JP5668689B2 - ポリテトラフルオロエチレン水性乳化液及びその製造方法、該水性乳化液を用いて得られるポリテトラフルオロエチレン水性分散液、ポリテトラフルオロエチレンファインパウダー並びに延伸多孔体 - Google Patents

ポリテトラフルオロエチレン水性乳化液及びその製造方法、該水性乳化液を用いて得られるポリテトラフルオロエチレン水性分散液、ポリテトラフルオロエチレンファインパウダー並びに延伸多孔体 Download PDF

Info

Publication number
JP5668689B2
JP5668689B2 JP2011539417A JP2011539417A JP5668689B2 JP 5668689 B2 JP5668689 B2 JP 5668689B2 JP 2011539417 A JP2011539417 A JP 2011539417A JP 2011539417 A JP2011539417 A JP 2011539417A JP 5668689 B2 JP5668689 B2 JP 5668689B2
Authority
JP
Japan
Prior art keywords
ptfe
emulsion
polytetrafluoroethylene
aqueous
aqueous emulsion
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
JP2011539417A
Other languages
English (en)
Japanese (ja)
Other versions
JPWO2011055824A1 (ja
Inventor
信弥 樋口
信弥 樋口
松岡 康彦
康彦 松岡
小林 茂樹
茂樹 小林
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
AGC Inc
Original Assignee
Asahi Glass Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=43970056&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=JP5668689(B2) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Asahi Glass Co Ltd filed Critical Asahi Glass Co Ltd
Priority to JP2011539417A priority Critical patent/JP5668689B2/ja
Publication of JPWO2011055824A1 publication Critical patent/JPWO2011055824A1/ja
Application granted granted Critical
Publication of JP5668689B2 publication Critical patent/JP5668689B2/ja
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F214/00Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen
    • C08F214/18Monomers containing fluorine
    • C08F214/26Tetrafluoroethene
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F14/00Homopolymers and copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen
    • C08F14/18Monomers containing fluorine
    • C08F14/26Tetrafluoroethene
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08JWORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J3/00Processes of treating or compounding macromolecular substances
    • C08J3/02Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques
    • C08J3/03Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques in aqueous media
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08JWORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2327/00Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Derivatives of such polymers
    • C08J2327/02Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Derivatives of such polymers not modified by chemical after-treatment
    • C08J2327/12Characterised by the use of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by a halogen; Derivatives of such polymers not modified by chemical after-treatment containing fluorine atoms
    • C08J2327/18Homopolymers or copolymers of tetrafluoroethylene

Landscapes

  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Dispersion Chemistry (AREA)
  • Polymerisation Methods In General (AREA)
  • Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
  • Manufacture Of Porous Articles, And Recovery And Treatment Of Waste Products (AREA)
JP2011539417A 2009-11-09 2010-11-08 ポリテトラフルオロエチレン水性乳化液及びその製造方法、該水性乳化液を用いて得られるポリテトラフルオロエチレン水性分散液、ポリテトラフルオロエチレンファインパウダー並びに延伸多孔体 Active JP5668689B2 (ja)

Priority Applications (1)

Application Number Priority Date Filing Date Title
JP2011539417A JP5668689B2 (ja) 2009-11-09 2010-11-08 ポリテトラフルオロエチレン水性乳化液及びその製造方法、該水性乳化液を用いて得られるポリテトラフルオロエチレン水性分散液、ポリテトラフルオロエチレンファインパウダー並びに延伸多孔体

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
JP2009255949 2009-11-09
JP2009255949 2009-11-09
PCT/JP2010/069863 WO2011055824A1 (ja) 2009-11-09 2010-11-08 ポリテトラフルオロエチレン水性乳化液及びその製造方法、該水性乳化液を用いて得られるポリテトラフルオロエチレン水性分散液、ポリテトラフルオロエチレンファインパウダー並びに延伸多孔体
JP2011539417A JP5668689B2 (ja) 2009-11-09 2010-11-08 ポリテトラフルオロエチレン水性乳化液及びその製造方法、該水性乳化液を用いて得られるポリテトラフルオロエチレン水性分散液、ポリテトラフルオロエチレンファインパウダー並びに延伸多孔体

Related Child Applications (1)

Application Number Title Priority Date Filing Date
JP2014249831A Division JP5949883B2 (ja) 2009-11-09 2014-12-10 ポリテトラフルオロエチレン水性乳化液及びその製造方法、該水性乳化液を用いて得られるポリテトラフルオロエチレン水性分散液、ポリテトラフルオロエチレンファインパウダー並びに延伸多孔体

Publications (2)

Publication Number Publication Date
JPWO2011055824A1 JPWO2011055824A1 (ja) 2013-03-28
JP5668689B2 true JP5668689B2 (ja) 2015-02-12

Family

ID=43970056

Family Applications (2)

Application Number Title Priority Date Filing Date
JP2011539417A Active JP5668689B2 (ja) 2009-11-09 2010-11-08 ポリテトラフルオロエチレン水性乳化液及びその製造方法、該水性乳化液を用いて得られるポリテトラフルオロエチレン水性分散液、ポリテトラフルオロエチレンファインパウダー並びに延伸多孔体
JP2014249831A Active JP5949883B2 (ja) 2009-11-09 2014-12-10 ポリテトラフルオロエチレン水性乳化液及びその製造方法、該水性乳化液を用いて得られるポリテトラフルオロエチレン水性分散液、ポリテトラフルオロエチレンファインパウダー並びに延伸多孔体

Family Applications After (1)

Application Number Title Priority Date Filing Date
JP2014249831A Active JP5949883B2 (ja) 2009-11-09 2014-12-10 ポリテトラフルオロエチレン水性乳化液及びその製造方法、該水性乳化液を用いて得られるポリテトラフルオロエチレン水性分散液、ポリテトラフルオロエチレンファインパウダー並びに延伸多孔体

Country Status (5)

Country Link
US (1) US9376520B2 (OSRAM)
EP (1) EP2500366B2 (OSRAM)
JP (2) JP5668689B2 (OSRAM)
CN (1) CN102639574B (OSRAM)
WO (1) WO2011055824A1 (OSRAM)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2015045030A (ja) * 2009-11-09 2015-03-12 旭硝子株式会社 ポリテトラフルオロエチレン水性乳化液及びその製造方法、該水性乳化液を用いて得られるポリテトラフルオロエチレン水性分散液、ポリテトラフルオロエチレンファインパウダー並びに延伸多孔体

Families Citing this family (24)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102356095B (zh) 2009-03-30 2015-12-02 大金工业株式会社 聚四氟乙烯及其制造方法
EP2621967B1 (en) * 2010-09-30 2020-08-05 Daikin Industries, Ltd. Process for producing polytetrafluoroethylene fine powder
WO2012043754A1 (ja) 2010-09-30 2012-04-05 ダイキン工業株式会社 ドリップ防止剤、並びに、樹脂組成物
WO2012043757A1 (ja) 2010-09-30 2012-04-05 ダイキン工業株式会社 ポリテトラフルオロエチレンファインパウダーの製造方法
JP6065836B2 (ja) * 2011-08-18 2017-01-25 旭硝子株式会社 界面活性剤水溶液の濃縮回収方法
CN106046219B (zh) * 2011-08-25 2019-07-05 大金工业株式会社 聚四氟乙烯水性分散液的制造方法
EP2810958B1 (en) 2012-02-02 2016-11-30 Asahi Glass Company, Limited Method for producing polytetrafluoroethylene fine powder
TWI543811B (zh) 2012-04-20 2016-08-01 大金工業股份有限公司 以聚四氟乙烯(ptfe)為主成分之組合物、混合粉末、成形用材料及過濾用濾材、空氣過濾單元與多孔膜之製造方法
CN102775617B (zh) * 2012-07-18 2014-12-31 浙江巨圣氟化学有限公司 一种彩色聚四氟乙烯树脂的制备方法
EP2918613B1 (en) * 2012-11-30 2020-06-03 Daikin Industries, Ltd. Production method for polytetrafluoroethylene aqueous dispersion
EP3061512B1 (en) 2013-10-23 2020-12-09 Daikin Industries, Ltd. Embossed filter medium for air filter, filter pack, air filter unit, and production method for embossed filter medium for air filter
CN107922519A (zh) 2015-08-19 2018-04-17 旭硝子株式会社 改性聚四氟乙烯的水性乳化液、细粉及拉伸多孔体的制造方法
EP3348590B1 (en) * 2015-09-08 2020-08-26 AGC Inc. Modified polytetrafluoroethylene fine powder, method for producing same, and method for producing tube or hose
EP3385291B1 (en) * 2015-12-01 2020-08-05 AGC Inc. Method for producing tetrafluoroethylene copolymer aqueous dispersion
JP6673230B2 (ja) 2017-01-12 2020-03-25 ダイキン工業株式会社 エアフィルタ濾材
EP3632939B1 (en) * 2017-06-02 2023-07-26 AGC Inc. Modified polytetrafluoroethylene and method for producing same
CN110709450B (zh) * 2017-07-05 2022-05-17 富士胶片株式会社 构件、容器、药液收容体、药液的纯化装置、制造槽
CN111148770B (zh) * 2017-09-28 2023-01-10 Agc株式会社 改性聚四氟乙烯的制造方法、改性聚四氟乙烯粉末的制造方法、拉伸多孔体的制造方法
CN112552530B (zh) * 2019-09-26 2021-12-03 中昊晨光化工研究院有限公司 一种聚四氟乙烯浓缩分散液及其制备方法
JP7740238B2 (ja) * 2020-06-01 2025-09-17 Agc株式会社 パウダーの製造方法、パウダー及びパウダー分散液
EP4353344A4 (en) 2021-06-04 2024-08-21 Daikin Industries, Ltd. AIR FILTER MEDIA, PLEATED FILTER MEDIA, AIR FILTER UNIT, MASK FILTRATION MEDIA, AND METHOD FOR RECYCLING AIR FILTER MEDIA
TW202419485A (zh) 2022-08-10 2024-05-16 日商大金工業股份有限公司 改質聚四氟乙烯、及延伸體
WO2024075791A1 (ja) 2022-10-07 2024-04-11 ダイキン工業株式会社 誘電体及びその製造方法
CN116813828A (zh) * 2023-04-17 2023-09-29 浙江汉丞新能源有限公司 一种高分子量四氟乙烯共聚分散树脂及其制备方法

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5626242B2 (OSRAM) * 1974-09-09 1981-06-17
JPH11240917A (ja) * 1997-12-26 1999-09-07 Asahi Glass Co Ltd テトラフルオロエチレン系共重合体とその用途
JP2002308914A (ja) * 2001-04-17 2002-10-23 Daikin Ind Ltd 含フッ素重合体ラテックスの製造方法
JP2003119204A (ja) * 2001-10-05 2003-04-23 Daikin Ind Ltd 含フッ素重合体ラテックスの製造方法
WO2007046345A1 (ja) * 2005-10-17 2007-04-26 Asahi Glass Company, Limited ポリテトラフルオロエチレン水性乳化液、それから得られるポリテトラフルオロエチレンファインパウダーおよび多孔体

Family Cites Families (31)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
USRE31907E (en) * 1975-09-24 1985-06-04 E. I. Du Pont De Nemours And Company Tetrafluoroethylene copolymer fine powder resin
US4792594A (en) * 1982-12-13 1988-12-20 E. I. Du Pont De Nemours And Company Tetrafluoroethylene copolymers
US4636549A (en) * 1982-12-13 1987-01-13 E. I. Du Pont De Nemours And Company Tetrafluoroethylene copolymers
US4576869A (en) 1984-06-18 1986-03-18 E. I. Du Pont De Nemours And Company Tetrafluoroethylene fine powder and preparation thereof
US5709944A (en) * 1992-02-05 1998-01-20 Daikin Industries, Ltd. Polytetrafluoroethylene molding powder
JPH07102413A (ja) 1993-09-16 1995-04-18 Japan Gore Tex Inc ポリテトラフルオロエチレン糸状物
JP3453759B2 (ja) * 1995-03-15 2003-10-06 ダイキン工業株式会社 ポリテトラフルオロエチレン成形用粉末の製造方法
US6747108B1 (en) * 1998-07-13 2004-06-08 Daikin Industries, Ltd. Modified polytetrafluoroethylene fine powder and process for preparing the same
DE60135894D1 (de) * 2000-10-30 2008-11-06 Asahi Glass Co Ltd Tetrafluoroethylenpolymer für Dehnung
US7279522B2 (en) * 2001-09-05 2007-10-09 3M Innovative Properties Company Fluoropolymer dispersions containing no or little low molecular weight fluorinated surfactant
JP4207442B2 (ja) 2002-03-20 2009-01-14 旭硝子株式会社 ポリテトラフルオロエチレン水性分散液組成物の製造方法
EP1469104A1 (en) 2003-04-16 2004-10-20 ATOFINA Research Société Anonyme Metallocene produced polyethylene for fibres applications
JP5217090B2 (ja) * 2003-10-22 2013-06-19 ダイキン工業株式会社 テトラフルオロエチレン重合体水性分散液、その製造方法、テトラフルオロエチレン重合体粉末及びテトラフルオロエチレン重合体成形体
JP4951970B2 (ja) 2003-12-22 2012-06-13 ダイキン工業株式会社 非溶融加工性ポリテトラフルオロエチレン及びそのファインパウダー
US7514484B2 (en) * 2005-06-06 2009-04-07 Asahi Glass Company, Limited Aqueous dispersion of polytetrafluoroethylene and process for its production
US7531611B2 (en) * 2005-07-05 2009-05-12 Gore Enterprise Holdings, Inc. Copolymers of tetrafluoroethylene
JP4956925B2 (ja) * 2005-07-13 2012-06-20 旭硝子株式会社 ポリテトラフルオロエチレン水性分散液およびその製造方法
GB0514398D0 (en) * 2005-07-15 2005-08-17 3M Innovative Properties Co Aqueous emulsion polymerization of fluorinated monomers using a fluorinated surfactant
GB0514387D0 (en) 2005-07-15 2005-08-17 3M Innovative Properties Co Aqueous emulsion polymerization of fluorinated monomers using a perfluoropolyether surfactant
JP4792873B2 (ja) * 2005-08-19 2011-10-12 旭硝子株式会社 精製ポリテトラフルオロエチレン水性分散液の製造方法
CN101291987B (zh) * 2005-10-20 2012-05-09 旭硝子株式会社 聚四氟乙烯水性分散液及其制品
EP1939223B1 (en) * 2005-10-20 2011-07-13 Asahi Glass Company, Limited Method for producing melt-moldable fluororesin
JP5343355B2 (ja) * 2005-10-26 2013-11-13 旭硝子株式会社 含フッ素乳化剤の残留量が少ないフッ素樹脂およびその製造方法
JP5588679B2 (ja) 2006-11-09 2014-09-10 イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニー フルオロポリエーテル酸または塩および短鎖フッ素系界面活性剤を含む重合剤を用いるフッ素化モノマーの水性重合
RU2448982C2 (ru) 2007-04-13 2012-04-27 Асахи Гласс Компани, Лимитед Способ получения фторполимера с использованием производного фторкарбоновой кислоты
JP2010229164A (ja) 2007-07-24 2010-10-14 Daikin Ind Ltd フルオロポリマーの製造方法
JP5392251B2 (ja) * 2008-04-14 2014-01-22 旭硝子株式会社 ポリテトラフルオロエチレンファインパウダーの製造方法
JP5139871B2 (ja) 2008-04-17 2013-02-06 三菱電機株式会社 バケット
RU2478653C2 (ru) * 2008-05-21 2013-04-10 Асахи Гласс Компани, Лимитед Способ получения тонкодисперсного порошка политетрафторэтилена
RU2012120435A (ru) * 2009-10-16 2013-11-27 Асахи Гласс Компани, Лимитед Способ получения водной политетрафторэтиленовой дисперсии для процесса коагуляции и водная политетрафторэтиленовая дисперсия для процесса коагуляции
EP2500366B2 (en) * 2009-11-09 2022-03-16 AGC Inc. Aqueous polytetrafluoroethylene emulsion and process for production thereof, aqueous polytetrafluoroethylene dispersion obtained using the emulsion, polytetrafluoroethylene fine powder, and stretch-expanded body

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5626242B2 (OSRAM) * 1974-09-09 1981-06-17
JPH11240917A (ja) * 1997-12-26 1999-09-07 Asahi Glass Co Ltd テトラフルオロエチレン系共重合体とその用途
JP2002308914A (ja) * 2001-04-17 2002-10-23 Daikin Ind Ltd 含フッ素重合体ラテックスの製造方法
JP2003119204A (ja) * 2001-10-05 2003-04-23 Daikin Ind Ltd 含フッ素重合体ラテックスの製造方法
WO2007046345A1 (ja) * 2005-10-17 2007-04-26 Asahi Glass Company, Limited ポリテトラフルオロエチレン水性乳化液、それから得られるポリテトラフルオロエチレンファインパウダーおよび多孔体

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2015045030A (ja) * 2009-11-09 2015-03-12 旭硝子株式会社 ポリテトラフルオロエチレン水性乳化液及びその製造方法、該水性乳化液を用いて得られるポリテトラフルオロエチレン水性分散液、ポリテトラフルオロエチレンファインパウダー並びに延伸多孔体

Also Published As

Publication number Publication date
CN102639574A (zh) 2012-08-15
JP2015045030A (ja) 2015-03-12
EP2500366B1 (en) 2014-01-08
US9376520B2 (en) 2016-06-28
WO2011055824A1 (ja) 2011-05-12
US20120202906A1 (en) 2012-08-09
JPWO2011055824A1 (ja) 2013-03-28
RU2012124022A (ru) 2013-12-20
JP5949883B2 (ja) 2016-07-13
CN102639574B (zh) 2015-11-25
EP2500366A1 (en) 2012-09-19
EP2500366B2 (en) 2022-03-16
EP2500366A4 (en) 2013-04-03

Similar Documents

Publication Publication Date Title
JP5949883B2 (ja) ポリテトラフルオロエチレン水性乳化液及びその製造方法、該水性乳化液を用いて得られるポリテトラフルオロエチレン水性分散液、ポリテトラフルオロエチレンファインパウダー並びに延伸多孔体
US10865257B2 (en) Production methods for aqueous emulsion, fine powder and stretched porous body of modified polytetrafluoroethylene
JP5392251B2 (ja) ポリテトラフルオロエチレンファインパウダーの製造方法
US9580590B2 (en) Method for producing aqueous polytetrafluoroethylene dispersion
JP5732850B2 (ja) ポリテトラフルオロエチレンファインパウダーの製造方法
EP2810958B1 (en) Method for producing polytetrafluoroethylene fine powder
JP2009227754A (ja) 含フッ素共重合体の製造法
RU2575009C2 (ru) Политетрафторэтиленовая водная эмульсия и способ ее получения, политетрафторэтиленовая водная дисперсия, получаемая при использовании такой водной эмульсии, политетрафторэтиленовый тонкодисперсный порошок и растянутый пористый материал
WO2024019010A1 (ja) 変性ポリテトラフルオロエチレン、成形物、延伸多孔体の製造方法

Legal Events

Date Code Title Description
A621 Written request for application examination

Free format text: JAPANESE INTERMEDIATE CODE: A621

Effective date: 20130808

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20140826

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20141020

TRDD Decision of grant or rejection written
A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

Effective date: 20141118

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20141201

R150 Certificate of patent or registration of utility model

Ref document number: 5668689

Country of ref document: JP

Free format text: JAPANESE INTERMEDIATE CODE: R150

S533 Written request for registration of change of name

Free format text: JAPANESE INTERMEDIATE CODE: R313533

R350 Written notification of registration of transfer

Free format text: JAPANESE INTERMEDIATE CODE: R350

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250