CN102781892B - 用于从1,3-丁二烯原料蒸馏萃取纯1,3-丁二烯的方法和设备 - Google Patents

用于从1,3-丁二烯原料蒸馏萃取纯1,3-丁二烯的方法和设备 Download PDF

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Publication number
CN102781892B
CN102781892B CN201180012423.XA CN201180012423A CN102781892B CN 102781892 B CN102781892 B CN 102781892B CN 201180012423 A CN201180012423 A CN 201180012423A CN 102781892 B CN102781892 B CN 102781892B
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butadiene
column
fraction
stream
pure
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CN102781892A (zh
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B·海达
R·胡戈
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BASF SE
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BASF SE
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C7/00—Purification; Separation; Use of additives
    • C07C7/04—Purification; Separation; Use of additives by distillation
    • C07C7/05—Purification; Separation; Use of additives by distillation with the aid of auxiliary compounds
    • C07C7/08—Purification; Separation; Use of additives by distillation with the aid of auxiliary compounds by extractive distillation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14—Fractional distillation or use of a fractionation or rectification column
    • B01D3/141—Fractional distillation or use of a fractionation or rectification column where at least one distillation column contains at least one dividing wall
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/34—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances
    • B01D3/40—Extractive distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C11/00—Aliphatic unsaturated hydrocarbons
    • C07C11/12—Alkadienes
    • C07C11/16—Alkadienes with four carbon atoms
    • C07C11/167—1, 3-Butadiene

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Analytical Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Water Supply & Treatment (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
CN201180012423.XA 2010-03-11 2011-03-08 用于从1,3-丁二烯原料蒸馏萃取纯1,3-丁二烯的方法和设备 Active CN102781892B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE102010011014.0 2010-03-11
DE102010011014A DE102010011014A1 (de) 2010-03-11 2010-03-11 Verfahren und Vorrichtung zur destillativen Gewinnung von Rein-1,3-Butadien aus Roh-1,3-Butadien
PCT/EP2011/053473 WO2011110562A1 (de) 2010-03-11 2011-03-08 Verfahren und vorrichtung zur destillativen gewinnung von rein-1,3-butadien aus roh-1,3-butadien

Publications (2)

Publication Number Publication Date
CN102781892A CN102781892A (zh) 2012-11-14
CN102781892B true CN102781892B (zh) 2016-05-04

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Application Number Title Priority Date Filing Date
CN201180012423.XA Active CN102781892B (zh) 2010-03-11 2011-03-08 用于从1,3-丁二烯原料蒸馏萃取纯1,3-丁二烯的方法和设备

Country Status (8)

Country Link
EP (1) EP2545019B1 (enExample)
JP (1) JP5758922B2 (enExample)
KR (1) KR101850562B1 (enExample)
CN (1) CN102781892B (enExample)
DE (1) DE102010011014A1 (enExample)
PL (1) PL2545019T3 (enExample)
TW (1) TWI500601B (enExample)
WO (1) WO2011110562A1 (enExample)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP6153535B2 (ja) * 2011-12-05 2017-06-28 ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ 抽出蒸留プロセスのための供給流として選択的な溶媒を用いて蒸気精製粗製ｃ４留分を調製する方法
US8642828B2 (en) 2012-01-03 2014-02-04 Basf Se Process for purifying a recycle stream from a 1,3-butadiene processing plant
WO2013102625A1 (de) * 2012-01-03 2013-07-11 Basf Se Verfahren zur aufreinigung eines recycle-stromes aus einer 1,3-butadien verarbeitenden anlage
US8766029B2 (en) 2012-01-11 2014-07-01 Basf Se Process for providing a vaporous purified crude C4 cut as a feed steam for an extractive distillation with a selective solvent
HUE040522T2 (hu) 2012-09-20 2019-03-28 Lummus Technology Inc Butadién-extrakciós elõabszorber
CN102942437A (zh) * 2012-11-22 2013-02-27 万达集团股份有限公司 Nmp法丁二烯一段抽提方法
KR102358867B1 (ko) * 2014-07-08 2022-02-08 바스프 에스이 선택적인 용매를 사용하여 추출 증류에 의해서 탄화수소 및/또는 탄화수소 유도체의 혼합물을 분리하기 위한 분리 장치를 갖는 컬럼
JP7055812B2 (ja) * 2017-01-25 2022-04-18 ビーエーエスエフ ソシエタス・ヨーロピア 純粋な１，３－ブタジエンを得る方法
EP3596033B1 (de) * 2017-03-13 2021-05-12 Basf Se Vereinfachtes verfahren zur gewinnung von rein-1,3-butadien
US11952333B2 (en) 2019-09-13 2024-04-09 Sabic Global Technologies B.V. Integrated systems and methods for producing 1,3-butadiene via extractive distillation, distillation, and/or selective hydrogenation

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB2073235A (en) * 1980-03-27 1981-10-14 El Paso Products Co Recovery of 1,3-butadiene
CN1298375A (zh) * 1998-04-27 2001-06-06 巴斯福股份公司 C4烃混合物的分离方法
WO2010008109A1 (en) * 2008-07-17 2010-01-21 Sk Energy Co., Ltd. Process for 1,3-butadiene separation from a crude c4 stream with acetylene converter

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4277311A (en) 1976-06-14 1981-07-07 Bethlehem Steel Corporation Apparatus for distillation
FR2440984A1 (fr) * 1978-11-10 1980-06-06 Inst Francais Du Petrole Procede de traitement d'une coupe d'hydrocarbures c4 en vue de la recuperation du butadiene
JPS5754129A (ja) * 1980-09-18 1982-03-31 Japan Synthetic Rubber Co Ltd Butajenmatahaisopurennoseiseihoho
JPS57123123A (en) * 1981-01-23 1982-07-31 Nippon Oil Co Ltd Preparation of high purity butadiene
DE10056841A1 (de) * 2000-11-16 2002-05-23 Basf Ag Verfahren und Vorrichtung zur destillativen Gewinnung von 1,3-Reinbutadien aus 1,3-Rohbutadien
DE10105660A1 (de) * 2001-02-08 2002-08-14 Basf Ag Verfahren zur Gewinnung von Roh-1,3-Butadien durch Extraktivdestillation aus einem C4-Schnitt
DE10233621A1 (de) * 2002-07-24 2004-02-19 Basf Ag Verfahren zur Aufarbeitung von Roh-1,3-Butadien
DE10322655A1 (de) 2003-05-20 2004-12-09 Basf Ag Verfahren zur Gewinnung von Roh-1,3-Butadien aus einem C4-Schnitt
CN101172929B (zh) 2006-10-31 2010-05-19 中国石油化工股份有限公司 Nmp法丁二烯一段抽提方法
CN101665399B (zh) * 2008-09-05 2012-07-25 中国石油化工股份有限公司 丁二烯生产方法

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB2073235A (en) * 1980-03-27 1981-10-14 El Paso Products Co Recovery of 1,3-butadiene
CN1298375A (zh) * 1998-04-27 2001-06-06 巴斯福股份公司 C4烃混合物的分离方法
WO2010008109A1 (en) * 2008-07-17 2010-01-21 Sk Energy Co., Ltd. Process for 1,3-butadiene separation from a crude c4 stream with acetylene converter

Also Published As

Publication number Publication date
KR20130016264A (ko) 2013-02-14
JP2013522175A (ja) 2013-06-13
CN102781892A (zh) 2012-11-14
KR101850562B1 (ko) 2018-04-19
EP2545019A1 (de) 2013-01-16
TWI500601B (zh) 2015-09-21
TW201139368A (en) 2011-11-16
PL2545019T3 (pl) 2014-08-29
JP5758922B2 (ja) 2015-08-05
DE102010011014A1 (de) 2011-09-15
WO2011110562A1 (de) 2011-09-15
EP2545019B1 (de) 2014-03-05

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