28Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
    • G01N1/32Polishing; Etching
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/28Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
    • HELECTRICITY
    • H01ELECTRIC ELEMENTS
    • H01LSEMICONDUCTOR DEVICES NOT COVERED BY CLASS H10
    • H01L21/00Processes or apparatus adapted for the manufacture or treatment of semiconductor or solid state devices or of parts thereof
    • H01L21/02Manufacture or treatment of semiconductor devices or of parts thereof
    • H01L21/04Manufacture or treatment of semiconductor devices or of parts thereof the devices having potential barriers, e.g. a PN junction, depletion layer or carrier concentration layer
    • H01L21/18Manufacture or treatment of semiconductor devices or of parts thereof the devices having potential barriers, e.g. a PN junction, depletion layer or carrier concentration layer the devices having semiconductor bodies comprising elements of Group IV of the Periodic Table or AIIIBV compounds with or without impurities, e.g. doping materials
    • H01L21/30Treatment of semiconductor bodies using processes or apparatus not provided for in groups H01L21/20 - H01L21/26
    • H01L21/302Treatment of semiconductor bodies using processes or apparatus not provided for in groups H01L21/20 - H01L21/26 to change their surface-physical characteristics or shape, e.g. etching, polishing, cutting
    • H01L21/306Chemical or electrical treatment, e.g. electrolytic etching
    • H01L21/3065Plasma etching; Reactive-ion etching
    • H01L21/30655Plasma etching; Reactive-ion etching comprising alternated and repeated etching and passivation steps, e.g. Bosch process

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  • Physics & Mathematics (AREA)
  • General Physics & Mathematics (AREA)
  • Engineering & Computer Science (AREA)
  • Biochemistry (AREA)
  • Analytical Chemistry (AREA)
  • Chemical & Material Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Health & Medical Sciences (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • Plasma & Fusion (AREA)
  • Manufacturing & Machinery (AREA)
  • Computer Hardware Design (AREA)
  • Microelectronics & Electronic Packaging (AREA)
  • Power Engineering (AREA)
  • Sampling And Sample Adjustment (AREA)
  • Analysing Materials By The Use Of Radiation (AREA)
  • Testing Or Measuring Of Semiconductors Or The Like (AREA)
JP2013268368A 2012-12-31 2013-12-26 撮像のための試料調製方法 Active JP5925182B2 (ja)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
US201261747512P 2012-12-31 2012-12-31
US61/747,512 2012-12-31
US14/081,947 2013-11-15
US14/081,947 US8912490B2 (en) 2011-06-03 2013-11-15 Method for preparing samples for imaging

Publications (3)

Publication Number Publication Date
JP2014130145A JP2014130145A (ja) 2014-07-10
JP2014130145A5 JP2014130145A5 (enExample) 2016-04-14
JP5925182B2 true JP5925182B2 (ja) 2016-05-25

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Family Applications (2)

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JP2013268368A Active JP5925182B2 (ja) 2012-12-31 2013-12-26 撮像のための試料調製方法
JP2015550848A Pending JP2016509669A (ja) 2012-12-31 2013-12-30 画像化用の試料を作製する方法

Family Applications After (1)

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JP2015550848A Pending JP2016509669A (ja) 2012-12-31 2013-12-30 画像化用の試料を作製する方法

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US (1) US20150330877A1 (enExample)
EP (2) EP2749863A3 (enExample)
JP (2) JP5925182B2 (enExample)
CN (2) CN105103270A (enExample)
TW (1) TW201432242A (enExample)
WO (1) WO2014106200A2 (enExample)

Families Citing this family (33)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR102155834B1 (ko) 2012-10-05 2020-09-14 에프이아이 컴파니 높은 종횡비 구조 분석
JP6199979B2 (ja) * 2012-10-05 2017-09-20 エフ・イ−・アイ・カンパニー 傾斜ミリング保護のためのバルク付着
US20150369710A1 (en) * 2014-06-24 2015-12-24 Fei Company Method and System of Creating a Symmetrical FIB Deposition
CN105200394A (zh) * 2014-06-24 2015-12-30 Fei公司 创建对称fib沉积的方法和系统
KR102358551B1 (ko) * 2014-08-29 2022-02-04 가부시키가이샤 히다치 하이테크 사이언스 자동 시료편 제작 장치
CN104237567B (zh) * 2014-09-10 2016-05-11 武汉新芯集成电路制造有限公司 一种超薄平面透射电镜样品的制备方法
JP6584786B2 (ja) * 2015-02-13 2019-10-02 株式会社日立ハイテクノロジーズ プラズマイオン源および荷電粒子ビーム装置
CN105223383B (zh) * 2015-08-11 2018-08-28 上海华力微电子有限公司 一种平面tem样品的制备方法
CN105136539B (zh) * 2015-08-26 2019-05-03 上海华力微电子有限公司 一种制备tem芯片样品的方法
CN105300754B (zh) * 2015-09-11 2019-06-28 上海华力微电子有限公司 一种防止tem芯片样品破裂的方法
US9978586B2 (en) 2015-11-06 2018-05-22 Fei Company Method of material deposition
US10103008B2 (en) 2016-01-12 2018-10-16 Fei Company Charged particle beam-induced etching
EP3249676B1 (en) 2016-05-27 2018-10-03 FEI Company Dual-beam charged-particle microscope with in situ deposition functionality
US10324049B2 (en) 2017-02-15 2019-06-18 Saudi Arabian Oil Company Rock sample preparation method by using focused ion beam for minimizing curtain effect
JP7214262B2 (ja) * 2017-03-27 2023-01-30 株式会社日立ハイテクサイエンス 荷電粒子ビーム装置、試料加工方法
JP2020518117A (ja) * 2017-04-20 2020-06-18 エレメンタル・サイエンティフィック・レーザーズ・リミテッド・ライアビリティ・カンパニーElemental Scientific Lasers, Llc 超高速信号ウォッシュアウトのための調整可能なサンプルフロア
US10546719B2 (en) * 2017-06-02 2020-01-28 Fei Company Face-on, gas-assisted etching for plan-view lamellae preparation
DE102017212020B3 (de) * 2017-07-13 2018-05-30 Carl Zeiss Microscopy Gmbh Verfahren zur In-situ-Präparation und zum Transfer mikroskopischer Proben, Computerprogrammprodukt sowie mikroskopische Probe
CN108956669A (zh) * 2018-06-08 2018-12-07 浙江大学 一种金属燃料颗粒表面氧化层检测方法
CN110940689B (zh) * 2018-09-20 2022-06-21 无锡华润上华科技有限公司 SiC器件样品的制备方法及SiC器件的形貌分析方法
WO2020100179A1 (ja) * 2018-11-12 2020-05-22 株式会社日立ハイテク 画像形成方法及び画像形成システム
WO2020104031A1 (en) * 2018-11-22 2020-05-28 Applied Materials, Inc. Method for critical dimension measurement on a substrate, and apparatus for inspecting and cutting an electronic device on the substrate
US11440151B2 (en) * 2019-06-07 2022-09-13 Applied Materials Israel Ltd. Milling a multi-layered object
DE102019214939A1 (de) * 2019-09-27 2021-04-01 Carl Zeiss Microscopy Gmbh Verfahren zum Analysieren, Abbilden und/oder Bearbeiten eines Gebiets eines Objektsund Teilchenstrahlvorrichtung zum Ausführen des Verfahrens
US10903044B1 (en) 2020-02-12 2021-01-26 Applied Materials Israel Ltd. Filling empty structures with deposition under high-energy SEM for uniform DE layering
CN111195777A (zh) * 2020-03-02 2020-05-26 河北工程大学 一种陶瓷颗粒增强金属基复合材料超快激光精密刻蚀加工方法
WO2022016502A1 (en) * 2020-07-24 2022-01-27 Yangtze Memory Technologies Co., Ltd. Method of preparing and analyzing thin films
GB202013591D0 (en) * 2020-08-28 2020-10-14 Oxford Instr Nanotechnology Ltd Sample preparation and method aparatus
TWI753739B (zh) 2021-01-08 2022-01-21 閎康科技股份有限公司 物性分析方法、物性分析試片及其製備方法
US11501951B1 (en) 2021-05-14 2022-11-15 Applied Materials Israel Ltd. X-ray imaging in cross-section using un-cut lamella with background material
CN114942209A (zh) * 2021-09-23 2022-08-26 数岩科技股份有限公司 岩石的三维成像方法、装置、电子设备及存储介质
CN117007625A (zh) * 2023-09-28 2023-11-07 北京中科科仪股份有限公司 一种pn结的扫描电镜测试方法
CN119395064B (zh) * 2024-12-27 2025-04-18 北京特思迪半导体设备有限公司 半导体材料亚表面损伤层的检测方法

Family Cites Families (22)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0763064B2 (ja) * 1986-03-31 1995-07-05 株式会社日立製作所 Ic素子における配線接続方法
JP2595083B2 (ja) * 1988-06-08 1997-03-26 株式会社日立製作所 配線形成方法及びその装置
JPH0794512A (ja) * 1993-09-20 1995-04-07 Hitachi Ltd 配線形成方法及び装置
US6188068B1 (en) * 1997-06-16 2001-02-13 Frederick F. Shaapur Methods of examining a specimen and of preparing a specimen for transmission microscopic examination
US6039000A (en) 1998-02-11 2000-03-21 Micrion Corporation Focused particle beam systems and methods using a tilt column
JP2002167665A (ja) * 2000-11-30 2002-06-11 Sumitomo Heavy Ind Ltd 成膜装置及び方法
JP2004537758A (ja) * 2001-07-27 2004-12-16 エフ・イ−・アイ・カンパニー 電子ビーム処理
US7053370B2 (en) * 2001-10-05 2006-05-30 Canon Kabushiki Kaisha Information acquisition apparatus, cross section evaluating apparatus, cross section evaluating method, and cross section working apparatus
JP2004164966A (ja) * 2002-11-12 2004-06-10 Seiko Instruments Inc 関連情報をコード化して書き込む機能を備えたtem試料加工用集束イオンビーム装置
JP2004226079A (ja) * 2003-01-20 2004-08-12 Seiko Instruments Inc 表面あるいは断面加工観察方法及びその装置
US6958248B1 (en) * 2003-02-28 2005-10-25 Credence Systems Corporation Method and apparatus for the improvement of material/voltage contrast
JP4318962B2 (ja) * 2003-06-02 2009-08-26 エスアイアイ・ナノテクノロジー株式会社 薄膜加工における膜厚制御方法とそれを実行するシステム
US7611610B2 (en) * 2003-11-18 2009-11-03 Fei Company Method and apparatus for controlling topographical variation on a milled cross-section of a structure
US7442924B2 (en) 2005-02-23 2008-10-28 Fei, Company Repetitive circumferential milling for sample preparation
US7423263B2 (en) * 2006-06-23 2008-09-09 Fei Company Planar view sample preparation
JP5959139B2 (ja) * 2006-10-20 2016-08-02 エフ・イ−・アイ・カンパニー S/temのサンプルを分析する方法
US8835880B2 (en) * 2006-10-31 2014-09-16 Fei Company Charged particle-beam processing using a cluster source
JP5017059B2 (ja) * 2007-10-29 2012-09-05 エスアイアイ・ナノテクノロジー株式会社 試料作成装置および試料姿勢転換方法
JP2010230518A (ja) * 2009-03-27 2010-10-14 Toppan Printing Co Ltd 薄片試料作製方法
EP2402475A1 (en) * 2010-06-30 2012-01-04 Fei Company Beam-induced deposition at cryogenic temperatures
CN102401758A (zh) * 2010-09-17 2012-04-04 中芯国际集成电路制造(上海)有限公司 Tem样品制造方法
US8859963B2 (en) * 2011-06-03 2014-10-14 Fei Company Methods for preparing thin samples for TEM imaging

Also Published As

Publication number Publication date
TW201432242A (zh) 2014-08-16
US20150330877A1 (en) 2015-11-19
WO2014106200A2 (en) 2014-07-03
CN103913363A (zh) 2014-07-09
EP2939260A2 (en) 2015-11-04
CN105103270A (zh) 2015-11-25
EP2749863A2 (en) 2014-07-02
EP2939260A4 (en) 2016-01-20
JP2014130145A (ja) 2014-07-10
JP2016509669A (ja) 2016-03-31
EP2749863A3 (en) 2016-05-04
WO2014106200A3 (en) 2014-08-21

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