JP4357379B2 - インクジェット記録媒体の製造方法 - Google Patents
インクジェット記録媒体の製造方法 Download PDFInfo
- Publication number
- JP4357379B2 JP4357379B2 JP2004201492A JP2004201492A JP4357379B2 JP 4357379 B2 JP4357379 B2 JP 4357379B2 JP 2004201492 A JP2004201492 A JP 2004201492A JP 2004201492 A JP2004201492 A JP 2004201492A JP 4357379 B2 JP4357379 B2 JP 4357379B2
- Authority
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- Japan
- Prior art keywords
- inorganic fine
- fine particle
- coating
- particle layer
- silica
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 238000000034 method Methods 0.000 title claims abstract description 50
- 238000004519 manufacturing process Methods 0.000 title claims description 10
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 176
- 239000010419 fine particle Substances 0.000 claims abstract description 114
- 238000000576 coating method Methods 0.000 claims abstract description 113
- 239000011248 coating agent Substances 0.000 claims abstract description 105
- 239000000377 silicon dioxide Substances 0.000 claims abstract description 70
- 239000011163 secondary particle Substances 0.000 claims abstract description 10
- 239000007787 solid Substances 0.000 claims abstract description 7
- 239000007788 liquid Substances 0.000 claims description 49
- 239000008119 colloidal silica Substances 0.000 claims description 25
- 239000011800 void material Substances 0.000 claims description 23
- 238000005303 weighing Methods 0.000 claims description 6
- 239000000463 material Substances 0.000 abstract description 4
- 239000010410 layer Substances 0.000 description 152
- 239000000243 solution Substances 0.000 description 43
- 239000002609 medium Substances 0.000 description 28
- 239000000203 mixture Substances 0.000 description 26
- 238000009472 formulation Methods 0.000 description 22
- 239000000123 paper Substances 0.000 description 22
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 21
- 239000011164 primary particle Substances 0.000 description 20
- 230000000052 comparative effect Effects 0.000 description 19
- 239000006185 dispersion Substances 0.000 description 17
- 229920005989 resin Polymers 0.000 description 15
- 239000011347 resin Substances 0.000 description 15
- 235000012239 silicon dioxide Nutrition 0.000 description 15
- 239000002245 particle Substances 0.000 description 13
- 239000002002 slurry Substances 0.000 description 13
- 238000010521 absorption reaction Methods 0.000 description 12
- 239000011230 binding agent Substances 0.000 description 12
- 239000000126 substance Substances 0.000 description 12
- 239000008199 coating composition Substances 0.000 description 11
- 238000001035 drying Methods 0.000 description 11
- -1 polydiallylamine Polymers 0.000 description 11
- 239000007789 gas Substances 0.000 description 9
- 239000012071 phase Substances 0.000 description 8
- 239000012808 vapor phase Substances 0.000 description 8
- 239000007864 aqueous solution Substances 0.000 description 7
- 239000011324 bead Substances 0.000 description 7
- 150000001875 compounds Chemical class 0.000 description 7
- 230000008569 process Effects 0.000 description 7
- 229920006317 cationic polymer Polymers 0.000 description 6
- 229920002451 polyvinyl alcohol Polymers 0.000 description 6
- 235000019422 polyvinyl alcohol Nutrition 0.000 description 6
- 239000004372 Polyvinyl alcohol Substances 0.000 description 5
- 238000001179 sorption measurement Methods 0.000 description 5
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 4
- 239000003513 alkali Substances 0.000 description 4
- 229910052782 aluminium Inorganic materials 0.000 description 4
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 4
- 150000001767 cationic compounds Chemical class 0.000 description 4
- 238000003851 corona treatment Methods 0.000 description 4
- 238000001125 extrusion Methods 0.000 description 4
- 239000010408 film Substances 0.000 description 4
- 229920005672 polyolefin resin Polymers 0.000 description 4
- 238000010298 pulverizing process Methods 0.000 description 4
- VXEGSRKPIUDPQT-UHFFFAOYSA-N 4-[4-(4-methoxyphenyl)piperazin-1-yl]aniline Chemical compound C1=CC(OC)=CC=C1N1CCN(C=2C=CC(N)=CC=2)CC1 VXEGSRKPIUDPQT-UHFFFAOYSA-N 0.000 description 3
- 239000004115 Sodium Silicate Substances 0.000 description 3
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 3
- QCWXUUIWCKQGHC-UHFFFAOYSA-N Zirconium Chemical compound [Zr] QCWXUUIWCKQGHC-UHFFFAOYSA-N 0.000 description 3
- 239000002585 base Substances 0.000 description 3
- 239000003795 chemical substances by application Substances 0.000 description 3
- 230000003247 decreasing effect Effects 0.000 description 3
- 239000000499 gel Substances 0.000 description 3
- 229920001684 low density polyethylene Polymers 0.000 description 3
- 239000004702 low-density polyethylene Substances 0.000 description 3
- 150000002736 metal compounds Chemical class 0.000 description 3
- 229920000642 polymer Polymers 0.000 description 3
- 239000011148 porous material Substances 0.000 description 3
- 239000005049 silicon tetrachloride Substances 0.000 description 3
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 description 3
- 229910052911 sodium silicate Inorganic materials 0.000 description 3
- 238000003756 stirring Methods 0.000 description 3
- 239000004094 surface-active agent Substances 0.000 description 3
- 229920003002 synthetic resin Polymers 0.000 description 3
- 239000000057 synthetic resin Substances 0.000 description 3
- 229910052719 titanium Inorganic materials 0.000 description 3
- 239000010936 titanium Substances 0.000 description 3
- 229910052726 zirconium Inorganic materials 0.000 description 3
- XJUNLJFOHNHSAR-UHFFFAOYSA-J zirconium(4+);dicarbonate Chemical compound [Zr+4].[O-]C([O-])=O.[O-]C([O-])=O XJUNLJFOHNHSAR-UHFFFAOYSA-J 0.000 description 3
- XFSMEWPSXDHRNU-UHFFFAOYSA-N 4-(2-ethylhexoxy)-4-oxo-3-sulfobutanoic acid Chemical class CCCCC(CC)COC(=O)C(S(O)(=O)=O)CC(O)=O XFSMEWPSXDHRNU-UHFFFAOYSA-N 0.000 description 2
- 229920000178 Acrylic resin Polymers 0.000 description 2
- 239000004925 Acrylic resin Substances 0.000 description 2
- 229910002012 Aerosil® Inorganic materials 0.000 description 2
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonia chloride Chemical compound [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 description 2
- 238000004438 BET method Methods 0.000 description 2
- 108010010803 Gelatin Proteins 0.000 description 2
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 2
- 230000009471 action Effects 0.000 description 2
- 239000000654 additive Substances 0.000 description 2
- 230000032683 aging Effects 0.000 description 2
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 2
- VSCWAEJMTAWNJL-UHFFFAOYSA-K aluminium trichloride Chemical compound Cl[Al](Cl)Cl VSCWAEJMTAWNJL-UHFFFAOYSA-K 0.000 description 2
- 239000002216 antistatic agent Substances 0.000 description 2
- 230000008859 change Effects 0.000 description 2
- 230000006866 deterioration Effects 0.000 description 2
- 208000028659 discharge Diseases 0.000 description 2
- 239000008273 gelatin Substances 0.000 description 2
- 229920000159 gelatin Polymers 0.000 description 2
- 235000019322 gelatine Nutrition 0.000 description 2
- 235000011852 gelatine desserts Nutrition 0.000 description 2
- 230000006872 improvement Effects 0.000 description 2
- 238000005342 ion exchange Methods 0.000 description 2
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 description 2
- 239000012669 liquid formulation Substances 0.000 description 2
- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 2
- 229910052753 mercury Inorganic materials 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 229910044991 metal oxide Inorganic materials 0.000 description 2
- 150000004706 metal oxides Chemical class 0.000 description 2
- 229920005615 natural polymer Polymers 0.000 description 2
- 239000003921 oil Substances 0.000 description 2
- 230000000737 periodic effect Effects 0.000 description 2
- 238000006116 polymerization reaction Methods 0.000 description 2
- 239000004576 sand Substances 0.000 description 2
- 238000007127 saponification reaction Methods 0.000 description 2
- RMAQACBXLXPBSY-UHFFFAOYSA-N silicic acid Chemical compound O[Si](O)(O)O RMAQACBXLXPBSY-UHFFFAOYSA-N 0.000 description 2
- 239000010409 thin film Substances 0.000 description 2
- OERNJTNJEZOPIA-UHFFFAOYSA-N zirconium nitrate Chemical compound [Zr+4].[O-][N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O.[O-][N+]([O-])=O OERNJTNJEZOPIA-UHFFFAOYSA-N 0.000 description 2
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 description 1
- IVORCBKUUYGUOL-UHFFFAOYSA-N 1-ethynyl-2,4-dimethoxybenzene Chemical compound COC1=CC=C(C#C)C(OC)=C1 IVORCBKUUYGUOL-UHFFFAOYSA-N 0.000 description 1
- OEPOKWHJYJXUGD-UHFFFAOYSA-N 2-(3-phenylmethoxyphenyl)-1,3-thiazole-4-carbaldehyde Chemical compound O=CC1=CSC(C=2C=C(OCC=3C=CC=CC=3)C=CC=2)=N1 OEPOKWHJYJXUGD-UHFFFAOYSA-N 0.000 description 1
- LYPJRFIBDHNQLY-UHFFFAOYSA-J 2-hydroxypropanoate;zirconium(4+) Chemical compound [Zr+4].CC(O)C([O-])=O.CC(O)C([O-])=O.CC(O)C([O-])=O.CC(O)C([O-])=O LYPJRFIBDHNQLY-UHFFFAOYSA-J 0.000 description 1
- DUFCMRCMPHIFTR-UHFFFAOYSA-N 5-(dimethylsulfamoyl)-2-methylfuran-3-carboxylic acid Chemical compound CN(C)S(=O)(=O)C1=CC(C(O)=O)=C(C)O1 DUFCMRCMPHIFTR-UHFFFAOYSA-N 0.000 description 1
- 229910018072 Al 2 O 3 Inorganic materials 0.000 description 1
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 1
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 1
- 229920002134 Carboxymethyl cellulose Polymers 0.000 description 1
- 229920000298 Cellophane Polymers 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 1
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 description 1
- 239000004971 Cross linker Substances 0.000 description 1
- 229920001353 Dextrin Polymers 0.000 description 1
- 239000004375 Dextrin Substances 0.000 description 1
- BRLQWZUYTZBJKN-UHFFFAOYSA-N Epichlorohydrin Chemical compound ClCC1CO1 BRLQWZUYTZBJKN-UHFFFAOYSA-N 0.000 description 1
- 239000004593 Epoxy Substances 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- 239000004594 Masterbatch (MB) Substances 0.000 description 1
- 229920000881 Modified starch Polymers 0.000 description 1
- 239000004368 Modified starch Substances 0.000 description 1
- 239000004952 Polyamide Substances 0.000 description 1
- 239000004698 Polyethylene Substances 0.000 description 1
- 239000002202 Polyethylene glycol Substances 0.000 description 1
- 229920002873 Polyethylenimine Polymers 0.000 description 1
- 239000004743 Polypropylene Substances 0.000 description 1
- 239000004793 Polystyrene Substances 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical group [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 1
- 229920002472 Starch Polymers 0.000 description 1
- XTXRWKRVRITETP-UHFFFAOYSA-N Vinyl acetate Chemical compound CC(=O)OC=C XTXRWKRVRITETP-UHFFFAOYSA-N 0.000 description 1
- BZHJMEDXRYGGRV-UHFFFAOYSA-N Vinyl chloride Chemical compound ClC=C BZHJMEDXRYGGRV-UHFFFAOYSA-N 0.000 description 1
- JSIVLBGUDVQDHZ-UHFFFAOYSA-J [Cl-].[Cl-].[Cl-].O[Zr+3] Chemical compound [Cl-].[Cl-].[Cl-].O[Zr+3] JSIVLBGUDVQDHZ-UHFFFAOYSA-J 0.000 description 1
- 230000002159 abnormal effect Effects 0.000 description 1
- 230000005856 abnormality Effects 0.000 description 1
- 239000002250 absorbent Substances 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 239000012190 activator Substances 0.000 description 1
- 238000005054 agglomeration Methods 0.000 description 1
- 230000002776 aggregation Effects 0.000 description 1
- 150000003973 alkyl amines Chemical class 0.000 description 1
- 229940037003 alum Drugs 0.000 description 1
- AZDRQVAHHNSJOQ-UHFFFAOYSA-N alumane Chemical group [AlH3] AZDRQVAHHNSJOQ-UHFFFAOYSA-N 0.000 description 1
- 235000011124 aluminium ammonium sulphate Nutrition 0.000 description 1
- DIZPMCHEQGEION-UHFFFAOYSA-H aluminium sulfate (anhydrous) Chemical compound [Al+3].[Al+3].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O DIZPMCHEQGEION-UHFFFAOYSA-H 0.000 description 1
- LCQXXBOSCBRNNT-UHFFFAOYSA-K ammonium aluminium sulfate Chemical compound [NH4+].[Al+3].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O LCQXXBOSCBRNNT-UHFFFAOYSA-K 0.000 description 1
- 235000019270 ammonium chloride Nutrition 0.000 description 1
- 150000001450 anions Chemical group 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 230000003078 antioxidant effect Effects 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- 239000012736 aqueous medium Substances 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 238000007611 bar coating method Methods 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- KGBXLFKZBHKPEV-UHFFFAOYSA-N boric acid Chemical compound OB(O)O KGBXLFKZBHKPEV-UHFFFAOYSA-N 0.000 description 1
- 239000004327 boric acid Substances 0.000 description 1
- 235000010948 carboxy methyl cellulose Nutrition 0.000 description 1
- 239000001768 carboxy methyl cellulose Substances 0.000 description 1
- 239000008112 carboxymethyl-cellulose Substances 0.000 description 1
- 239000005018 casein Substances 0.000 description 1
- BECPQYXYKAMYBN-UHFFFAOYSA-N casein, tech. Chemical compound NCCCCC(C(O)=O)N=C(O)C(CC(O)=O)N=C(O)C(CCC(O)=N)N=C(O)C(CC(C)C)N=C(O)C(CCC(O)=O)N=C(O)C(CC(O)=O)N=C(O)C(CCC(O)=O)N=C(O)C(C(C)O)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=N)N=C(O)C(CCC(O)=O)N=C(O)C(CCC(O)=O)N=C(O)C(COP(O)(O)=O)N=C(O)C(CCC(O)=N)N=C(O)C(N)CC1=CC=CC=C1 BECPQYXYKAMYBN-UHFFFAOYSA-N 0.000 description 1
- 235000021240 caseins Nutrition 0.000 description 1
- 125000002091 cationic group Chemical group 0.000 description 1
- 229910052804 chromium Inorganic materials 0.000 description 1
- 239000011651 chromium Substances 0.000 description 1
- 239000011247 coating layer Substances 0.000 description 1
- 239000000084 colloidal system Substances 0.000 description 1
- 238000005336 cracking Methods 0.000 description 1
- 230000001186 cumulative effect Effects 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 235000019425 dextrin Nutrition 0.000 description 1
- 239000000539 dimer Substances 0.000 description 1
- 229910001873 dinitrogen Inorganic materials 0.000 description 1
- 239000002612 dispersion medium Substances 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000011121 hardwood Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 229920001903 high density polyethylene Polymers 0.000 description 1
- 239000004700 high-density polyethylene Substances 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 description 1
- 239000003112 inhibitor Substances 0.000 description 1
- 230000005764 inhibitory process Effects 0.000 description 1
- 229910017053 inorganic salt Inorganic materials 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 239000003456 ion exchange resin Substances 0.000 description 1
- 229920003303 ion-exchange polymer Polymers 0.000 description 1
- 238000004898 kneading Methods 0.000 description 1
- 239000002655 kraft paper Substances 0.000 description 1
- FPYJFEHAWHCUMM-UHFFFAOYSA-N maleic anhydride Chemical compound O=C1OC(=O)C=C1 FPYJFEHAWHCUMM-UHFFFAOYSA-N 0.000 description 1
- 239000006224 matting agent Substances 0.000 description 1
- 238000000691 measurement method Methods 0.000 description 1
- 238000010299 mechanically pulverizing process Methods 0.000 description 1
- 238000005649 metathesis reaction Methods 0.000 description 1
- 239000005055 methyl trichlorosilane Substances 0.000 description 1
- JLUFWMXJHAVVNN-UHFFFAOYSA-N methyltrichlorosilane Chemical compound C[Si](Cl)(Cl)Cl JLUFWMXJHAVVNN-UHFFFAOYSA-N 0.000 description 1
- 239000011859 microparticle Substances 0.000 description 1
- 238000002156 mixing Methods 0.000 description 1
- DYUWTXWIYMHBQS-UHFFFAOYSA-N n-prop-2-enylprop-2-en-1-amine Chemical class C=CCNCC=C DYUWTXWIYMHBQS-UHFFFAOYSA-N 0.000 description 1
- 230000003287 optical effect Effects 0.000 description 1
- CMOAHYOGLLEOGO-UHFFFAOYSA-N oxozirconium;dihydrochloride Chemical compound Cl.Cl.[Zr]=O CMOAHYOGLLEOGO-UHFFFAOYSA-N 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- DCKVFVYPWDKYDN-UHFFFAOYSA-L oxygen(2-);titanium(4+);sulfate Chemical compound [O-2].[Ti+4].[O-]S([O-])(=O)=O DCKVFVYPWDKYDN-UHFFFAOYSA-L 0.000 description 1
- 239000003002 pH adjusting agent Substances 0.000 description 1
- 238000004806 packaging method and process Methods 0.000 description 1
- 230000035699 permeability Effects 0.000 description 1
- 230000010363 phase shift Effects 0.000 description 1
- 239000000049 pigment Substances 0.000 description 1
- 238000009832 plasma treatment Methods 0.000 description 1
- 229920000083 poly(allylamine) Polymers 0.000 description 1
- 229920003207 poly(ethylene-2,6-naphthalate) Polymers 0.000 description 1
- 229920002401 polyacrylamide Polymers 0.000 description 1
- 229920002647 polyamide Polymers 0.000 description 1
- 229920006122 polyamide resin Polymers 0.000 description 1
- 229920000768 polyamine Polymers 0.000 description 1
- 229920001225 polyester resin Polymers 0.000 description 1
- 239000004645 polyester resin Substances 0.000 description 1
- 229920000573 polyethylene Polymers 0.000 description 1
- 229920001223 polyethylene glycol Polymers 0.000 description 1
- 239000011112 polyethylene naphthalate Substances 0.000 description 1
- 229920000139 polyethylene terephthalate Polymers 0.000 description 1
- 239000005020 polyethylene terephthalate Substances 0.000 description 1
- 229920001155 polypropylene Polymers 0.000 description 1
- 229920002223 polystyrene Polymers 0.000 description 1
- 229920005749 polyurethane resin Polymers 0.000 description 1
- 229920000915 polyvinyl chloride Polymers 0.000 description 1
- 239000004800 polyvinyl chloride Substances 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 230000002265 prevention Effects 0.000 description 1
- 125000001453 quaternary ammonium group Chemical group 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 230000005070 ripening Effects 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 238000007493 shaping process Methods 0.000 description 1
- 150000004756 silanes Chemical class 0.000 description 1
- 238000004513 sizing Methods 0.000 description 1
- 238000003980 solgel method Methods 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 238000003892 spreading Methods 0.000 description 1
- 230000007480 spreading Effects 0.000 description 1
- 235000019698 starch Nutrition 0.000 description 1
- 239000008107 starch Substances 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- 238000004381 surface treatment Methods 0.000 description 1
- 230000002522 swelling effect Effects 0.000 description 1
- 125000001302 tertiary amino group Chemical group 0.000 description 1
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 1
- 229910000348 titanium sulfate Inorganic materials 0.000 description 1
- XJDNKRIXUMDJCW-UHFFFAOYSA-J titanium tetrachloride Chemical compound Cl[Ti](Cl)(Cl)Cl XJDNKRIXUMDJCW-UHFFFAOYSA-J 0.000 description 1
- ILJSQTXMGCGYMG-UHFFFAOYSA-N triacetic acid Chemical compound CC(=O)CC(=O)CC(O)=O ILJSQTXMGCGYMG-UHFFFAOYSA-N 0.000 description 1
- ZDHXKXAHOVTTAH-UHFFFAOYSA-N trichlorosilane Chemical compound Cl[SiH](Cl)Cl ZDHXKXAHOVTTAH-UHFFFAOYSA-N 0.000 description 1
- 239000005052 trichlorosilane Substances 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 239000003021 water soluble solvent Substances 0.000 description 1
- 238000010947 wet-dispersion method Methods 0.000 description 1
- XOOUIPVCVHRTMJ-UHFFFAOYSA-L zinc stearate Chemical compound [Zn+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O XOOUIPVCVHRTMJ-UHFFFAOYSA-L 0.000 description 1
- DUNKXUFBGCUVQW-UHFFFAOYSA-J zirconium tetrachloride Chemical compound Cl[Zr](Cl)(Cl)Cl DUNKXUFBGCUVQW-UHFFFAOYSA-J 0.000 description 1
- OMQSJNWFFJOIMO-UHFFFAOYSA-J zirconium tetrafluoride Chemical class F[Zr](F)(F)F OMQSJNWFFJOIMO-UHFFFAOYSA-J 0.000 description 1
- ZXAUZSQITFJWPS-UHFFFAOYSA-J zirconium(4+);disulfate Chemical compound [Zr+4].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O ZXAUZSQITFJWPS-UHFFFAOYSA-J 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B41—PRINTING; LINING MACHINES; TYPEWRITERS; STAMPS
- B41M—PRINTING, DUPLICATING, MARKING, OR COPYING PROCESSES; COLOUR PRINTING
- B41M5/00—Duplicating or marking methods; Sheet materials for use therein
- B41M5/50—Recording sheets characterised by the coating used to improve ink, dye or pigment receptivity, e.g. for ink-jet or thermal dye transfer recording
- B41M5/52—Macromolecular coatings
- B41M5/5218—Macromolecular coatings characterised by inorganic additives, e.g. pigments, clays
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B41—PRINTING; LINING MACHINES; TYPEWRITERS; STAMPS
- B41M—PRINTING, DUPLICATING, MARKING, OR COPYING PROCESSES; COLOUR PRINTING
- B41M5/00—Duplicating or marking methods; Sheet materials for use therein
- B41M5/50—Recording sheets characterised by the coating used to improve ink, dye or pigment receptivity, e.g. for ink-jet or thermal dye transfer recording
- B41M5/502—Recording sheets characterised by the coating used to improve ink, dye or pigment receptivity, e.g. for ink-jet or thermal dye transfer recording characterised by structural details, e.g. multilayer materials
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B41—PRINTING; LINING MACHINES; TYPEWRITERS; STAMPS
- B41M—PRINTING, DUPLICATING, MARKING, OR COPYING PROCESSES; COLOUR PRINTING
- B41M5/00—Duplicating or marking methods; Sheet materials for use therein
- B41M5/50—Recording sheets characterised by the coating used to improve ink, dye or pigment receptivity, e.g. for ink-jet or thermal dye transfer recording
- B41M5/502—Recording sheets characterised by the coating used to improve ink, dye or pigment receptivity, e.g. for ink-jet or thermal dye transfer recording characterised by structural details, e.g. multilayer materials
- B41M5/506—Intermediate layers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B41—PRINTING; LINING MACHINES; TYPEWRITERS; STAMPS
- B41M—PRINTING, DUPLICATING, MARKING, OR COPYING PROCESSES; COLOUR PRINTING
- B41M5/00—Duplicating or marking methods; Sheet materials for use therein
- B41M5/50—Recording sheets characterised by the coating used to improve ink, dye or pigment receptivity, e.g. for ink-jet or thermal dye transfer recording
- B41M5/502—Recording sheets characterised by the coating used to improve ink, dye or pigment receptivity, e.g. for ink-jet or thermal dye transfer recording characterised by structural details, e.g. multilayer materials
- B41M5/508—Supports
Landscapes
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Ink Jet Recording Methods And Recording Media Thereof (AREA)
- Ink Jet (AREA)
- Application Of Or Painting With Fluid Materials (AREA)
Description
[Al(OH)3]nAlCl3 一般式2
Aln(OH)mCl(3n-m) 0<m<3n 一般式3
低密度ポリエチレン 30部
(密度0.920g/cm3)
高密度ポリエチレン 70部
(密度0.967g/cm3)
<表樹脂配合>
マスターバッチ 15部
(密度0.918g/cm3の低密度ポリエチレン39.1部、Al2O3換算0.8質量%の表面被覆アナタ−ゼ型酸化チタン60部、ステアリン酸亜鉛0.9部をバンバリーミキサーで混練)
低密度ポリエチレン 85部
(密度0.920g/cm3)
<バックコート塗液配合>
無水マレイン酸重合体のアルカリ加水分解物25%液 4部
コロイド状シリカ20%スラリー
(日産化学工業(株)製スノーテックス20) 20部
エポキシタイプ架橋剤10%液 1.5部
スルフォコハク酸−2−エチルヘキシルエステル塩5%液 0.5部
水にて全量を100部とした。
<下引き液配合>
石灰処理ゼラチン2%水溶液 50部
スルフォコハク酸−2−エチルヘキシルエステル塩5%液 0.5部
クロム明ばん5%水溶液 2部
水にて全量を100部とした。
<多孔質層塗布液配合1>
気相法シリカ20%スラリー 70部
(平均一次粒径12nm)
ポリジメチルアリルアンモニウムクロライド10%水溶液 2.8部
硼酸10%水溶液 4.2部
ポリビルアルコール10%水溶液 21部
(鹸化度88%、平均重合度3500)
界面活性剤5%水溶液 0.84部
水にて全量を100部とした。
<無機微粒子層塗布液配合1>
コロイド状シリカ20%スラリー 8部
(日産化学工業(株)製スノーテックスO;平均一次粒径15nm)
水にて全量を100部とした。(シリカ濃度1.6質量%)
粘度は1.3mPa・sであった。
(算定厚み187nm:湿分塗布量(19ml/m2)×塗布液濃度(0.016)÷二酸化珪素の密度(2.2g/cm3)÷0.74)
<無機微粒子層塗布液配合2>
コロイド状シリカ20%スラリー 6部
(日産化学工業(株)製スノーテックスO;平均一次粒径15nm)
水にて全量を100部とした。(シリカ濃度1.2質量%)
粘度は1.3mPa・sであった。
(算定厚み140nm:湿分塗布量(19ml/m2)×塗布液濃度(0.012)÷二酸化珪素の密度(2.2g/cm3)÷0.74)
<無機微粒子層塗布液配合3>
コロイド状シリカ20%スラリー 4部
(日産化学工業(株)製スノーテックスO;平均一次粒径15nm)
水にて全量を100部とした。(シリカ濃度0.8質量%)
粘度は1.3mPa・sであった。
(算定厚み93nm:湿分塗布量(19ml/m2)×塗布液濃度(0.008)÷二酸化珪素の密度(2.2g/cm3)÷0.74)
実施例1の無機微粒子層塗布液配合を無機微粒子層塗布液配合4に代える以外は同様にして比較例1のインクジェット記録媒体を得た。
<無機微粒子層塗布液配合4>
コロイド状シリカ20%スラリー 20部
(日産化学工業(株)製スノーテックスO;平均一次粒径15nm)
水にて全量を100部とした。(シリカ濃度4.0質量%)
粘度は1.3mPa・sであった。
(算定厚み477nm:湿分塗布量(19ml/m2)×塗布液濃度(0.04)÷二酸化珪素の密度(2.2g/cm3)÷0.74)
実施例3に於いて無機微粒子層塗布液の塗布量を30ml/m2にする以外は同様にして比較例2のインクジェット記録媒体を得た。
(算定厚み147nm:湿分塗布量(30ml/m2)×塗布液濃度(0.008)÷二酸化珪素の密度(2.2g/cm3)÷0.74)
(算定厚み147nm:湿分塗布量(20ml/m2)×塗布液濃度(0.012)÷二酸化珪素の密度(2.2g/cm3)÷0.74)
(算定厚み98nm:湿分塗布量(20ml/m2)×塗布液濃度(0.008)÷二酸化珪素の密度(2.2g/cm3)÷0.74)
実施例4の無機微粒子層塗布液配合を無機微粒子層塗布液配合4に代える以外は同様にして比較例3のインクジェット記録媒体を得た。
(算定厚み502nm:湿分塗布量(20ml/m2)×塗布液濃度(0.04)÷二酸化珪素の密度(2.2g/cm3)÷0.74)
<無機微粒子層塗布液配合5>
コロイド状シリカ20%スラリー 6部
(扶桑化学工業製クォートロンPL−3L、平均一次粒径35nm)
水にて全量を100部とした。(シリカ濃度1.2質量%)
粘度は1.3mPa・sであった。
(算定厚み147nm:湿分塗布量(20ml/m2)×塗布液濃度(0.012)÷二酸化珪素の密度(2.2g/cm3)÷0.74)
<無機微粒子層塗布液配合6>
コロイド状シリカ20%スラリー 4部
(扶桑化学工業製クォートロンPL−3L、平均一次粒径35nm)
水にて全量を100部とした。(シリカ濃度0.8質量%)
粘度は1.3mPa・sであった。
(算定厚み98nm:湿分塗布量(20ml/m2)×塗布液濃度(0.008)÷二酸化珪素の密度(2.2g/cm3)÷0.74)
実施例4の無機微粒子層塗布液配合を無機微粒子層塗布液配合7に代える以外は同様にして比較例4のインクジェット記録媒体を得た。
<無機微粒子層塗布液配合7>
コロイド状シリカ20%スラリー 20部
(日産化学工業(株)製スノーテックスO;平均一次粒径15nm)
水にて全量を100部とした。(シリカ濃度4.0質量%)
(算定厚み502nm:湿分塗布量(20ml/m2)×塗布液濃度(0.04)÷二酸化珪素の密度(2.2g/cm3)÷0.74)
<無機微粒子層塗布液配合8>
コロイド状シリカ12%スラリー 10部
(扶桑化学工業製クォートロンPL−1、平均一次粒径15nm)
水にて全量を100部とした。(シリカ濃度1.2質量%)
粘度は1.3mPa・sであった。
(算定厚み147nm:湿分塗布量(20ml/m2)×塗布液濃度(0.012)÷二酸化珪素の密度(2.2g/cm3)÷0.74)
<無機微粒子層塗布液配合9>
コロイド状シリカ12%スラリー 6.7部
(扶桑化学工業製クォートロンPL−1、平均一次粒径15nm)
水にて全量を100部とした。(シリカ濃度0.8質量%)
(算定厚み98nm:湿分塗布量(20ml/m2)×塗布液濃度(0.008)÷二酸化珪素の密度(2.2g/cm3)÷0.74)
実施例4の無機微粒子層塗布液配合を無機微粒子層塗布液配合10に代える以外は同様にして比較例5のインクジェット記録媒体を得た。
<無機微粒子層塗布液配合10>
コロイド状シリカ12%スラリー 33部
(扶桑化学工業製クォートロンPL−1、平均一次粒径15nm)
水にて全量を100部とした。(シリカ濃度4.0質量%)
(算定厚み502nm:湿分塗布量(20ml/m2)×塗布液濃度(0.04)÷二酸化珪素の密度(2.2g/cm3)÷0.74)
なお、実施例1〜9及び比較例1〜4の無機微粒子層塗液の吸収所要時間は何れも0.3秒以内であった。
実施例9の塗布方法をアプリケーターロールで塗布液を供給後、エアナイフで掻き落として塗布量を調節する後計量タイプの塗布方式に変更して比較例6のインクジェット記録媒体を得た。湿分塗布量は塗布中における単位時間当たりの塗液減少量から計算された。
(算定厚み88nm:湿分塗布量(18ml/m2)×塗布液濃度(0.008)÷二酸化珪素の密度(2.2g/cm3)÷0.74)
実施例1の無機微粒子層塗布前の試料を比較例7のインクジェット記録媒体とした。
これらインクジェット記録媒体は、密封包装のもと50℃24時間経時後、以下の評価を行った。
<インク吸収性>
インクジェット記録媒体を23℃、湿度55%RHに一昼夜調湿後、同条件下でセイコーエプソン社製インクジェットプリンターMJ−800Cで黒ベタ印字後、時間間隔を変化して印字面にPPC用紙を重ねて軽く圧着し、剥がしてPPC用紙へのインク裏写りを評価した。
◎;20秒後でも全く裏写り無し。
○;20秒後ではやや裏写り有るが、25秒後では全く裏写り無し。
△;25秒後ではやや裏写り有るが、30秒後では全く裏写り無し。
×;30秒後でも裏写りが有る
インクジェット記録媒体の印字していない部分の光沢を目視で判定した。
○;写真用印画紙並で非常に良好。
△;アート、コート紙のレベルで良好。
×;マット紙に近く大幅に悪い。
インクジェット記録媒体の観察角度を変えながら干渉縞の見え方を分類した。
○;十分に傾けて干渉縞を探すと見える。
△;普通は見えないが大きく傾けた時、干渉縞が見える。
×;通常の観察角度の範囲でも干渉縞が見えることが有る。
また、表中「−」は無機微粒子層が無いか、表面の乱れのため光沢が無く、干渉縞の評価が出来ないことを表す。
外観上の故障の有無を観察した。以上結果を表1に示す。
Claims (1)
- 支持体上に、少なくとも1層の、平均二次粒子径が500nm以下のシリカ微粒子を含有する多孔質層を形成した後に、該多孔質層の上に無機微粒子層を設けるインクジェット記録媒体の製造方法であって、該多孔質層を形成した後に該無機微粒子層の塗布液を塗布するに際し、該無機微粒子層の塗布液は無機微粒子として球状のコロイド状シリカを含有し、且つ該無機微粒子層の塗布液の35℃粘度が10mPa・S以下であって、該多孔質層の空隙容量の90容量%以下の塗布量で、前計量タイプの塗布方式として直径100mm以下の斜線グラビアロールをリバース且つキスタッチにて使用する塗布装置にて塗布して、無機微粒子の固形分塗布量が0.304g/m2以下の無機微粒子層を設けることを特徴とするインクジェット記録媒体の製造方法。
Priority Applications (6)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2004201492A JP4357379B2 (ja) | 2003-11-10 | 2004-07-08 | インクジェット記録媒体の製造方法 |
EP04026303A EP1531057B1 (en) | 2003-11-10 | 2004-11-05 | Method for preparing ink-jet recording material |
DE602004018726T DE602004018726D1 (de) | 2003-11-10 | 2004-11-05 | Verfahren zur Herstellung eines Tintenstrahlaufzeichnungsmaterials |
AT04026303T ATE419124T1 (de) | 2003-11-10 | 2004-11-05 | Verfahren zur herstellung eines tintenstrahlaufzeichnungsmaterials |
CNB2004100923446A CN100375679C (zh) | 2003-11-10 | 2004-11-09 | 制备喷墨记录材料的方法 |
US10/983,721 US20050106317A1 (en) | 2003-10-10 | 2004-11-09 | Method for preparing ink-jet recording material |
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2003379240 | 2003-11-10 | ||
JP2004201492A JP4357379B2 (ja) | 2003-11-10 | 2004-07-08 | インクジェット記録媒体の製造方法 |
Publications (3)
Publication Number | Publication Date |
---|---|
JP2005161836A JP2005161836A (ja) | 2005-06-23 |
JP2005161836A5 JP2005161836A5 (ja) | 2006-12-14 |
JP4357379B2 true JP4357379B2 (ja) | 2009-11-04 |
Family
ID=34436965
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
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JP2004201492A Expired - Lifetime JP4357379B2 (ja) | 2003-10-10 | 2004-07-08 | インクジェット記録媒体の製造方法 |
Country Status (6)
Country | Link |
---|---|
US (1) | US20050106317A1 (ja) |
EP (1) | EP1531057B1 (ja) |
JP (1) | JP4357379B2 (ja) |
CN (1) | CN100375679C (ja) |
AT (1) | ATE419124T1 (ja) |
DE (1) | DE602004018726D1 (ja) |
Families Citing this family (16)
Publication number | Priority date | Publication date | Assignee | Title |
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US20060099408A1 (en) * | 2004-11-08 | 2006-05-11 | Akzo Nobel N.V. | Pigment composition |
US20060112855A1 (en) * | 2004-11-08 | 2006-06-01 | Akzo Nobel N.V. | Pigment composition |
US20060100338A1 (en) * | 2004-11-08 | 2006-05-11 | Akzo Nobel N.V. | Pigment composition |
JP4504306B2 (ja) * | 2005-12-06 | 2010-07-14 | 三菱製紙株式会社 | 顔料インク用インクジェット記録材料 |
JP4504316B2 (ja) * | 2006-01-06 | 2010-07-14 | 三菱製紙株式会社 | インクジェット用記録材料 |
JP4616816B2 (ja) * | 2006-10-24 | 2011-01-19 | 三菱製紙株式会社 | インクジェット記録方法 |
NZ579203A (en) * | 2007-02-26 | 2011-04-29 | Akzo Nobel Nv | Pigment composition containing polyalkyene glycol and colloidal silica or the like |
JP2009226371A (ja) * | 2008-03-25 | 2009-10-08 | Fujifilm Corp | 塗布方法及び装置 |
JP5167045B2 (ja) * | 2008-09-24 | 2013-03-21 | 三菱製紙株式会社 | インクジェット用記録紙 |
CA2765470A1 (en) * | 2009-06-26 | 2010-12-29 | Akzo Nobel Chemicals International B.V. | Coated substrate and method for the preparation thereof |
US8524336B2 (en) * | 2010-05-31 | 2013-09-03 | Canon Kabushiki Kaisha | Recording medium |
CN103889929B (zh) | 2011-10-11 | 2015-11-25 | 日立金属株式会社 | 陶瓷蜂窝结构体的制造方法和陶瓷蜂窝结构体 |
EP2770105A1 (de) * | 2013-02-20 | 2014-08-27 | Schoeller Technocell GmbH & Co. KG | Basispapier für dekorative Beschichtungswerkstoffe |
KR101761351B1 (ko) * | 2015-12-09 | 2017-07-26 | 주식회사 볼빅 | 골프공 커버 코팅용 조성물 및 이를 사용한 골프공 |
JP6775453B2 (ja) * | 2017-03-23 | 2020-10-28 | 山口精研工業株式会社 | 磁気ディスク基板用研磨剤組成物 |
US11584574B1 (en) | 2019-01-10 | 2023-02-21 | Printpack Illinois, Inc. | Recyclable packaging materials |
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EP0199874A1 (en) * | 1985-02-25 | 1986-11-05 | The Mead Corporation | Ink jet recording sheet having an ink-receptive layer containing polyethylene oxide |
JPH027663Y2 (ja) * | 1985-09-06 | 1990-02-23 | ||
US5275846A (en) * | 1991-07-24 | 1994-01-04 | Kanzaki Paper Mfg. Co., Ltd. | Method of producing a cast coated paper |
JP3402514B2 (ja) * | 1993-06-24 | 2003-05-06 | 三菱製紙株式会社 | インクジェット記録シート |
US5683501A (en) * | 1993-11-09 | 1997-11-04 | Nippon Shokubai Co., Ltd. | Compound fine particles and composition for forming film |
JP3684674B2 (ja) * | 1996-06-06 | 2005-08-17 | コニカミノルタホールディングス株式会社 | インクジェット記録用紙およびこれを用いた記録方法 |
US6465086B1 (en) * | 1997-05-15 | 2002-10-15 | Oji Paper Co., Ltd. | Ink jet recording material and process for producing same |
JP2000037944A (ja) * | 1998-07-24 | 2000-02-08 | Mitsubishi Paper Mills Ltd | インクジェット記録用シート |
US6472053B1 (en) * | 1998-10-07 | 2002-10-29 | Nippon Paper Industries Co., Ltd. | Ink jet recording sheet |
US6391428B1 (en) * | 1998-12-08 | 2002-05-21 | Nippon Paper Industries Co. Ltd. | Ink jet recording sheet |
JP4051838B2 (ja) * | 1999-04-26 | 2008-02-27 | 王子製紙株式会社 | 被記録体及びその製造方法 |
AU4255200A (en) * | 1999-08-10 | 2001-02-15 | Felix Schoeller Technical Papers, Inc. | High gloss ink-jet recording material |
WO2002003541A2 (en) * | 2000-06-30 | 2002-01-10 | Harris Corporation | Digitally modulated rf amplifier system having reduced intermodulation energy at rf channel edges |
JP2002067492A (ja) * | 2000-08-31 | 2002-03-05 | Konica Corp | インクジェット記録用紙 |
US6899930B2 (en) * | 2000-10-24 | 2005-05-31 | Mitsubishi Paper Mills Limited | Recording material for ink-jet |
JP2003145922A (ja) * | 2001-08-31 | 2003-05-21 | Mitsubishi Paper Mills Ltd | インクジェット記録材料及びその製造方法 |
US7303651B2 (en) * | 2001-11-08 | 2007-12-04 | Oji Paper Co., Ltd. | Ink jet recording paper |
US6789891B2 (en) * | 2001-12-04 | 2004-09-14 | Eastman Kodak Company | Ink jet printing method |
US7906187B2 (en) * | 2003-04-03 | 2011-03-15 | Hewlett-Packard Development Company, L.P. | Ink jet recording sheet with photoparity |
-
2004
- 2004-07-08 JP JP2004201492A patent/JP4357379B2/ja not_active Expired - Lifetime
- 2004-11-05 EP EP04026303A patent/EP1531057B1/en active Active
- 2004-11-05 DE DE602004018726T patent/DE602004018726D1/de active Active
- 2004-11-05 AT AT04026303T patent/ATE419124T1/de not_active IP Right Cessation
- 2004-11-09 CN CNB2004100923446A patent/CN100375679C/zh active Active
- 2004-11-09 US US10/983,721 patent/US20050106317A1/en not_active Abandoned
Also Published As
Publication number | Publication date |
---|---|
DE602004018726D1 (de) | 2009-02-12 |
JP2005161836A (ja) | 2005-06-23 |
EP1531057A3 (en) | 2007-07-18 |
ATE419124T1 (de) | 2009-01-15 |
EP1531057B1 (en) | 2008-12-31 |
EP1531057A2 (en) | 2005-05-18 |
CN100375679C (zh) | 2008-03-19 |
CN1616244A (zh) | 2005-05-18 |
US20050106317A1 (en) | 2005-05-19 |
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