JP4166089B2 - 結晶ナノ粒子から成る支持層に基づく機能性セラミック層 - Google Patents
結晶ナノ粒子から成る支持層に基づく機能性セラミック層 Download PDFInfo
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- C—CHEMISTRY; METALLURGY
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- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/009—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone characterised by the material treated
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
- C03C17/006—Surface treatment of glass, not in the form of fibres or filaments, by coating with materials of composite character
- C03C17/007—Surface treatment of glass, not in the form of fibres or filaments, by coating with materials of composite character containing a dispersed phase, e.g. particles, fibres or flakes, in a continuous phase
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
- C03C17/22—Surface treatment of glass, not in the form of fibres or filaments, by coating with other inorganic material
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- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
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- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
- C04B41/4582—Porous coatings, e.g. coating containing porous fillers
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- C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
- C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
- C04B41/81—Coating or impregnation
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- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C24/00—Coating starting from inorganic powder
- C23C24/08—Coating starting from inorganic powder by application of heat or pressure and heat
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C2217/00—Coatings on glass
- C03C2217/40—Coatings comprising at least one inhomogeneous layer
- C03C2217/425—Coatings comprising at least one inhomogeneous layer consisting of a porous layer
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/00474—Uses not provided for elsewhere in C04B2111/00
- C04B2111/00793—Uses not provided for elsewhere in C04B2111/00 as filters or diaphragms
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/12—All metal or with adjacent metals
- Y10T428/12493—Composite; i.e., plural, adjacent, spatially distinct metal components [e.g., layers, joint, etc.]
- Y10T428/12535—Composite; i.e., plural, adjacent, spatially distinct metal components [e.g., layers, joint, etc.] with additional, spatially distinct nonmetal component
- Y10T428/12611—Oxide-containing component
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/249921—Web or sheet containing structurally defined element or component
- Y10T428/249953—Composite having voids in a component [e.g., porous, cellular, etc.]
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/25—Web or sheet containing structurally defined element or component and including a second component containing structurally defined particles
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/25—Web or sheet containing structurally defined element or component and including a second component containing structurally defined particles
- Y10T428/252—Glass or ceramic [i.e., fired or glazed clay, cement, etc.] [porcelain, quartz, etc.]
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/25—Web or sheet containing structurally defined element or component and including a second component containing structurally defined particles
- Y10T428/254—Polymeric or resinous material
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- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Mechanical Engineering (AREA)
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- Dispersion Chemistry (AREA)
- Composite Materials (AREA)
- Laminated Bodies (AREA)
- Other Surface Treatments For Metallic Materials (AREA)
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- Compositions Of Oxide Ceramics (AREA)
- Porous Artificial Stone Or Porous Ceramic Products (AREA)
- Materials For Medical Uses (AREA)
Description
請求項2記載の方法は、請求項1記載の方法において、前記多孔質層は物質を充填するか、又は、処理パラメータの選択によって設定されるフラクタル(fractal)構造を有することを特徴とする。
請求項3記載の方法は、請求項1又は2記載の方法において、焼成前における前記塗布された層の前記ナノ粒子の固体含有量が少なくとも35容積%より大きく、そして特に好ましくは40容量%より大きいことを特徴とする。
請求項4記載の方法は、請求項1乃至3のいずれか1項に記載の方法において、前記セラミック層は可撓性を有し、損傷することなく90°より大きい、好ましくは120°より大きい曲げに耐えることを特徴とする。
請求項5記載の方法は、請求項1乃至4のいずれか1項に記載の方法において、前記多孔質層は理論密度近傍になるまで焼結されることを特徴とする。
請求項6記載の方法は、請求項1乃至5のいずれか1項に記載の方法において、前記セラミック層は透明であることを特徴とする。
請求項7記載の方法は、請求項1乃至6のいずれか1項に記載の方法において、前記多孔質層は、疎水性又は親水性を付与する防埃物質及び腐食防止物質、並びに細菌物質、香料、香水、吸入物質が充填されることを特徴とする。
請求項8記載の方法は、請求項7記載の方法において、前記セラミック層の孔内の前記物質は、必要により前記セラミック層の表面に移動することを特徴とする。
請求項9記載の方法は、請求項1乃至8のいずれか1項に記載の多孔質セラミック層を腐食防止層及び摩擦層として使用することを特徴とする。
請求項10記載の方法は、請求項1乃至8のいずれか1項に記載の多孔質セラミック層を自己洗浄又は洗浄容易な層として使用することを特徴とする。
請求項11記載の方法は、請求項1乃至8のいずれか1項に記載の多孔質セラミック層を薬物の搬送体として、好ましくは医療機器において使用することを特徴とする。
請求項12記載の方法は、請求項1記載のセラミック層をセラミック基板上に配設してセラミックフィルタとして使用することを特徴とする。
30gのイットリウムで安定化されたナノスケール二酸化ジルコニウム(一次粒径が10nm)を、水で希釈されたオキシカルボン酸と混合した。4.5gのポリビニルアルコールをこの懸濁液に加え、懸濁液を均質化する。透明又は半透明の溶液を液浸コーティングにより10×10cmの鋼基板(1.4511又は1.4301)上に配置し、80℃で乾燥室内で乾燥した。次いで、コーティングされた鋼基板1を、1時間500℃に保持した。加熱速度は5K/minであった。これにより、多孔質セラミック層が形成された。
実施例1と同様に、鋼基板に多孔質セラミック層を形成した。次いで、この層に、前もって加水分解された市販のフッ化シランを含浸させ、150℃で凝固させる。撥水性及び撥油性の耐引っかき性層を形成した。
30gのイットリウムで安定化されたナノスケール二酸化ジルコニウム(一次粒径が10nm)が、エチレングリコールで希釈されたオキシカルボン酸と混合した。アクリル結合剤(Laromer BASF社)とラディカルスタータとをこの懸濁液に加え、懸濁液を撹拌して均質化した。透明又は半透明の溶液を10×10cmの鋼基板(1.4511又は1.4301)に塗布し、UV光により硬化した。層を500℃で1時間に亘り成形した。
Claims (12)
- 金属、セラミック、エナメル、又はガラスから成る基板上に多孔質セラミック層を形成する方法であって、
a)3nm乃至100nmの範囲の粒径の粒子から成る酸化物、炭化物、窒化物、又は硫化物の粉末を、トリオキサデカン酸又はディオキサヘプタン酸と混合し、
b)前記粉末を、少なくとも1つの溶媒と少なくとも1つの重合結合剤との混合物、又はモノマーとラディカルスタータ(radical starter)との組み合わせと混合し、
c)前記a)における混合物及びb)における混合物の群の一つから選択される混合物は、30容積%より大きいナノ粒子(nanoparticles)固体含有量を有し、さらに、前記a)における混合物及びb)における混合物の群の一つから選択される混合物を、浸漬コーティング、回転コーティング(spin coating)、液浸(immersion)、浸水(flooding)、吹付け塗装、スクリーン印刷、又はフィルムキャスティング(film casting)によって前記基板上に塗布し、乾燥し、凝固させて多孔質層にする
工程を備える方法。 - 前記多孔質層は物質を充填するか、又は、その開放孔が表面に一様に分布されることを特徴とする請求項1記載の方法。
- 焼成前における前記塗布された層の前記ナノ粒子の固体含有量が少なくとも35容積%より大きいことを特徴とする請求項1又は2記載の方法。
- 焼成前における前記塗布された層の前記ナノ粒子の固体含有量が少なくとも40%容積より大きいことを特徴とする請求項3記載の方法。
- 前記多孔質セラミック層は前記多孔質層中の固形分が凝固を開始する温度以上で焼結されることを特徴とする請求項1乃至4のいずれか1項に記載の方法。
- 前記多孔質セラミック層は、疎水性又は親水性を付与する防埃物質及び腐食防止物質、並びに細菌物質、香料、香水、吸入物質が充填されることを特徴とする請求項1乃至5のいずれか1項に記載の方法。
- 前記セラミック層の孔内の前記物質は、前記セラミック層の表面に移動することを特徴とする請求項6記載の方法。
- 請求項1乃至7のいずれか1項に記載の方法によって形成された多孔質セラミック層を腐食防止層及び摩擦層として使用する方法。
- 請求項1乃至7のいずれか1項に記載の方法によって形成された多孔質セラミック層を自己洗浄又は洗浄容易な層として使用する方法。
- 請求項1乃至7のいずれか1項に記載の方法によって形成された多孔質セラミック層を薬物の搬送体として使用する方法。
- 前記多孔質セラミック層は医療機器において使用される請求項10記載の方法。
- 請求項1記載の方法によって形成された多孔質セラミック層をセラミック基板上に配設してセラミックフィルタとして使用する方法。
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
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DE10119538A DE10119538C2 (de) | 2001-04-21 | 2001-04-21 | Verfahren zur Beschichtung von Substraten und deren Verwendungen |
PCT/DE2002/001453 WO2002086194A2 (de) | 2001-04-21 | 2002-04-19 | Funktionelle keramische schichten, auf basis einer, mit kristallinen nanoteilchen hergestellten trägerschicht |
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JP2004530045A JP2004530045A (ja) | 2004-09-30 |
JP2004530045A5 JP2004530045A5 (ja) | 2005-12-22 |
JP4166089B2 true JP4166089B2 (ja) | 2008-10-15 |
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JP2002583704A Expired - Fee Related JP4166089B2 (ja) | 2001-04-21 | 2002-04-19 | 結晶ナノ粒子から成る支持層に基づく機能性セラミック層 |
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US (1) | US6953603B2 (ja) |
EP (1) | EP1383940B1 (ja) |
JP (1) | JP4166089B2 (ja) |
CN (1) | CN1284745C (ja) |
AT (1) | ATE291649T1 (ja) |
AU (1) | AU2002315652A1 (ja) |
DE (2) | DE10119538C2 (ja) |
ES (1) | ES2239233T3 (ja) |
WO (1) | WO2002086194A2 (ja) |
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AU2003270802A1 (en) * | 2002-09-20 | 2004-04-08 | The Children's Hospital Of Philadelphia | Engineering of material surfaces |
KR101076135B1 (ko) * | 2002-12-12 | 2011-10-21 | 엔테그리스, 아이엔씨. | 다공성 소결 복합 재료 |
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DE102007010955A1 (de) | 2007-03-05 | 2008-09-11 | Leibniz-Institut Für Neue Materialien Gemeinnützige Gmbh | Beschichtungszusammensetzung |
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DE102007030047A1 (de) * | 2007-06-26 | 2009-01-02 | Siemens Ag | Bauteil mit einer schweren benetzbaren keramischen Schicht und Verfahren zu deren Herstellung |
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JPS5854089B2 (ja) | 1979-06-22 | 1983-12-02 | 株式会社日立製作所 | 透明導電膜の形成方法 |
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US6803138B2 (en) * | 2001-07-02 | 2004-10-12 | Nextech Materials, Ltd. | Ceramic electrolyte coating methods |
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DE10119538C2 (de) | 2003-06-26 |
CN1284745C (zh) | 2006-11-15 |
ATE291649T1 (de) | 2005-04-15 |
US6953603B2 (en) | 2005-10-11 |
WO2002086194A2 (de) | 2002-10-31 |
DE10119538A1 (de) | 2002-10-24 |
US20040115416A1 (en) | 2004-06-17 |
WO2002086194A3 (de) | 2003-05-30 |
CN1503767A (zh) | 2004-06-09 |
EP1383940B1 (de) | 2005-03-23 |
JP2004530045A (ja) | 2004-09-30 |
DE50202546D1 (de) | 2005-04-28 |
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