JP4427190B2 - 高濃度モノエチレングリコールの製造方法 - Google Patents

高濃度モノエチレングリコールの製造方法 Download PDF

Info

Publication number
JP4427190B2
JP4427190B2 JP2000574053A JP2000574053A JP4427190B2 JP 4427190 B2 JP4427190 B2 JP 4427190B2 JP 2000574053 A JP2000574053 A JP 2000574053A JP 2000574053 A JP2000574053 A JP 2000574053A JP 4427190 B2 JP4427190 B2 JP 4427190B2
Authority
JP
Japan
Prior art keywords
monoethylene glycol
stream
tower
dehydration tower
vacuum
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
JP2000574053A
Other languages
English (en)
Japanese (ja)
Other versions
JP2002526463A (ja
JP2002526463A5 (enExample
Inventor
タイス,ゲールハルト
アドリアン,ティル
ベスリング,ベルント
ハッセ,ハンス
ヴァンザント,フランス
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BASF SE filed Critical BASF SE
Publication of JP2002526463A publication Critical patent/JP2002526463A/ja
Publication of JP2002526463A5 publication Critical patent/JP2002526463A5/ja
Application granted granted Critical
Publication of JP4427190B2 publication Critical patent/JP4427190B2/ja
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Images

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/76Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
    • C07C29/80Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10STECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S203/00Distillation: processes, separatory
    • Y10S203/20Power plant

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
JP2000574053A 1998-09-23 1999-09-21 高濃度モノエチレングリコールの製造方法 Expired - Lifetime JP4427190B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE19843697A DE19843697A1 (de) 1998-09-23 1998-09-23 Verfahren zur Herstellung von hochreinem Monoethylenglykol
DE19843697.1 1998-09-23
PCT/EP1999/006968 WO2000017141A1 (de) 1998-09-23 1999-09-21 Verfahren zur herstellung von hochreinem monoethylenglykol

Publications (3)

Publication Number Publication Date
JP2002526463A JP2002526463A (ja) 2002-08-20
JP2002526463A5 JP2002526463A5 (enExample) 2009-11-19
JP4427190B2 true JP4427190B2 (ja) 2010-03-03

Family

ID=7882020

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2000574053A Expired - Lifetime JP4427190B2 (ja) 1998-09-23 1999-09-21 高濃度モノエチレングリコールの製造方法

Country Status (19)

Country Link
US (1) US6605192B1 (enExample)
EP (1) EP1115682B1 (enExample)
JP (1) JP4427190B2 (enExample)
KR (1) KR100611284B1 (enExample)
CN (1) CN1217898C (enExample)
AR (1) AR020655A1 (enExample)
AT (1) ATE255084T1 (enExample)
AU (1) AU5980199A (enExample)
BR (1) BR9913889B1 (enExample)
CA (1) CA2345053C (enExample)
DE (2) DE19843697A1 (enExample)
ES (1) ES2212671T3 (enExample)
MY (1) MY121383A (enExample)
PL (1) PL195588B1 (enExample)
RU (1) RU2235710C2 (enExample)
SA (1) SA99200783B1 (enExample)
TW (1) TW475925B (enExample)
UA (1) UA60383C2 (enExample)
WO (1) WO2000017141A1 (enExample)

Families Citing this family (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6372925B1 (en) * 2000-06-09 2002-04-16 Shell Oil Company Process for operating the epoxidation of ethylene
US7095741B1 (en) * 2000-12-20 2006-08-22 Cisco Technology, Inc. Port isolation for restricting traffic flow on layer 2 switches
DE10321733A1 (de) * 2003-05-14 2004-12-02 Basf Ag Verfahren zur Herstellung von ameisensauren Formiaten
DE602006012549D1 (de) * 2005-12-29 2010-04-08 Basf Se Verfahren zur trennung von propylenglykol von wässrigen zusammensetzungen
RU2312696C1 (ru) * 2006-03-17 2007-12-20 Андрей Григорьевич Вендило Универсальная установка для очистки высококипящих растворителей вакуумной ректификацией и способы очистки вакуумной ректификацией на ней этиленгликоля, моноэтаноламина, метилцеллозольва, этилцеллозольва, бутилцеллозольва, n-метилпирролидона и бензилового спирта
EP2035359B1 (en) * 2006-06-13 2010-02-24 Shell Internationale Research Maatschappij B.V. Glycol separation and purification
RU2511442C2 (ru) * 2008-10-09 2014-04-10 Шелл Интернэшнл Рисерч Маатсхаппий Б.В. Способ регенерации моноэтиленгликоля
WO2010053900A2 (en) * 2008-11-10 2010-05-14 Dow Technology Investments, Llc Process for producing low color glycols
PL217778B1 (pl) 2011-06-20 2014-08-29 Piotr Medoń Sposób osuszania glikolu i układ do osuszania glikolu
CN103265401B (zh) * 2013-04-24 2014-12-17 河南朝歌日光新能源股份有限公司 一种煤制乙二醇工艺副产残液的回收方法
US9732019B1 (en) * 2016-04-01 2017-08-15 Cameron Solutions, Inc. System and method to remove organic acid from a rich MEG stream by stripping
GB201710508D0 (en) * 2017-06-30 2017-08-16 Johnson Matthey Davy Technologies Ltd Process
WO2019101707A1 (en) * 2017-11-23 2019-05-31 Shell Internationale Research Maatschappij B.V. Processes for the production of ethylene oxide and ethylene glycol
NL2025637B1 (en) * 2020-05-20 2021-12-07 Ioniqa Tech B V A separation method and reactor system for a glycol-water mixture
CN119868990B (zh) * 2025-03-12 2025-10-24 连云港石化有限公司 一种乙二醇预脱水塔装置及其使用方法

Family Cites Families (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2510548A (en) * 1947-06-20 1950-06-06 Lummus Co Multiple-effect distillation
DE1942094A1 (de) 1968-08-22 1970-02-26 Union Carbide Corp Verfahren zur Reinigung von verunreinigten Glykolen
IT972794B (it) 1972-12-22 1974-05-31 Sir Soc Italiana Resine Spa Procedimento perfezionato per la produzione del glicole etilenico
US4182659A (en) * 1977-10-31 1980-01-08 Davy International Aktiengesellschaft Method of concentrating a water-containing glycol
DE3001727A1 (de) 1980-01-18 1981-07-23 Hoechst Ag, 6000 Frankfurt Verfahren zur herstellung von hochreinem monoethylenglykol
DE3338488A1 (de) 1982-10-29 1984-05-03 Basf Ag, 6700 Ludwigshafen Verfahren zur gewinnung von temperaturempfindlichen produkten durch thermisch schonende destillation mittels eines mit einer destillationskolonne verbundenen duennschichtverdampfers und eine anordnung zur durchfuehrung des verfahrens
JPS6089439A (ja) 1983-10-24 1985-05-20 Mitsui Toatsu Chem Inc エチレングリコ−ルの製造方法
FR2564458B1 (fr) 1984-05-15 1986-09-12 Atochem Procede de separation de l'ethyleneglycol sous forme concentree dans un procede de fabrication d'oxyde d'ethylene
DE4306144A1 (de) * 1993-02-27 1994-09-01 Brown John Deutsche Eng Gmbh Verfahren und Polykondensationsanlage zur Aufbereitung von verunreinigtem Ethylenglykol
DE19602116A1 (de) 1996-01-22 1997-07-24 Basf Ag Verfahren zur Gewinnung von Glykolen mit niedrigem Aldehydgehalt
RU2111949C1 (ru) * 1996-08-19 1998-05-27 Акционерное общество "Нижнекамскнефтехим" Способ извлечения моно- и диэтиленгликолей из кубового остатка процесса выделения моноэтиленгликоля
US5738417A (en) * 1997-01-29 1998-04-14 Westinghouse Air Brake Company Brake pipe sensing unit

Also Published As

Publication number Publication date
DE19843697A1 (de) 2000-03-30
BR9913889B1 (pt) 2011-01-11
EP1115682B1 (de) 2003-11-26
AR020655A1 (es) 2002-05-22
JP2002526463A (ja) 2002-08-20
WO2000017141A1 (de) 2000-03-30
KR100611284B1 (ko) 2006-08-10
CA2345053C (en) 2008-07-15
TW475925B (en) 2002-02-11
AU5980199A (en) 2000-04-10
MY121383A (en) 2006-01-28
RU2235710C2 (ru) 2004-09-10
CN1217898C (zh) 2005-09-07
CN1319080A (zh) 2001-10-24
CA2345053A1 (en) 2000-03-30
EP1115682A1 (de) 2001-07-18
UA60383C2 (uk) 2003-10-15
ES2212671T3 (es) 2004-07-16
ATE255084T1 (de) 2003-12-15
DE59907884D1 (de) 2004-01-08
PL195588B1 (pl) 2007-10-31
PL347580A1 (en) 2002-04-08
SA99200783B1 (ar) 2006-08-12
BR9913889A (pt) 2001-07-03
US6605192B1 (en) 2003-08-12
KR20010075276A (ko) 2001-08-09

Similar Documents

Publication Publication Date Title
JP4427189B2 (ja) 高濃度モノエチレングリコールの製造方法
JP4427190B2 (ja) 高濃度モノエチレングリコールの製造方法
JP3712903B2 (ja) グリセリンの製造方法
US5426221A (en) Separation of acrylic acid from the reaction gases from the catalytic oxidation of propylene and/or acrolein
CN112566706A (zh) 回收环氧乙烷的方法
JP2002526462A5 (enExample)
WO1996016953A1 (en) Improved process for recovering ethylene oxide
JP2002526463A5 (enExample)
JP2004504293A (ja) 改良されたアセトニトリルの精製及び回収方法
EP1888194B1 (en) New stripper configuration for the production of ethylene oxide
US6437199B1 (en) Method for production of high-purity monoethylene glycol
JP5101710B2 (ja) エチレングリコールの精製方法
JP4740432B2 (ja) エチレングリコールの精製方法
US4966657A (en) Process for separating ethylene oxide from aldehyde impurities by distillation
KR20000005874A (ko) 원액비닐아세테이트의후처리방법
JPS6075478A (ja) 市販のホルムアルデヒド水溶液からトリオキサンを製造する方法及び装置
JP2001031600A (ja) 高純度モノエチレングリコールの製法
KR100584677B1 (ko) 고효율의 아크릴산 제조 방법
GB2045759A (en) Process for recovering methacrylic acid
JP3957297B2 (ja) アクリル酸の製造方法
US11724976B2 (en) Ethylene oxide purification
JPS6331458B2 (enExample)
MXPA01002968A (en) Method for producing highly pure monoethylene glycol
MXPA01002578A (en) Method for producing highly pure monoethylene glycol
JPS5955846A (ja) エチレングリコ−ルからのグリオキサ−ルの製造方法

Legal Events

Date Code Title Description
A621 Written request for application examination

Free format text: JAPANESE INTERMEDIATE CODE: A621

Effective date: 20060720

A977 Report on retrieval

Free format text: JAPANESE INTERMEDIATE CODE: A971007

Effective date: 20090212

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20090331

A601 Written request for extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A601

Effective date: 20090625

A602 Written permission of extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A602

Effective date: 20090702

A601 Written request for extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A601

Effective date: 20090724

A602 Written permission of extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A602

Effective date: 20090731

A601 Written request for extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A601

Effective date: 20090826

A602 Written permission of extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A602

Effective date: 20090902

A524 Written submission of copy of amendment under article 19 pct

Free format text: JAPANESE INTERMEDIATE CODE: A524

Effective date: 20090929

TRDD Decision of grant or rejection written
A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

Effective date: 20091116

A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20091214

R150 Certificate of patent or registration of utility model

Ref document number: 4427190

Country of ref document: JP

Free format text: JAPANESE INTERMEDIATE CODE: R150

Free format text: JAPANESE INTERMEDIATE CODE: R150

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20121218

Year of fee payment: 3

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20121218

Year of fee payment: 3

FPAY Renewal fee payment (event date is renewal date of database)

Free format text: PAYMENT UNTIL: 20131218

Year of fee payment: 4

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

EXPY Cancellation because of completion of term