JP5758922B2 - 粗１，３−ブタジエンから純粋な１，３−ブタジエンを蒸留抽出する方法及び装置 - Google Patents

粗１，３−ブタジエンから純粋な１，３−ブタジエンを蒸留抽出する方法及び装置 Download PDF

Info

Publication number
JP5758922B2
JP5758922B2 JP2012556488A JP2012556488A JP5758922B2 JP 5758922 B2 JP5758922 B2 JP 5758922B2 JP 2012556488 A JP2012556488 A JP 2012556488A JP 2012556488 A JP2012556488 A JP 2012556488A JP 5758922 B2 JP5758922 B2 JP 5758922B2
Authority
JP
Japan
Prior art keywords
butadiene
fraction
column
pure
stream
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
JP2012556488A
Other languages
English (en)
Japanese (ja)
Other versions
JP2013522175A5 (enExample
JP2013522175A (ja
Inventor
ハイダ，ベルント
フーゴ，ランドルフ
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BASF SE filed Critical BASF SE
Publication of JP2013522175A publication Critical patent/JP2013522175A/ja
Publication of JP2013522175A5 publication Critical patent/JP2013522175A5/ja
Application granted granted Critical
Publication of JP5758922B2 publication Critical patent/JP5758922B2/ja
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/34—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances
    • B01D3/40—Extractive distillation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14—Fractional distillation or use of a fractionation or rectification column
    • B01D3/141—Fractional distillation or use of a fractionation or rectification column where at least one distillation column contains at least one dividing wall
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C11/00—Aliphatic unsaturated hydrocarbons
    • C07C11/12—Alkadienes
    • C07C11/16—Alkadienes with four carbon atoms
    • C07C11/167—1, 3-Butadiene
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C7/00—Purification; Separation; Use of additives
    • C07C7/04—Purification; Separation; Use of additives by distillation
    • C07C7/05—Purification; Separation; Use of additives by distillation with the aid of auxiliary compounds
    • C07C7/08—Purification; Separation; Use of additives by distillation with the aid of auxiliary compounds by extractive distillation

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Analytical Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Water Supply & Treatment (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
JP2012556488A 2010-03-11 2011-03-08 粗１，３−ブタジエンから純粋な１，３−ブタジエンを蒸留抽出する方法及び装置 Active JP5758922B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE102010011014A DE102010011014A1 (de) 2010-03-11 2010-03-11 Verfahren und Vorrichtung zur destillativen Gewinnung von Rein-1,3-Butadien aus Roh-1,3-Butadien
DE102010011014.0 2010-03-11
PCT/EP2011/053473 WO2011110562A1 (de) 2010-03-11 2011-03-08 Verfahren und vorrichtung zur destillativen gewinnung von rein-1,3-butadien aus roh-1,3-butadien

Publications (3)

Publication Number Publication Date
JP2013522175A JP2013522175A (ja) 2013-06-13
JP2013522175A5 JP2013522175A5 (enExample) 2015-05-14
JP5758922B2 true JP5758922B2 (ja) 2015-08-05

Family

ID=43806920

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2012556488A Active JP5758922B2 (ja) 2010-03-11 2011-03-08 粗１，３−ブタジエンから純粋な１，３−ブタジエンを蒸留抽出する方法及び装置

Country Status (8)

Country Link
EP (1) EP2545019B1 (enExample)
JP (1) JP5758922B2 (enExample)
KR (1) KR101850562B1 (enExample)
CN (1) CN102781892B (enExample)
DE (1) DE102010011014A1 (enExample)
PL (1) PL2545019T3 (enExample)
TW (1) TWI500601B (enExample)
WO (1) WO2011110562A1 (enExample)

Families Citing this family (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR102014564B1 (ko) * 2011-12-05 2019-08-26 바스프 에스이 선택성 용매를 사용하는 추출 증류 공정을 위한 공급 스트림으로서의 증기상의 정제된 조 c4 분획을 제공하는 방법
US8642828B2 (en) 2012-01-03 2014-02-04 Basf Se Process for purifying a recycle stream from a 1,3-butadiene processing plant
WO2013102625A1 (de) * 2012-01-03 2013-07-11 Basf Se Verfahren zur aufreinigung eines recycle-stromes aus einer 1,3-butadien verarbeitenden anlage
US8766029B2 (en) 2012-01-11 2014-07-01 Basf Se Process for providing a vaporous purified crude C4 cut as a feed steam for an extractive distillation with a selective solvent
JP6216795B2 (ja) * 2012-09-20 2017-10-18 ルムス テクノロジー インコーポレイテッド ブタジエン抽出予備吸収塔
CN102942437A (zh) * 2012-11-22 2013-02-27 万达集团股份有限公司 Nmp法丁二烯一段抽提方法
BR112017000028B1 (pt) * 2014-07-08 2021-11-09 Basf Se Coluna, e, processo para separar uma mistura de hidrocarbonetos e/ou derivados de hidrocarboneto
US11034631B2 (en) 2017-01-25 2021-06-15 Basf Se Method for obtaining pure 1,3-butadiene
CN110418777B (zh) 2017-03-13 2023-04-28 巴斯夫欧洲公司 分离纯1,3-丁二烯的简化方法
US11952333B2 (en) 2019-09-13 2024-04-09 Sabic Global Technologies B.V. Integrated systems and methods for producing 1,3-butadiene via extractive distillation, distillation, and/or selective hydrogenation
WO2026162510A1 (en) 2025-01-29 2026-08-06 Basf Se Process for recovering 1,3-butadiene from a c4-fraction by extractive distillation using a selective solvent

Family Cites Families (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4277311A (en) 1976-06-14 1981-07-07 Bethlehem Steel Corporation Apparatus for distillation
FR2440984A1 (fr) * 1978-11-10 1980-06-06 Inst Francais Du Petrole Procede de traitement d'une coupe d'hydrocarbures c4 en vue de la recuperation du butadiene
US4277313A (en) * 1980-03-27 1981-07-07 El Paso Products Company Recovery of 1,3-butadiene
JPS5754129A (ja) * 1980-09-18 1982-03-31 Japan Synthetic Rubber Co Ltd Butajenmatahaisopurennoseiseihoho
JPS57123123A (en) * 1981-01-23 1982-07-31 Nippon Oil Co Ltd Preparation of high purity butadiene
DE19818810A1 (de) * 1998-04-27 1999-10-28 Basf Ag Verfahren zum Trennen eines C4-Kohlenwasserstoffgemisches
DE10056841A1 (de) * 2000-11-16 2002-05-23 Basf Ag Verfahren und Vorrichtung zur destillativen Gewinnung von 1,3-Reinbutadien aus 1,3-Rohbutadien
DE10105660A1 (de) * 2001-02-08 2002-08-14 Basf Ag Verfahren zur Gewinnung von Roh-1,3-Butadien durch Extraktivdestillation aus einem C4-Schnitt
DE10233621A1 (de) * 2002-07-24 2004-02-19 Basf Ag Verfahren zur Aufarbeitung von Roh-1,3-Butadien
DE10322655A1 (de) 2003-05-20 2004-12-09 Basf Ag Verfahren zur Gewinnung von Roh-1,3-Butadien aus einem C4-Schnitt
CN101172929B (zh) 2006-10-31 2010-05-19 中国石油化工股份有限公司 Nmp法丁二烯一段抽提方法
KR101111015B1 (ko) * 2008-07-17 2012-04-04 에스케이이노베이션 주식회사 아세틸렌 전환공정을 이용한 ｃ4 유분으로부터1,3-부타디엔을 분리하는 방법
CN101665399B (zh) * 2008-09-05 2012-07-25 中国石油化工股份有限公司 丁二烯生产方法

Also Published As

Publication number Publication date
EP2545019A1 (de) 2013-01-16
KR101850562B1 (ko) 2018-04-19
EP2545019B1 (de) 2014-03-05
CN102781892B (zh) 2016-05-04
KR20130016264A (ko) 2013-02-14
TW201139368A (en) 2011-11-16
TWI500601B (zh) 2015-09-21
WO2011110562A1 (de) 2011-09-15
CN102781892A (zh) 2012-11-14
PL2545019T3 (pl) 2014-08-29
JP2013522175A (ja) 2013-06-13
DE102010011014A1 (de) 2011-09-15

Similar Documents

Publication Publication Date Title
JP2013522175A (ja) 粗１，３−ブタジエンから純粋な１，３−ブタジエンを蒸留抽出する方法及び装置
JP5038573B2 (ja) Ｃ４−カットを処理するための方法および装置
JP5327485B2 (ja) アセチレン転換を用いた原油ｃ４留分からの１，３−ブタジエン分離方法
JP2013522175A5 (enExample)
US4277313A (en) Recovery of 1,3-butadiene
KR100203555B1 (ko) 추출 증류에 의해 부텐과 부탄을 분리하는 방법
US7557257B2 (en) Method for the separation of a crude C4 cut
JP4243246B2 (ja) 粗−１，３−ブタジエンの後処理法
TW201105631A (en) Fractional extraction of butadiene
JP2020506184A (ja) 純粋な１，３−ブタジエンを得る方法
JP6153535B2 (ja) 抽出蒸留プロセスのための供給流として選択的な溶媒を用いて蒸気精製粗製ｃ４留分を調製する方法
TW201542518A (zh) 自裂解汽油回收異戊二烯的方法
KR102597623B1 (ko) 순수 1,3-부타디엔을 얻기 위한 단순화된 방법
JPH0413330B2 (enExample)
EP3438079B1 (en) Method and apparatus for producing 1, 3-butadiene
JP7216279B2 (ja) １，３－ブタジエンの分離回収方法および分離回収装置

Legal Events

Date Code Title Description
A621 Written request for application examination

Free format text: JAPANESE INTERMEDIATE CODE: A621

Effective date: 20140304

A977 Report on retrieval

Free format text: JAPANESE INTERMEDIATE CODE: A971007

Effective date: 20141208

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20141216

A601 Written request for extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A601

Effective date: 20150306

A524 Written submission of copy of amendment under article 19 pct

Free format text: JAPANESE INTERMEDIATE CODE: A524

Effective date: 20150325

TRDD Decision of grant or rejection written
A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

Effective date: 20150519

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20150604

R150 Certificate of patent or registration of utility model

Ref document number: 5758922

Country of ref document: JP

Free format text: JAPANESE INTERMEDIATE CODE: R150

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250