JP4347758B2 - シリコーン樹脂およびクレーを含むポリマーフィルム - Google Patents
シリコーン樹脂およびクレーを含むポリマーフィルム Download PDFInfo
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- JP4347758B2 JP4347758B2 JP2004199830A JP2004199830A JP4347758B2 JP 4347758 B2 JP4347758 B2 JP 4347758B2 JP 2004199830 A JP2004199830 A JP 2004199830A JP 2004199830 A JP2004199830 A JP 2004199830A JP 4347758 B2 JP4347758 B2 JP 4347758B2
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- Prior art keywords
- layer
- film
- silicone resin
- resin particles
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- Expired - Lifetime
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B27/00—Layered products comprising a layer of synthetic resin
- B32B27/18—Layered products comprising a layer of synthetic resin characterised by the use of special additives
- B32B27/20—Layered products comprising a layer of synthetic resin characterised by the use of special additives using fillers, pigments, thixotroping agents
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B27/00—Layered products comprising a layer of synthetic resin
- B32B27/06—Layered products comprising a layer of synthetic resin as the main or only constituent of a layer, which is next to another layer of the same or of a different material
- B32B27/08—Layered products comprising a layer of synthetic resin as the main or only constituent of a layer, which is next to another layer of the same or of a different material of synthetic resin
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B27/00—Layered products comprising a layer of synthetic resin
- B32B27/36—Layered products comprising a layer of synthetic resin comprising polyesters
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J7/00—Chemical treatment or coating of shaped articles made of macromolecular substances
- C08J7/04—Coating
- C08J7/0427—Coating with only one layer of a composition containing a polymer binder
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2250/00—Layers arrangement
- B32B2250/02—2 layers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2250/00—Layers arrangement
- B32B2250/24—All layers being polymeric
- B32B2250/244—All polymers belonging to those covered by group B32B27/36
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2255/00—Coating on the layer surface
- B32B2255/10—Coating on the layer surface on synthetic resin layer or on natural or synthetic rubber layer
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2255/00—Coating on the layer surface
- B32B2255/26—Polymeric coating
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2264/00—Composition or properties of particles which form a particulate layer or are present as additives
- B32B2264/02—Synthetic macromolecular particles
- B32B2264/0214—Particles made of materials belonging to B32B27/00
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2264/00—Composition or properties of particles which form a particulate layer or are present as additives
- B32B2264/10—Inorganic particles
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2307/00—Properties of the layers or laminate
- B32B2307/50—Properties of the layers or laminate having particular mechanical properties
- B32B2307/538—Roughness
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2439/00—Containers; Receptacles
- B32B2439/40—Closed containers
- B32B2439/62—Boxes, cartons, cases
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
- C08J2483/00—Characterised by the use of macromolecular compounds obtained by reactions forming in the main chain of the macromolecule a linkage containing silicon with or without sulfur, nitrogen, oxygen, or carbon only; Derivatives of such polymers
-
- H—ELECTRICITY
- H05—ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR
- H05K—PRINTED CIRCUITS; CASINGS OR CONSTRUCTIONAL DETAILS OF ELECTRIC APPARATUS; MANUFACTURE OF ASSEMBLAGES OF ELECTRICAL COMPONENTS
- H05K1/00—Printed circuits
- H05K1/02—Details
- H05K1/03—Use of materials for the substrate
- H05K1/0313—Organic insulating material
- H05K1/0353—Organic insulating material consisting of two or more materials, e.g. two or more polymers, polymer + filler, + reinforcement
- H05K1/036—Multilayers with layers of different types
-
- H—ELECTRICITY
- H05—ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR
- H05K—PRINTED CIRCUITS; CASINGS OR CONSTRUCTIONAL DETAILS OF ELECTRIC APPARATUS; MANUFACTURE OF ASSEMBLAGES OF ELECTRICAL COMPONENTS
- H05K1/00—Printed circuits
- H05K1/02—Details
- H05K1/03—Use of materials for the substrate
- H05K1/0313—Organic insulating material
- H05K1/0353—Organic insulating material consisting of two or more materials, e.g. two or more polymers, polymer + filler, + reinforcement
- H05K1/0373—Organic insulating material consisting of two or more materials, e.g. two or more polymers, polymer + filler, + reinforcement containing additives, e.g. fillers
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/25—Web or sheet containing structurally defined element or component and including a second component containing structurally defined particles
- Y10T428/252—Glass or ceramic [i.e., fired or glazed clay, cement, etc.] [porcelain, quartz, etc.]
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/25—Web or sheet containing structurally defined element or component and including a second component containing structurally defined particles
- Y10T428/254—Polymeric or resinous material
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/31504—Composite [nonstructural laminate]
- Y10T428/31786—Of polyester [e.g., alkyd, etc.]
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Laminated Bodies (AREA)
- Manufacture Of Macromolecular Shaped Articles (AREA)
- Thermal Transfer Or Thermal Recording In General (AREA)
- Shaping By String And By Release Of Stress In Plastics And The Like (AREA)
Description
式中、xは1以上であり、好ましくは1〜1.9であり、より好ましくは1〜1.5であり、そして特に1〜1.2である。Rは脂肪族炭化水素基、例えば、メチル、エチルまたはブチル基、または、芳香族炭化水素基、例えば、フェニル基、または、不飽和炭化水素基、例えば、ビニル基のような有機基である。本発明の好ましい態様において、Rは1〜8個の炭素原子、より好ましくは1〜5個の炭素原子を有する炭化水素基である。本発明の特に好ましい態様において、Rはメチル基である。Rは上記の炭化水素基のいずれかの2種以上の混合物を含むことができる。特に好ましい樹脂粒子はメチルセスキオキサンを含む。
式中、Rはシリコーン樹脂粒子に関して上記において規定した有機基である。焼成の間に、少なくとも空気中においては、R基の消失、並びに、Si−OH結合および更なるSi−O−Si結合の生成が起こる。焼成の前には、シリコーン樹脂粒子中に存在するSi−OH結合は実質的に存在しない。更に、焼成はSi−OH結合のSi−O−Si結合への転化をもたらし、そしてシリカ粒子の最終的な生成をもたらした。xの値は好ましくは0〜0.9の範囲であり、より好ましくは0.05〜0.7であり、特に、0.1〜0.5であり、そして特に0.15〜0.3である。yの値は、好ましくは、0〜1.2であり、より好ましくは0.2〜1.0であり、特に0.4〜0.8であり、そして更に特に0.5〜0.7である。xおよびyの値は、例えば、29SiマジックアングルスピニングNMR分光器により決定されうる。
体積分布メジアン粒径および粒径分布比、D25/D75およびD10/D90をコルターLS130(Coulter Electronics Ltd.,Luton,UK)粒径測定器を使用して測定した。
ポリマーフィルムの動摩擦係数を、Instron Universal Testing Machine(Instron,UK)を使用して、ASTM 試験D 1894−87の手順により、ポリマーフィルム自体に対して測定した。
(ii)粒径分布比D25/D75=1.40
(iii)粒径分布比D10/D90=1.85
(iv)BET比表面積=45m2/g
(v)骨格密度=2.06g/cm3
(vi)メチル器の珪素原子に対する比=0.2
2)第二層の二乗平均粗さ=150nm
3)第二層のシェフィールド粗さ=10シェフィールド単位
4)曇り度=2%
Claims (13)
- ポリマー材料の第一層を含み、その少なくとも片側表面上にポリマー材料の第二層を有する光学的に透明なポリマーフィルムであって、前記ポリマー材料の第一層は500ppm未満の充填剤を含み、そして前記ポリマー材料の第二層は、第二層中のポリマーの重量を基準にして、(a)1.5〜12.5μmの体積分布メジアン粒径を有する焼成シリコーン樹脂粒子0.05〜2.0重量%、および、(b)0.1〜2.0μmの体積分布メジアン粒径を有する焼成チャイナクレー粒子0.005〜1.0重量%を含み、前記焼成シリコーン樹脂粒子が以下の式:
Rx(OH)ySiO2-((x+y)/2)
(式中、Rは有機基であり、xは0.05〜0.9であり、そしてyは0〜1.2である)の三次元ポリマー鎖構造を含む、光学的に透明なポリマーフィルム。 - 前記第一層が充填剤を含まない請求項1に記載のフィルム。
- 前記フィルムの合計厚さが、少なくとも80μmである請求項1または2に記載のフィルム。
- 前記フィルムの合計厚さが、80〜200μmである請求項3に記載のフィルム。
- 前記フィルムは、3%未満の広角曇り度を有する請求項1ないし4のいずれか1つに記載のフィルム。
- 前記焼成シリコーン樹脂粒子が以下の式:
Rx(OH)ySiO2-((x+y)/2)
(式中、Rは有機基であり、xは0.05〜0.7であり、そしてyは0〜1.2である)の三次元ポリマー鎖構造を含む請求項1ないし5のいずれか1つに記載のフィルム。 - 前記焼成シリコーン樹脂粒子が80m2/g未満のBET比表面積を有する請求項1ないし6のいずれか1つに記載のフィルム。
- 前記焼成シリコーン樹脂粒子の体積分布メジアン粒径が2.8〜5.0μmの範囲である請求項1ないし7のいずれか1つに記載のフィルム。
- 前記第二層が焼成シリコーン樹脂粒子を0.2〜0.5重量%含む請求項1ないし8のいずれか1つに記載のフィルム。
- 前記焼成チャイナクレー粒子の体積分布メジアン粒径が、0.2〜0.6μmの範囲である請求項1ないし8のいずれか1つに記載のフィルム。
- 前記第二層が0.015〜0.1重量%の焼成チャイナクレー粒子を含む請求項1ないし10のいずれか1つに記載のフィルム。
- 前記第一層または第二層のうちの少なくとも片方が結晶性または半結晶性のポリエチレンテレフタレートおよび/またはポリエチレンナフタレートを含む請求項1ないし11のいずれか1つに記載のフィルム。
- 少なくとも片側表面上にポリマー材料の第二層を有するポリマー材料の第一層基材を成形することを含むポリマーフィルムを製造するための方法であって、前記ポリマー材料の第一層は500ppm未満の充填剤を含み、そして前記ポリマー材料の第二層は、第二層中のポリマーの重量を基準にして、(a)1.5〜12.5μmの体積分布メジアン粒径を有する焼成シリコーン樹脂粒子0.05〜2.0重量%、および、(b)0.1〜2.0μmの体積分布メジアン粒径を有する焼成チャイナクレー粒子0.005〜1.0重量%を含み、前記焼成シリコーン樹脂粒子が以下の式:
Rx(OH)ySiO2-((x+y)/2)
(式中、Rは有機基であり、xは0.05〜0.9であり、そしてyは0〜1.2である)の三次元ポリマー鎖構造を含む、方法。
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US08/271,448 US5614313A (en) | 1994-07-07 | 1994-07-07 | Polymeric film having a layer comprising calcined silicone particles and china clay particles |
Related Parent Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP50418196A Division JP4205160B2 (ja) | 1994-07-07 | 1995-07-06 | シリコーン樹脂およびクレーを含むポリマーフィルム |
Publications (2)
Publication Number | Publication Date |
---|---|
JP2004330791A JP2004330791A (ja) | 2004-11-25 |
JP4347758B2 true JP4347758B2 (ja) | 2009-10-21 |
Family
ID=23035621
Family Applications (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP50418196A Expired - Lifetime JP4205160B2 (ja) | 1994-07-07 | 1995-07-06 | シリコーン樹脂およびクレーを含むポリマーフィルム |
JP2004199830A Expired - Lifetime JP4347758B2 (ja) | 1994-07-07 | 2004-07-06 | シリコーン樹脂およびクレーを含むポリマーフィルム |
Family Applications Before (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP50418196A Expired - Lifetime JP4205160B2 (ja) | 1994-07-07 | 1995-07-06 | シリコーン樹脂およびクレーを含むポリマーフィルム |
Country Status (11)
Country | Link |
---|---|
US (1) | US5614313A (ja) |
EP (1) | EP0768952B1 (ja) |
JP (2) | JP4205160B2 (ja) |
KR (1) | KR100354097B1 (ja) |
CN (1) | CN1078846C (ja) |
AT (1) | ATE172151T1 (ja) |
AU (1) | AU2985195A (ja) |
CA (1) | CA2193619A1 (ja) |
DE (1) | DE69505388T2 (ja) |
TW (1) | TW412570B (ja) |
WO (1) | WO1996001739A1 (ja) |
Families Citing this family (14)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR20010033739A (ko) * | 1997-12-31 | 2001-04-25 | 메리 이. 보울러 | 흐림도가 낮고 반점이 없는 폴리에스테르 필름 |
US6060156A (en) * | 1998-03-30 | 2000-05-09 | E. I. Du Pont De Nemours And Company | Porous alumina and partially calcined polysiloxane particles in interdraw coating resins for polyester film |
US6291632B1 (en) * | 1998-12-10 | 2001-09-18 | Grantec Inc. | Microspheres of melamine |
GB0209355D0 (en) * | 2002-04-24 | 2002-06-05 | Imerys Minerals Ltd | An opacified polymer composition |
FR2844142B1 (fr) * | 2002-09-11 | 2007-08-17 | Bayer Cropscience Sa | Plantes transformees a biosynthese de prenylquinones amelioree |
EP1428684A3 (de) * | 2002-11-29 | 2004-09-22 | Folex Coating GmbH | Dekorfolie |
FR2848064B1 (fr) * | 2002-12-06 | 2006-01-13 | Bayer Cropscience Sa | Plantes legumineuses transplastomiques fertiles |
US6893476B2 (en) | 2002-12-09 | 2005-05-17 | Dupont Air Products Nanomaterials Llc | Composition and associated methods for chemical mechanical planarization having high selectivity for metal removal |
FR2848570B1 (fr) | 2002-12-12 | 2005-04-01 | Bayer Cropscience Sa | Cassette d'expression codant pour une 5-enol pyruvylshikimate-3-phosphate synthase (epsps) et plantes tolerantes aux herbicides la contenant |
JP4583105B2 (ja) * | 2004-08-12 | 2010-11-17 | 三菱樹脂株式会社 | 共押出し積層ポリエテルフィルム |
GB0505967D0 (en) * | 2005-03-23 | 2005-04-27 | Imerys Minerals Ltd | Infrared absorbing polymer compositions and films |
US20080003387A1 (en) * | 2006-06-16 | 2008-01-03 | Gene Michael Altonen | Plastic pressurized dispenser |
AR074941A1 (es) | 2009-01-07 | 2011-02-23 | Bayer Cropscience Sa | Plantas transplastomicas exentas de marcador de seleccion |
KR102401310B1 (ko) * | 2020-07-06 | 2022-05-23 | 도레이첨단소재 주식회사 | 적층 폴리에스테르 필름 |
Family Cites Families (13)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
IT577841A (ja) * | 1956-09-12 | |||
US3980611A (en) * | 1970-07-07 | 1976-09-14 | E. I. Du Pont De Nemours And Company | Filled thermoplastic films |
US3821156A (en) * | 1972-01-03 | 1974-06-28 | Celanese Corp | Polyethylene terephthalate film |
US4533509A (en) * | 1983-04-28 | 1985-08-06 | Mobil Oil Corporation | Low coefficient of friction film structure and method of forming the same |
FR2549076B1 (fr) * | 1983-07-13 | 1986-10-10 | Rhone Poulenc Films | Films en polyester charges et bi-etires et utilisation de ces films pour la fabrication notamment de bandes magnetiques |
FR2548958B1 (fr) * | 1983-07-13 | 1986-03-21 | Rhone Poulenc Films | Films polyesters composites |
US4761327A (en) * | 1986-01-17 | 1988-08-02 | Teijin Limited | Biaxially oriented aromatic polyester film |
US4818581A (en) * | 1986-08-27 | 1989-04-04 | Teijin Limited | Biaxially oriented polyester film |
GB9110902D0 (en) * | 1991-05-21 | 1991-07-10 | Ici Plc | Polymeric film |
GB9112843D0 (en) * | 1991-06-14 | 1991-07-31 | Ici Plc | Polymeric film |
EP0604057A1 (en) * | 1992-12-23 | 1994-06-29 | Imperial Chemical Industries Plc | Polymeric film |
GB9324989D0 (en) * | 1992-12-23 | 1994-01-26 | Ici Plc | Polymeric film |
US5372879A (en) * | 1993-02-22 | 1994-12-13 | Teijin Limited | Biaxially oriented polyester film |
-
1994
- 1994-07-07 US US08/271,448 patent/US5614313A/en not_active Expired - Lifetime
-
1995
- 1995-07-06 CA CA 2193619 patent/CA2193619A1/en not_active Abandoned
- 1995-07-06 KR KR1019970700035A patent/KR100354097B1/ko not_active IP Right Cessation
- 1995-07-06 AU AU29851/95A patent/AU2985195A/en not_active Abandoned
- 1995-07-06 DE DE69505388T patent/DE69505388T2/de not_active Expired - Lifetime
- 1995-07-06 JP JP50418196A patent/JP4205160B2/ja not_active Expired - Lifetime
- 1995-07-06 CN CN95193974A patent/CN1078846C/zh not_active Expired - Lifetime
- 1995-07-06 AT AT95925899T patent/ATE172151T1/de not_active IP Right Cessation
- 1995-07-06 WO PCT/GB1995/001589 patent/WO1996001739A1/en active IP Right Grant
- 1995-07-06 EP EP19950925899 patent/EP0768952B1/en not_active Expired - Lifetime
- 1995-07-13 TW TW84107268A patent/TW412570B/zh not_active IP Right Cessation
-
2004
- 2004-07-06 JP JP2004199830A patent/JP4347758B2/ja not_active Expired - Lifetime
Also Published As
Publication number | Publication date |
---|---|
TW412570B (en) | 2000-11-21 |
WO1996001739A1 (en) | 1996-01-25 |
CA2193619A1 (en) | 1996-01-25 |
AU2985195A (en) | 1996-02-09 |
KR970704578A (ko) | 1997-09-06 |
JP4205160B2 (ja) | 2009-01-07 |
DE69505388T2 (de) | 1999-05-06 |
US5614313A (en) | 1997-03-25 |
EP0768952A1 (en) | 1997-04-23 |
JPH10502587A (ja) | 1998-03-10 |
KR100354097B1 (ko) | 2003-03-15 |
CN1151714A (zh) | 1997-06-11 |
CN1078846C (zh) | 2002-02-06 |
JP2004330791A (ja) | 2004-11-25 |
EP0768952B1 (en) | 1998-10-14 |
DE69505388D1 (de) | 1998-11-19 |
ATE172151T1 (de) | 1998-10-15 |
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