JP5684968B2 - レオロジー調整剤/ヘアスタイリング樹脂 - Google Patents
レオロジー調整剤/ヘアスタイリング樹脂 Download PDFInfo
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- JP5684968B2 JP5684968B2 JP2007536731A JP2007536731A JP5684968B2 JP 5684968 B2 JP5684968 B2 JP 5684968B2 JP 2007536731 A JP2007536731 A JP 2007536731A JP 2007536731 A JP2007536731 A JP 2007536731A JP 5684968 B2 JP5684968 B2 JP 5684968B2
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- copolymer
- resin
- acid
- hair care
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- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 claims description 31
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- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 1
- 229940042585 tocopherol acetate Drugs 0.000 description 1
- NGSWKAQJJWESNS-ZZXKWVIFSA-N trans-4-coumaric acid Chemical class OC(=O)\C=C\C1=CC=C(O)C=C1 NGSWKAQJJWESNS-ZZXKWVIFSA-N 0.000 description 1
- LDHQCZJRKDOVOX-UHFFFAOYSA-N trans-crotonic acid Natural products CC=CC(O)=O LDHQCZJRKDOVOX-UHFFFAOYSA-N 0.000 description 1
- LOIYMIARKYCTBW-OWOJBTEDSA-N trans-urocanic acid Chemical compound OC(=O)\C=C\C1=CNC=N1 LOIYMIARKYCTBW-OWOJBTEDSA-N 0.000 description 1
- LOIYMIARKYCTBW-UHFFFAOYSA-N trans-urocanic acid Natural products OC(=O)C=CC1=CNC=N1 LOIYMIARKYCTBW-UHFFFAOYSA-N 0.000 description 1
- 125000005208 trialkylammonium group Chemical group 0.000 description 1
- 150000003628 tricarboxylic acids Chemical class 0.000 description 1
- 229940087291 tridecyl alcohol Drugs 0.000 description 1
- HHLJUSLZGFYWKW-UHFFFAOYSA-N triethanolamine hydrochloride Chemical compound Cl.OCCN(CCO)CCO HHLJUSLZGFYWKW-UHFFFAOYSA-N 0.000 description 1
- DGXNWWJYEMQHED-UHFFFAOYSA-N trimethyl-(4-methyl-3-oxopent-4-enyl)azanium Chemical compound CC(=C)C(=O)CC[N+](C)(C)C DGXNWWJYEMQHED-UHFFFAOYSA-N 0.000 description 1
- RRHXZLALVWBDKH-UHFFFAOYSA-M trimethyl-[2-(2-methylprop-2-enoyloxy)ethyl]azanium;chloride Chemical compound [Cl-].CC(=C)C(=O)OCC[N+](C)(C)C RRHXZLALVWBDKH-UHFFFAOYSA-M 0.000 description 1
- UUJLHYCIMQOUKC-UHFFFAOYSA-N trimethyl-[oxo(trimethylsilylperoxy)silyl]peroxysilane Chemical compound C[Si](C)(C)OO[Si](=O)OO[Si](C)(C)C UUJLHYCIMQOUKC-UHFFFAOYSA-N 0.000 description 1
- YRIDFQASBDRMBJ-UHFFFAOYSA-N undec-10-enamide Chemical compound NC(=O)CCCCCCCCC=C YRIDFQASBDRMBJ-UHFFFAOYSA-N 0.000 description 1
- 229940057402 undecyl alcohol Drugs 0.000 description 1
- AQLJVWUFPCUVLO-UHFFFAOYSA-N urea hydrogen peroxide Chemical compound OO.NC(N)=O AQLJVWUFPCUVLO-UHFFFAOYSA-N 0.000 description 1
- 229920001567 vinyl ester resin Polymers 0.000 description 1
- 235000019155 vitamin A Nutrition 0.000 description 1
- 239000011719 vitamin A Substances 0.000 description 1
- 235000019156 vitamin B Nutrition 0.000 description 1
- 239000011720 vitamin B Substances 0.000 description 1
- 235000019160 vitamin B3 Nutrition 0.000 description 1
- 239000011708 vitamin B3 Substances 0.000 description 1
- 235000019154 vitamin C Nutrition 0.000 description 1
- 239000011718 vitamin C Substances 0.000 description 1
- 235000019165 vitamin E Nutrition 0.000 description 1
- 229940046009 vitamin E Drugs 0.000 description 1
- 239000011709 vitamin E Substances 0.000 description 1
- 229940045997 vitamin a Drugs 0.000 description 1
- 239000008170 walnut oil Substances 0.000 description 1
- 239000011787 zinc oxide Substances 0.000 description 1
Images
Classifications
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/06—Preparations for styling the hair, e.g. by temporary shaping or colouring
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/817—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a single or double bond to nitrogen or by a heterocyclic ring containing nitrogen; Compositions or derivatives of such polymers, e.g. vinylimidazol, vinylcaprolactame, allylamines (Polyquaternium 6)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/817—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a single or double bond to nitrogen or by a heterocyclic ring containing nitrogen; Compositions or derivatives of such polymers, e.g. vinylimidazol, vinylcaprolactame, allylamines (Polyquaternium 6)
- A61K8/8176—Homopolymers of N-vinyl-pyrrolidones. Compositions of derivatives of such polymers
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- A—HUMAN NECESSITIES
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- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
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- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/48—Thickener, Thickening system
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
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- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
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- A61Q5/12—Preparations containing hair conditioners
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Description
2つの供給ポンプ、アンカー攪拌器(anchor agitator)、熱電対及びコンデンサーを備えた1リットルの四首のガラスケトルに、溶媒として500gのヘプタンを充填し、プロセスを通じて、窒素でパージしながら200rpmで攪拌した。次に、溶媒を、油浴で65℃に加熱し、その状態を30分間維持した。50gのN−ビニルピロリドン(VP)と1.0gのペンタエリトリトールトリアリルエーテル(PETE)を混合することによって供給溶液Iを用意した。50gのアクリル酸(AA)を瓶に量り取ることによって供給溶液IIを用意した。開始剤として200マイクロリットルのLuperox(登録商標)11M75をケトルに充填した。次に、供給溶液I及びIIを4時間に渡って一定の供給速度でケトルにポンプで同時に注入した。その後、生じた溶液を65℃で1時間保持し、反応温度を90℃まで上昇させた。次いで、100マイクロリットルのLuperox(登録商標)11M75を2時間ごとに4回さらに添加し、反応装置を、最後の分量のLuperox(登録商標)11M75を充填した後、さらに2時間、90℃で保持した。次に、内容物を冷却し、排出した。溶媒を100℃の温度のオーブンにて除去した。さらに、生じた樹脂粉末を100℃の真空オーブンで乾燥した。生成物はVP/AA/PETEの重量比が50/50/1であるPETEで架橋された、VPとAAの架橋した直線状コポリマーであった。
アンカー攪拌器(anchor agitator)、熱電対及びコンデンサーを備えた1リットルの四首のガラスケトルに、溶媒として500gのヘプタンを充填し、プロセスを通じて、窒素でパージしながら200rpmで攪拌した。次に、溶媒を、油浴で65℃に加熱し、その状態を30分間維持した。50gのN−ビニルカプロラクタム(VCL)と1.5gのペンタエリトリトールトリアリルエーテル(PETE)を混合することによって供給溶液Iを用意した。50gのアクリル酸(AA)を瓶に量り取ることによって供給溶液IIを用意した。次に、200マイクロリットルのt−ブチルペルオキシピバレート開始剤をケトルに充填した。供給溶液I及びIIを4時間に渡って一定の供給速度でケトルに同時に充填した。溶液を65℃で1時間保持し、温度を90℃まで上昇させた。次いで、200マイクロリットルのt−ブチルペルオキシピバレートを2時間ごとに4回さらに添加し、反応装置を、最後の分量のt−ブチルペルオキシピバレートを充填した後、さらに2時間、90℃で保持した。次に、内容物を冷却し、排出した。溶媒を100℃の温度のオーブンにて除去した。生じた樹脂粉末を100℃の真空オーブンでさらに乾燥した。生成物はVCL/AA/PETEの重量比が50/50/1.5であるPETEで架橋された、VCLとAAの架橋した直線状コポリマーであった。
2つの供給ポンプ、アンカー攪拌器(anchor agitator)、熱電対及びコンデンサーを備えた1リットルの四首のガラスケトルに、溶媒として500gのヘプタンを充填し、プロセスを通じて、窒素でパージしながら200rpmで攪拌した。次に、溶媒を、油浴で65℃に加熱し、その状態を30分間維持した。60gのN−ビニルピロリドン(VP)と、15gのステアリルメタクリレート(SM)と、1.0gのペンタエリトリトールトリアリルエーテル(PETE)を混合することによって供給溶液Iを用意した。25gのアクリル酸(AA)を瓶に量り取ることによって供給溶液IIを用意した。開始剤として200マイクロリットルのLuperox(登録商標)11M75をケトルに充填した。その後、供給溶液I及びIIを4時間に渡って一定の供給速度でケトルに同時にポンプで注入した。次に、生じた溶液を65℃で1時間保持し、反応温度を90℃まで上昇させた。次いで、100マイクロリットルのLuperox(登録商標)11M75を2時間ごとに4回さらに添加し、反応装置を、最後の分量のLuperox(登録商標)11M75を充填した後でさらに2時間、90℃で保持した。次に、内容物を冷却し、排出した。溶媒を100℃の温度のオーブンにて除去した。生じた樹脂粉末を100℃の真空オーブンでさらに乾燥した。生成物はVP/AA/SM/PETEの重量比が600/25/15/1であるPETEで架橋された、VPとAAとSMの架橋した直線状三元重合体であった。
2つの供給ポンプ、アンカー攪拌器(anchor agitator)、熱電対及びコンデンサーを備えた1リットルの四首のガラスケトルに、溶媒として600gのヘプタンを充填し、プロセスを通じて、窒素でパージしながら300rpmで攪拌した。次に、溶媒を、油浴で70℃に加熱し、その状態を30分間維持した。50gのN−ビニルピロリドン(VP)と1.0gのペンタエリトリトールトリアリルエーテル(PETE)を混合することによって供給溶液Iを用意した。50gのメタクリル酸(MAA)を瓶に量り取ることによって供給溶液IIを用意した。300マイクロリットルのt−ブチルペルオキシピバレート開始剤をケトルに充填した。供給溶液I及び供給溶液IIを5時間に渡って一定の供給速度でケトルにポンプで同時に注入した。溶液を70℃で1時間保持し、溶液をステンレスの高圧反応装置に移した。次いで、0.5gのジ−t−ブチルペルオキシドをさらに添加した。反応装置の温度を130℃まで上昇させ、10時間保持した。次に、内容物を冷却し、排出した。溶媒を100℃の温度のオーブンにて除去した。生じた樹脂粉末を100℃の真空オーブンでさらに乾燥した。生成物はVP/MAA/PETEの重量比が50/50/1であるPETEで架橋された、VPとMAAの架橋した直線状コポリマーであった。
1.93.51部の蒸留水を適当な容器に充填する。
2.0.05部の前中和剤(pre-neutralizer)である2−アミノ−2−メチルプロパノール(AMP)を添加する。
3.中程度の速さで攪拌を開始する。
4.1.0部のポリマー粉末にゆっくりと撒く。もう一つの方法としては、粉末を、最終的にはそのまま全体にわたって分散するように「ダンプする」ことができる。
5.中程度の速さで30〜60分間混合して、完全に分散するようにし、白色の粒子が存在する場合、粒子が見えなくなるまで混合し続ける。ポリマーを「ダンプした」場合、混合時間を2倍にする。
6.0.44部の中和剤AMPと5部の蒸留水を予め混合し、メインのバッチに添加する。
7.回転数を下げて、過剰な空気混入を防ぐ。
8.30〜60分間混合して、均一なゲルを確保する。
9.生成物がpH6.7、10rpmにおける粘度RV TCが50,000cPsである透明なゲルとして生じる。
1.A相の成分を組み合わせ、混合する。
2.B相を組み合わせ、均一になるまで混合する。
3.B相をA相に添加し、混合する。
4.C相を添加する。
5.D相の成分を添加する。
6.E相を組み合わせ、透明になるまで混合する。
7.E相を添加し、混合する。
1.A相の成分を組み合わせ、混合する。
2.B相を組み合わせ、均一になるまで混合する。
3.B相をA相に添加し、混合する。
4.C相を添加する。
5.D相の成分を添加する。
6.E相を組み合わせ、透明になるまで混合する。
7.E相を添加し、混合する。
1.A相の成分を水中に分散させ、攪拌する。
2.最初の5種のB相の成分を組み合わせる。均一になるまで攪拌する。
3.B相をA相に添加し、室温で均質化する。均一になるまで攪拌する。
4.均一になったら、C相を添加する。
5.D相の成分を添加し、攪拌する。水の損失を定量分析する(QS for water loss)。
1.A相の成分を水中に分散させ、攪拌する。
2.最初の5種のB相の成分を組み合わせる。均一になるまで攪拌する。
3.B相をA相に添加し、室温で均質化する。均一になるまで攪拌する。
4.均一になったら、C相を添加する。
5.D相の成分を添加し、攪拌する。水の損失を定量分析する(QS for water loss)。
1.A相の成分を水に添加し、攪拌する。65℃に加熱する。
2.B相を組み合わせる。加熱し、P-151が溶解するまで攪拌する。
3.B相をA相に添加し、均質化する。
4.均一になったら、C相を添加し、均質化する。35℃に冷却する。
5.D相の成分を添加し、攪拌する。水の損失を定量分析する(QS for water loss)。
(1)アクリルエステル、メタクリルエステル、アクリルアミド又はメタクリルアミド由来のホモポリマー及びコポリマー(コポリマーは、アクリルアミド、メタクリルアミド、ジアセトン・アクリルアミド、アクリルアミド及びメタクリルアミド、アクリル酸もしくはメタクリル酸もしくはそれらのエステル、ビニルピロリドンもしくはビニルカプロラクタムなどのビニルラクタム、並びにビニルエステルに由来する1種または複数の単位を含んでもよい。具体的な例としては、アクリルアミドと、硫酸ジメチル又はハロゲン化アルキルで4級化したジメチルアミノエチルメタクリレートとのコポリマー;アクリルアミドと、塩化メタクリロイルオキシエチルトリメチルアンモニウムとのコポリマー;アクリルアミドとメタクリロイルオキシエチルトリメチルアンモニウムメトサルフェートとのコポリマー;International Specialty Products社によってGAFQUATの名の下で市販されている製品などのビニルピロリドン/任意選択的に4級化されている、ジアルキルアミノアルキルアクリレート又はジアルキルアミノアルキルメタクリレートのコポリマー;International Specialty Products社によってGAFFIX VC 713の名の下で市販されている製品などのジメチルアミノエチルメタクリレート/ビニルカプロラクタム/ビニルピロリドンの三元重合体;International Specialty Products社によってSTYLEZE CC 10の名の下で市販されているビニルピロリドン/メタクリルアミドプロピルジメチルアミンのコポリマー;並びにInternational Specialty Products社によってGAFQUAT HS 100の名の下で市販されている製品などのビニルピロリドン/4級化ジメチルアミノプロピルメタクリルアミドコポリマーが挙げられる。)、
(2)トリメチルアンモニウム基で置換したエポキシドと反応したヒドロキシエチルセルロース第4級アンモニウムなどの第4級アンモニウム基を含むセルロースエーテルの誘導体、
(3)セルロースコポリマーなどのカチオン性セルロースの誘導体、又はメタクリロイルエチルトリメチルアンモニウム、メタクリルアミドプロピルトリメチルアンモニムもしくはジメチルジアリルアンモニウムの塩でグラフトされたヒドロキシアルキルセルロース、及びヒドロキシメチル−、ヒドロキシエチル−もしくはヒドロキシプロピル−セルロースなどの米国特許第4,131,576号に記載されている水溶性の第4級アンモニウムモノマーでグラフトされたセルロースの誘導体、
(4)米国特許第3,589,578号、米国特許第4,031,307号に記載されているものなどのカチオン性多糖類、カチオン性トリアルキルアンモニウム基を含むグアールガム及び例えば2,3−エポキシプロプルトリメチルアンモニウムの塩化物といった塩で修飾されたグアールガム、
(5)できる限り酸素原子、硫黄原子、窒素原子又は芳香族環もしくは複素環によって割り込まれている直鎖もしくは分岐鎖を有する、ピペラジニル単位及びアルキレンもしくはヒロドキシアルキレンの二価のラジカルからなるポリマー、並びに当該ポリマーの酸化及び/又は四級化の生成物、
(6)酸化合物とポリアミンとの重縮合によって製造された水溶性ポリアミノアミド。これらのポリアミノアミド(これらのポリアミノアミドは網目状となっていてもよい)、
(7)ポリアルコイレンポリアミン(polyalcoylene polyamine)とポリカルボン酸との縮合後、二官能性剤によってアルコイレーション(alcoylation)することにより生じたポリアミノアミドの誘導体
(8)2つの第1級アミン基と少なくとも1つの第2級アミン基を含むポリアルキレンポリアミンとジグリコール酸及び3〜8の炭素原子を有する飽和ジカルボキシル脂肪族系酸の中から選択されるジオキシカルボキシル酸との反応によって得られたポリマー(当該ポリマーは米国特許第3,227,615号及び米国特許第2,962,347号に記載されている)、
(9)塩化ジメチルジアリルアンモニウムのホモポリマー及び塩化ジアリルジメチルアンモニウムとアクリルアミドとのコポリマーなどのアルキルジアリルアミン又はジアルキルジアリルアンモニウムのシクロポリマー、
(10)塩化ヘキサジメトリンなどの第4級ジアンモニウムポリマー(この種のポリマーは、特に、米国特許第2,273,780号、米国特許第2,375,853号、米国特許第2,388,614号、米国特許第2,454,547号、米国特許第3,206,462号、米国特許第2,261,002号、米国特許第2,271,378号、米国特許第3,874,870号、米国特許第4,001,432号、米国特許第3,929,990号、米国特許第3,966,904号、米国特許第4,005,193号、米国特許第4,025,617号、米国特許第4,025,627号、米国特許第4,025,653号、米国特許第4,026,945号及び米国特許第4,027,020号に記載されている)、
(11)第4級ポリアンモニウムポリマー(例えば、Miranol社によって市販されているMirapol(登録商標)A 15、、Mirapol(登録商標)AD1、、Mirapol(登録商標)AZ1及び、Mirapol(登録商標)175の製品が挙げられる)、
(12)BASF社によってLuviquat(登録商標)FC 905、FC 550、及びFC 370の名の下で市販されている製品などのビニルピロリドンとビニルイミダゾールの第4級ポリマー、
(13)第4級ポリアミン、
(14)本技術分野にて既知である網目状ポリマー、
などがある。
a)窒素上でアルキルラジカルで置換されたアクリルアミド又はメタクリルアミドから選択される少なくとも1種のモノマー、
b)1種又は複数の反応性カルボキシル基を含む少なくとも1種の酸のコポリマー、
c)アクリル酸及びメタクリル酸の第1級、第2級、第3級及び第4級のアミノ置換基を有するエステル、並びにジメチルスルフェート又はジエチルスルフェートでジメチルアミノエチルメタクリレートを4級化した生成物などの少なくとも1種の塩基性のコモノマー
に由来する繰り返し単位を含むポリマーから選択される両性ポリマーであってもよい。
及び(U):
アクリル酸ナトリウム/ビニルアルコール・コポリマー;ナトリウム・カルボマー;ナトリウム・カルボキシメチルキチン;ナトリウム・カルボキシメチルデキストラン;ナトリウム・カルボキシメチル・ベータ−グルカン;ナトリウム・カルボキシメチルスターチ;ナトリウム・カラゲナン;ナトリウム・セルロース・スルフェート;塩化ナトリウム;ナトリウム・シクロデキストリン・スルフェート;ナトリウム・ヒドロキシプロピル・スターチ・ホスフェート;ナトリウム・イソオクチレン/MAコポリマー;ナトリウム・マグネシウム・フルオロシリケート;オレイン酸ナトリウム;パルミチン酸ナトリウム;ナトリウム・パームカーネレート;ポリアクリル酸ナトリウム;ナトリウム・ポリアクリレート・スターチ;ナトリウム・ポリアクリロイルジメチルタウレート;ポリガンマ−グルタミン酸ナトリウム;ポリメタクリル酸ナトリウム;ナトリウム・ポリスチレン・スルホネート;ナトリウム・シリコアルミネート;ナトリウム・スターチ・オクテニルスクシネート;ステアリン酸ナトリウム;ナトリウム・ステアロキシPG−ヒドロキシエチルセルロース・スルホネート;ナトリウム・スチレン/アクリレートコポリマー;硫酸ナトリウム;牛脂脂肪酸ナトリウム;ナトリウム・タウリド(tauride)・アクリレート/アクリル酸/アクリロナイトロジェンコポリマー;ナトリウム・トコフェリル・ホスフェート;Solanum Tuberosum(ジャガイモ)デンプン;ソイアミド DEA;ソイアミドプロピルベタイン;スターチ/アクリレート/アクリルアミドコポリマー;スターチ・ヒドロキシプロピルトリモニウム・クロライド;ステアルアミド AMP;ステアルアミド DEA;ステアルアミド DEA−ジステアレート;ステアルアミド DIBA−ステアレート;ステアルアミド MEA;ステアルアミド MEA−ステアレート;ステアルアミド MIPA;ステアルアミドプロピルベタイン;ステアレス−60 セチルエーテル;ステアレス-100/PEG-136/HDIコポリマー;ステアリルアルコール;ステアリルベタイン;Sterculia Urensガム;合成金雲母;トールアミド DEA;牛脂アルコール;牛脂アミド DEA;牛脂アミド MEA;牛脂アミドプロピルベタイン;牛脂アミドプロピルヒドロキシスルタイン;牛脂アミンオキシド;牛脂ベタイン;牛脂ジヒドロキシエチルベタイン;Tamarindus Indica種子ガム;タピオカデンプン;TEA-アルギネート;TEA-カルボマー;TEA-ヒドロクロライド;トリデセス−2 カルボキシアミド MEA;トリデシルアルコール;トリエチレングリコールジベンゾエート;トリメチルペンタノールヒドロキシエチルエーテル;Triticum Vulgare(コムギ)胚芽粉末;Triticum Vulgare(コムギ)穀粒;Triticum Vulgare(コムギ)デンプン;トロメタミンアクリレート/アクリロナイトロジェンコポリマー;トロメタミン・マグネシウム・アルミニウム・シリケート;ウンデシルアルコール;ウンデシレンアミド DEA;ウンデシレンアミド MEA;ウンデシレンアミドプロピルベタイン;ウェランガム;コムギ胚芽油脂肪酸アミド DEA;コムギ胚芽油脂肪酸アミドプロピルベタイン;キサンタンガムの酵母ベータグルカン;酵母ポリ多糖及びZea Mays(コーン)デンプンなどがある。
次に、最終的に水で該組成物をすすぐことからなることを特徴とする。したがって、本発明による方法は、ヘアースタイル、トリートメント、ケア、洗浄又は皮膚、髪及びその他のケラチン物質の化粧品の除去を維持することを可能にする。
Claims (14)
- 架橋した直線状ポリ(ビニルアミド/重合可能なカルボン酸)コポリマーを含み、
該コポリマーは、モノマーの総重量に対して、ビニルピロリドンからなる25〜75%のビニルアミドモノマーと、(メタ)アクリル酸からなる25〜75%の重合可能なカルボン酸モノマーと、ペンタエリトリトールトリアリルエーテルからなる0.5〜2%の架橋剤とが沈殿重合してなり、
pH9の水溶液における粘度が55,000cps(ブルックフィールドRVT, T-bar C@10rpm, 60秒, 1%固形分)であることを特徴とするレオロジー調整樹脂。 - 前記重合可能なカルボン酸がアクリル酸である請求項1記載のレオロジー調整樹脂。
- モノマーの総重量に基づいて、50〜95%の非極性で除去可能な有機溶媒中で、0.1〜5%のフリーラジカル開始剤の存在下で、総モノマーに基づいて、25〜75%のビニルピロリドンからなるビニルアミドと、25〜75%の(メタ)アクリル酸からなる重合可能なカルボン酸と、0.5〜2%のペンタエリトリトールトリアリルエーテルからなる架橋剤との5〜50重量%の反応混合物を沈殿重合し、溶媒を除去して、粉末状の樹脂を得ることからなる請求項1記載のレオロジー調整樹脂を製造する方法。
- 前記反応混合物が10〜25%の前記モノマーと75〜90%の前記溶媒を含む請求項3記載の方法。
- 請求項1記載のレオロジー調整樹脂を含むヘアケア組成物。
- 0.1〜20重量%の前記樹脂を含む請求項5記載のヘアケア組成物。
- 90%RH及び26.7℃(80°F)で4時間に渡って80〜100%のカール保持力を示す請求項5記載のヘアケア組成物。
- 前記保持力が90%である請求項7記載のヘアケア組成物。
- 請求項1記載の樹脂を含むスキンケア処方物。
- 0.0001〜1Pa(10〜100,000ダイン/cm2)の降伏応力値を有する請求項5記載のヘアケア組成物。
- 前記値が0.001〜0.1Pa(100〜10,000ダイン/cm2)である請求項10記載の組成物。
- 髪固定剤、スタイリングジェル、クリーム、ムース又はスプレーである請求項1記載のレオロジー調整剤を含むヘアケア組成物。
- 0.2〜10%の前記樹脂を含む請求項6記載のヘアケア組成物。
- 0.5〜5%の前記樹脂を含む請求項13記載のヘアケア組成物。
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CN109988269A (zh) * | 2018-01-02 | 2019-07-09 | 博爱新开源医疗科技集团股份有限公司 | 一种新型粉末增粘剂及其制备方法 |
KR20210008483A (ko) | 2018-04-12 | 2021-01-22 | 루브리졸 어드밴스드 머티어리얼스, 인코포레이티드 | 모발 개질 조성물 및 이의 방법 |
US11878067B2 (en) * | 2019-07-31 | 2024-01-23 | L'oreal | Gel compositions containing copolymer of vinylpyrrolidone and acrylic acid |
WO2021021978A1 (en) | 2019-07-31 | 2021-02-04 | L'oreal | Compositions containing copolymer of vinylpyrrolidone and acrylic acid and film forming agent |
JP2024519822A (ja) | 2021-05-17 | 2024-05-21 | ルブリゾル アドバンスド マテリアルズ, インコーポレイテッド | 色落ちを軽減するためのヘアカラー組成物 |
KR20240057426A (ko) | 2021-09-03 | 2024-05-02 | 루브리졸 어드밴스드 머티어리얼스, 인코포레이티드 | 모발 성장을 촉진하기 위한 미로탐누스 종의 추출물의 용도 |
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US5015708A (en) | 1989-06-26 | 1991-05-14 | Gaf Chemicals Corporation | Precipitation polymerization of terpolymers of a vinyl lactam, a polymerizable carboxylic acid and a hydrophobic monomer in an aliphatic hydrocarbon solvent |
JP3042546B2 (ja) * | 1991-04-23 | 2000-05-15 | 昭和電工株式会社 | 微粒子状の架橋型n−ビニルアミド樹脂及びミクロゲル、その製造法及び用途 |
JP3188283B2 (ja) * | 1991-05-21 | 2001-07-16 | 昭和電工株式会社 | 液体吸収剤 |
US5711951A (en) * | 1996-03-13 | 1998-01-27 | Isp Investments Inc. | Aqueous product comprising discrete, stabilized, microdroplets of an oil and an in situ polymerized vinyl monomer, containing a thickening agent to homogeneously suspend the microdroplets throughout the medium |
JPH1017479A (ja) * | 1996-07-01 | 1998-01-20 | Showa Denko Kk | 塩含有外用剤 |
JP2000016914A (ja) * | 1998-07-01 | 2000-01-18 | Kanebo Ltd | 化粧料 |
US6368607B1 (en) * | 1998-07-24 | 2002-04-09 | Isp Investments Inc. | Product-structurant composition for personal care formulations |
US6361768B1 (en) * | 1998-12-29 | 2002-03-26 | Pmd Holdings Corp. | Hydrophilic ampholytic polymer |
JP2000351717A (ja) * | 1999-04-09 | 2000-12-19 | Kose Corp | 毛髪化粧料 |
WO2002032975A1 (de) | 2000-10-18 | 2002-04-25 | Basf Aktiengesellschaft | Hydrogel-bildende polymerisate |
CN100335032C (zh) * | 2002-10-09 | 2007-09-05 | 宝洁公司 | 降低粘着性的化妆品组合物 |
US6566473B1 (en) * | 2002-11-20 | 2003-05-20 | Isp Investments Inc. | Process for making a vinyl amide polymer composition for skin and hair compositions |
DE10261750A1 (de) * | 2002-12-30 | 2004-07-15 | Basf Ag | Ampholytisches Copolymer und dessen Verwendung |
US7205271B2 (en) * | 2004-10-14 | 2007-04-17 | Isp Investments Inc. | Rheology modifier/hair styling resin |
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KR20080016778A (ko) | 2008-02-22 |
JP2008516950A (ja) | 2008-05-22 |
WO2006044193A3 (en) | 2006-10-05 |
BRPI0516089B1 (pt) | 2016-08-09 |
CN101341239B (zh) | 2012-11-28 |
AU2005296052B2 (en) | 2011-07-21 |
EP1809731B1 (en) | 2017-04-19 |
CA2584177C (en) | 2013-09-10 |
AU2005296052A1 (en) | 2006-04-27 |
CA2584177A1 (en) | 2006-04-27 |
US7205271B2 (en) | 2007-04-17 |
BRPI0516089A (pt) | 2008-08-19 |
EP1809731A4 (en) | 2008-05-28 |
MX2007004468A (es) | 2007-05-07 |
KR101261080B1 (ko) | 2013-05-06 |
CN101341239A (zh) | 2009-01-07 |
US20070202064A1 (en) | 2007-08-30 |
US20060084586A1 (en) | 2006-04-20 |
EP1809731A2 (en) | 2007-07-25 |
WO2006044193A2 (en) | 2006-04-27 |
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