JP5800044B2 - 蒸気発生設備のスケール除去方法及びスケール除去剤 - Google Patents

蒸気発生設備のスケール除去方法及びスケール除去剤 Download PDF

Info

Publication number
JP5800044B2
JP5800044B2 JP2014025459A JP2014025459A JP5800044B2 JP 5800044 B2 JP5800044 B2 JP 5800044B2 JP 2014025459 A JP2014025459 A JP 2014025459A JP 2014025459 A JP2014025459 A JP 2014025459A JP 5800044 B2 JP5800044 B2 JP 5800044B2
Authority
JP
Japan
Prior art keywords
salt
scale
water
polyacrylic acid
acid
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
JP2014025459A
Other languages
English (en)
Japanese (ja)
Other versions
JP2015150484A (ja
Inventor
瑞之 酒井
瑞之 酒井
幸祐 志村
幸祐 志村
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Kurita Water Industries Ltd
Original Assignee
Kurita Water Industries Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority to JP2014025459A priority Critical patent/JP5800044B2/ja
Application filed by Kurita Water Industries Ltd filed Critical Kurita Water Industries Ltd
Priority to EP15748848.7A priority patent/EP3106439B1/en
Priority to CN201580008475.8A priority patent/CN105980317A/zh
Priority to PL15748848.7T priority patent/PL3106439T3/pl
Priority to US15/115,493 priority patent/US10384966B2/en
Priority to SG11201606348VA priority patent/SG11201606348VA/en
Priority to ES15748848T priority patent/ES2943022T3/es
Priority to MYPI2016702811A priority patent/MY183247A/en
Priority to PCT/JP2015/052012 priority patent/WO2015122264A1/ja
Priority to KR1020167021274A priority patent/KR20160120723A/ko
Priority to BR112016017693-6A priority patent/BR112016017693B1/pt
Priority to TW104103753A priority patent/TWI642636B/zh
Publication of JP2015150484A publication Critical patent/JP2015150484A/ja
Application granted granted Critical
Publication of JP5800044B2 publication Critical patent/JP5800044B2/ja
Priority to PH12016501568A priority patent/PH12016501568B1/en
Priority to US15/935,850 priority patent/US10703659B2/en
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Classifications

    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F5/00Softening water; Preventing scale; Adding scale preventatives or scale removers to water, e.g. adding sequestering agents
    • C02F5/08Treatment of water with complexing chemicals or other solubilising agents for softening, scale prevention or scale removal, e.g. adding sequestering agents
    • C02F5/10Treatment of water with complexing chemicals or other solubilising agents for softening, scale prevention or scale removal, e.g. adding sequestering agents using organic substances
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B08CLEANING
    • B08BCLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
    • B08B3/00Cleaning by methods involving the use or presence of liquid or steam
    • B08B3/02Cleaning by the force of jets or sprays
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B08CLEANING
    • B08BCLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
    • B08B3/00Cleaning by methods involving the use or presence of liquid or steam
    • B08B3/02Cleaning by the force of jets or sprays
    • B08B3/022Cleaning travelling work
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B08CLEANING
    • B08BCLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
    • B08B3/00Cleaning by methods involving the use or presence of liquid or steam
    • B08B3/04Cleaning involving contact with liquid
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B08CLEANING
    • B08BCLEANING IN GENERAL; PREVENTION OF FOULING IN GENERAL
    • B08B3/00Cleaning by methods involving the use or presence of liquid or steam
    • B08B3/04Cleaning involving contact with liquid
    • B08B3/041Cleaning travelling work
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F120/00Homopolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical or a salt, anhydride, ester, amide, imide or nitrile thereof
    • C08F120/02Monocarboxylic acids having less than ten carbon atoms; Derivatives thereof
    • C08F120/04Acids; Metal salts or ammonium salts thereof
    • C08F120/06Acrylic acid; Methacrylic acid; Metal salts or ammonium salts thereof
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L33/00Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
    • C08L33/02Homopolymers or copolymers of acids; Metal or ammonium salts thereof
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/20Organic compounds containing oxygen
    • C11D3/2075Carboxylic acids-salts thereof
    • C11D3/2082Polycarboxylic acids-salts thereof
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/37Polymers
    • C11D3/3746Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • C11D3/3757(Co)polymerised carboxylic acids, -anhydrides, -esters in solid and liquid compositions
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16Organic compounds
    • C11D3/37Polymers
    • C11D3/3746Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • C11D3/3757(Co)polymerised carboxylic acids, -anhydrides, -esters in solid and liquid compositions
    • C11D3/3765(Co)polymerised carboxylic acids, -anhydrides, -esters in solid and liquid compositions in liquid compositions
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D7/00Compositions of detergents based essentially on non-surface-active compounds
    • C11D7/22Organic compounds
    • C11D7/26Organic compounds containing oxygen
    • C11D7/265Carboxylic acids or salts thereof
    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23FNON-MECHANICAL REMOVAL OF METALLIC MATERIAL FROM SURFACE; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL; MULTI-STEP PROCESSES FOR SURFACE TREATMENT OF METALLIC MATERIAL INVOLVING AT LEAST ONE PROCESS PROVIDED FOR IN CLASS C23 AND AT LEAST ONE PROCESS COVERED BY SUBCLASS C21D OR C22F OR CLASS C25
    • C23F14/00Inhibiting incrustation in apparatus for heating liquids for physical or chemical purposes
    • C23F14/02Inhibiting incrustation in apparatus for heating liquids for physical or chemical purposes by chemical means
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F22STEAM GENERATION
    • F22BMETHODS OF STEAM GENERATION; STEAM BOILERS
    • F22B37/00Component parts or details of steam boilers
    • F22B37/02Component parts or details of steam boilers applicable to more than one kind or type of steam boiler
    • F22B37/48Devices or arrangements for removing water, minerals or sludge from boilers ; Arrangement of cleaning apparatus in boilers; Combinations thereof with boilers
    • F22B37/52Washing-out devices
    • CCHEMISTRY; METALLURGY
    • C02TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02FTREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2303/00Specific treatment goals
    • C02F2303/22Eliminating or preventing deposits, scale removal, scale prevention
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D2111/00Cleaning compositions characterised by the objects to be cleaned; Cleaning compositions characterised by non-standard cleaning or washing processes
    • C11D2111/10Objects to be cleaned
    • C11D2111/14Hard surfaces
    • C11D2111/20Industrial or commercial equipment, e.g. reactors, tubes or engines

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • General Chemical & Material Sciences (AREA)
  • Mechanical Engineering (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Environmental & Geological Engineering (AREA)
  • Water Supply & Treatment (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Hydrology & Water Resources (AREA)
  • General Engineering & Computer Science (AREA)
  • Emergency Medicine (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Preventing Corrosion Or Incrustation Of Metals (AREA)
  • Detergent Compositions (AREA)
  • Cleaning And De-Greasing Of Metallic Materials By Chemical Methods (AREA)
  • Air Humidification (AREA)
JP2014025459A 2014-02-13 2014-02-13 蒸気発生設備のスケール除去方法及びスケール除去剤 Active JP5800044B2 (ja)

Priority Applications (14)

Application Number Priority Date Filing Date Title
JP2014025459A JP5800044B2 (ja) 2014-02-13 2014-02-13 蒸気発生設備のスケール除去方法及びスケール除去剤
BR112016017693-6A BR112016017693B1 (pt) 2014-02-13 2015-01-26 Removedor de incrustação para remover incrustações depositadas em um sistema de uma instalação de geração de vapor
PL15748848.7T PL3106439T3 (pl) 2014-02-13 2015-01-26 Sposób usuwania kamienia kotłowego dla instalacji do wytwarzania pary
US15/115,493 US10384966B2 (en) 2014-02-13 2015-01-26 Method for removing scale and scale remover in steam generating facility
SG11201606348VA SG11201606348VA (en) 2014-02-13 2015-01-26 Scale removal method and scale removal agent for steam generating facilities
ES15748848T ES2943022T3 (es) 2014-02-13 2015-01-26 Método de eliminación de incrustación para instalaciones de generación de vapor
MYPI2016702811A MY183247A (en) 2014-02-13 2015-01-26 Method for removing scale and scale remover in steam generating facility
PCT/JP2015/052012 WO2015122264A1 (ja) 2014-02-13 2015-01-26 蒸気発生設備のスケール除去方法及びスケール除去剤
EP15748848.7A EP3106439B1 (en) 2014-02-13 2015-01-26 Scale removal method for steam generating facilities
CN201580008475.8A CN105980317A (zh) 2014-02-13 2015-01-26 蒸气产生设备的垢去除方法和垢去除剂
KR1020167021274A KR20160120723A (ko) 2014-02-13 2015-01-26 증기 발생 설비의 스케일 제거 방법 및 스케일 제거제
TW104103753A TWI642636B (zh) 2014-02-13 2015-02-04 蒸氣產生設備之水垢去除方法以及水垢去除劑
PH12016501568A PH12016501568B1 (en) 2014-02-13 2016-08-08 Method for removing scale and scale remover in steam generating facility
US15/935,850 US10703659B2 (en) 2014-02-13 2018-03-26 Scale remover in steam generating facility

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP2014025459A JP5800044B2 (ja) 2014-02-13 2014-02-13 蒸気発生設備のスケール除去方法及びスケール除去剤

Publications (2)

Publication Number Publication Date
JP2015150484A JP2015150484A (ja) 2015-08-24
JP5800044B2 true JP5800044B2 (ja) 2015-10-28

Family

ID=53800012

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2014025459A Active JP5800044B2 (ja) 2014-02-13 2014-02-13 蒸気発生設備のスケール除去方法及びスケール除去剤

Country Status (13)

Country Link
US (2) US10384966B2 (enExample)
EP (1) EP3106439B1 (enExample)
JP (1) JP5800044B2 (enExample)
KR (1) KR20160120723A (enExample)
CN (1) CN105980317A (enExample)
BR (1) BR112016017693B1 (enExample)
ES (1) ES2943022T3 (enExample)
MY (1) MY183247A (enExample)
PH (1) PH12016501568B1 (enExample)
PL (1) PL3106439T3 (enExample)
SG (1) SG11201606348VA (enExample)
TW (1) TWI642636B (enExample)
WO (1) WO2015122264A1 (enExample)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US10384966B2 (en) 2014-02-13 2019-08-20 Kurita Water Industries Ltd. Method for removing scale and scale remover in steam generating facility

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105753182A (zh) * 2016-03-08 2016-07-13 佛山市聚成生化技术研发有限公司 一种苯乙烯酮-马来酸酐-丁二烯-丁烯醇阻垢剂的制备方法及所制备的阻垢剂
CN106838874B (zh) * 2016-12-25 2019-01-18 大庆让胡路区轩鸿科技有限公司 一种无损型锅炉除垢的方法
CN109323237B (zh) * 2018-09-14 2020-01-07 福建宁德核电有限公司 核级聚丙烯酸分散剂用于核电厂蒸汽发生器湿保养的方法
CN111748147B (zh) * 2019-03-28 2022-04-05 合肥杰事杰新材料股份有限公司 一种阻垢聚丙烯材料及其制备方法
KR102144295B1 (ko) * 2019-04-19 2020-08-13 최영환 보일러 자동 세관 시스템
JP7050840B2 (ja) * 2020-03-12 2022-04-08 栗田工業株式会社 ボイラにおける蒸発管の腐食疲労の抑制方法
JP7083365B2 (ja) * 2020-03-12 2022-06-10 栗田工業株式会社 ボイラにおける蒸発管の腐食疲労の抑制方法
CN115448472A (zh) * 2022-08-17 2022-12-09 中核武汉核电运行技术股份有限公司 一种核级聚丙烯酸高温高压最优在线添加工艺
CN116947224A (zh) * 2023-09-21 2023-10-27 山东上远环保科技有限公司 一种循环水处理剂及其制备方法
US12146825B1 (en) * 2024-06-24 2024-11-19 King Fahd University Of Petroleum And Minerals System and methods for assessment of scale deposits in pipelines

Family Cites Families (21)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CA863696A (en) 1971-02-16 L. Salutsky Murrell Control of scaling in evaporators
GB1433221A (en) 1973-03-27 1976-04-22 Ciba Geigy Ag Water treatment
JPS5884099A (ja) 1981-11-05 1983-05-20 ナルコ・ケミカル・カンパニ− ボイラ−水のスケ−ル防止処理方法
AU563415B2 (en) * 1983-04-12 1987-07-09 Diversey Corporation Descaling heat exchangers with polyacrylate solution
CA2042341C (en) * 1990-05-23 2001-06-12 Judy H. Bardsley Silica scale inhibition
JP2923039B2 (ja) 1990-11-28 1999-07-26 三菱重工業株式会社 スケールの除去組成物
CN1068313A (zh) 1991-07-08 1993-01-27 化学工业部天津化工研究院 锅炉水处理剂
JP2000154996A (ja) 1998-08-19 2000-06-06 Miura Co Ltd ボイラのスケ―ル除去方法
JP2002273478A (ja) 2001-03-21 2002-09-24 Jsr Corp スケール防止方法
JP4725513B2 (ja) 2004-05-25 2011-07-13 栗田工業株式会社 冷却水の処理方法
JP2008006369A (ja) * 2006-06-29 2008-01-17 Kurita Water Ind Ltd スケール防止方法
DE102007019428A1 (de) * 2006-07-07 2008-10-30 Henkel Ag & Co. Kgaa Wasch-, Reinigungs- und Pflegemittel 2
DE102006047229A1 (de) * 2006-10-04 2008-04-10 Henkel Kgaa Wasch- oder Reinigungsmittelabgabesystem
JP5691128B2 (ja) * 2009-01-29 2015-04-01 栗田工業株式会社 スケール防止剤、およびスケール防止方法
JP5786277B2 (ja) 2010-03-31 2015-09-30 栗田工業株式会社 スケール除去方法及びスケール除去剤
JP5891630B2 (ja) 2011-07-22 2016-03-23 栗田工業株式会社 ボイラ水系のスケール除去方法
JP5862193B2 (ja) 2011-10-18 2016-02-16 栗田工業株式会社 蒸気発生器の水側缶内における鉄スケール防止方法
JP5900064B2 (ja) 2012-03-19 2016-04-06 栗田工業株式会社 エコノマイザを有するボイラの水処理方法
DE102013204824A1 (de) * 2013-03-15 2014-09-18 Henkel Ag & Co. Kgaa Reinigungsmittel für harte Oberflächen enthaltend Phosphorsäureester eines Polyether-modifizierten Alkylalkohols
PL2982655T3 (pl) 2013-04-02 2020-08-24 Kurita Water Industries Ltd. Sposób usuwania kamienia kotłowego w instalacji wytwarzania pary wodnej
JP5800044B2 (ja) 2014-02-13 2015-10-28 栗田工業株式会社 蒸気発生設備のスケール除去方法及びスケール除去剤

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US10384966B2 (en) 2014-02-13 2019-08-20 Kurita Water Industries Ltd. Method for removing scale and scale remover in steam generating facility
US10703659B2 (en) 2014-02-13 2020-07-07 Kurita Water Industries Ltd. Scale remover in steam generating facility

Also Published As

Publication number Publication date
US10384966B2 (en) 2019-08-20
BR112016017693A2 (enExample) 2017-08-08
JP2015150484A (ja) 2015-08-24
US20170050873A1 (en) 2017-02-23
SG11201606348VA (en) 2016-09-29
ES2943022T3 (es) 2023-06-08
EP3106439A4 (en) 2017-08-02
CN105980317A (zh) 2016-09-28
PH12016501568A1 (en) 2016-09-14
WO2015122264A1 (ja) 2015-08-20
US10703659B2 (en) 2020-07-07
US20180215637A1 (en) 2018-08-02
MY183247A (en) 2021-02-18
PL3106439T3 (pl) 2023-06-19
KR20160120723A (ko) 2016-10-18
TWI642636B (zh) 2018-12-01
PH12016501568B1 (en) 2016-09-14
EP3106439A1 (en) 2016-12-21
TW201538438A (zh) 2015-10-16
EP3106439B1 (en) 2023-03-22
BR112016017693B1 (pt) 2022-08-09

Similar Documents

Publication Publication Date Title
JP5800044B2 (ja) 蒸気発生設備のスケール除去方法及びスケール除去剤
JP5773091B2 (ja) 蒸気発生設備のスケール除去方法
JP5786277B2 (ja) スケール除去方法及びスケール除去剤
JP5970884B2 (ja) 防食方法
JP5891630B2 (ja) ボイラ水系のスケール除去方法
JP5900064B2 (ja) エコノマイザを有するボイラの水処理方法
JP5879699B2 (ja) ボイラ給水系の防食方法
JP6314560B2 (ja) 蒸気発生設備の水処理方法
JP5691697B2 (ja) 蒸気発生設備の水処理方法
JP5909956B2 (ja) ボイラにおけるエコノマイザの腐食抑制方法
JP2013068341A (ja) ボイラにおけるエコノマイザの防食方法
JP5862193B2 (ja) 蒸気発生器の水側缶内における鉄スケール防止方法
JP2011080725A (ja) ボイラ装置の運転方法
JP2014059076A (ja) ボイラ水系のスケール除去方法
JPWO2014199523A1 (ja) 蒸気発生設備の水処理方法
JP2012184465A (ja) ボイラ給水系及びボイラ缶内の防食方法
JP2012184466A (ja) ボイラ給水系及びボイラ缶内の防食方法

Legal Events

Date Code Title Description
A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20150519

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20150708

TRDD Decision of grant or rejection written
A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

Effective date: 20150728

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20150810

R150 Certificate of patent or registration of utility model

Ref document number: 5800044

Country of ref document: JP

Free format text: JAPANESE INTERMEDIATE CODE: R150

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250