JP4137383B2 - 高光拡散性顔料混合物 - Google Patents
高光拡散性顔料混合物 Download PDFInfo
- Publication number
- JP4137383B2 JP4137383B2 JP2000570251A JP2000570251A JP4137383B2 JP 4137383 B2 JP4137383 B2 JP 4137383B2 JP 2000570251 A JP2000570251 A JP 2000570251A JP 2000570251 A JP2000570251 A JP 2000570251A JP 4137383 B2 JP4137383 B2 JP 4137383B2
- Authority
- JP
- Japan
- Prior art keywords
- silicon dioxide
- weight
- pigment mixture
- component
- pigment
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 239000000203 mixture Substances 0.000 title claims description 46
- 239000000049 pigment Substances 0.000 title claims description 43
- 238000009792 diffusion process Methods 0.000 title description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 56
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 40
- 239000000377 silicon dioxide Substances 0.000 claims description 28
- 235000012239 silicon dioxide Nutrition 0.000 claims description 28
- 238000000576 coating method Methods 0.000 claims description 21
- 238000000034 method Methods 0.000 claims description 20
- 239000004408 titanium dioxide Substances 0.000 claims description 20
- 239000011248 coating agent Substances 0.000 claims description 19
- 238000003756 stirring Methods 0.000 claims description 15
- 239000000843 powder Substances 0.000 claims description 11
- 239000000725 suspension Substances 0.000 claims description 10
- 239000002537 cosmetic Substances 0.000 claims description 9
- 239000000976 ink Substances 0.000 claims description 9
- 238000002360 preparation method Methods 0.000 claims description 8
- 238000007639 printing Methods 0.000 claims description 8
- 229910010413 TiO 2 Inorganic materials 0.000 claims description 5
- LIKBJVNGSGBSGK-UHFFFAOYSA-N iron(3+);oxygen(2-) Chemical compound [O-2].[O-2].[O-2].[Fe+3].[Fe+3] LIKBJVNGSGBSGK-UHFFFAOYSA-N 0.000 claims description 5
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 claims description 5
- 238000002156 mixing Methods 0.000 claims description 5
- 238000009472 formulation Methods 0.000 claims description 4
- 239000003973 paint Substances 0.000 claims description 4
- 229920000642 polymer Polymers 0.000 claims description 4
- 239000002966 varnish Substances 0.000 claims description 4
- 229910004298 SiO 2 Inorganic materials 0.000 claims description 3
- 238000001035 drying Methods 0.000 claims description 3
- 239000012429 reaction media Substances 0.000 claims description 3
- 238000010304 firing Methods 0.000 claims description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Substances [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 2
- 238000010330 laser marking Methods 0.000 claims description 2
- 238000005406 washing Methods 0.000 claims description 2
- 239000000243 solution Substances 0.000 description 13
- 239000000047 product Substances 0.000 description 10
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 9
- 239000010410 layer Substances 0.000 description 8
- 239000002245 particle Substances 0.000 description 8
- 239000004615 ingredient Substances 0.000 description 7
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 description 6
- 239000008367 deionised water Substances 0.000 description 6
- 229910021641 deionized water Inorganic materials 0.000 description 6
- 239000000463 material Substances 0.000 description 5
- 150000003608 titanium Chemical class 0.000 description 5
- 239000006071 cream Substances 0.000 description 4
- RBTARNINKXHZNM-UHFFFAOYSA-K iron trichloride Chemical compound Cl[Fe](Cl)Cl RBTARNINKXHZNM-UHFFFAOYSA-K 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- XJDNKRIXUMDJCW-UHFFFAOYSA-J titanium tetrachloride Chemical compound Cl[Ti](Cl)(Cl)Cl XJDNKRIXUMDJCW-UHFFFAOYSA-J 0.000 description 4
- 230000037303 wrinkles Effects 0.000 description 4
- 238000005266 casting Methods 0.000 description 3
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- VTLYFUHAOXGGBS-UHFFFAOYSA-N Fe3+ Chemical compound [Fe+3] VTLYFUHAOXGGBS-UHFFFAOYSA-N 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- 229910021578 Iron(III) chloride Inorganic materials 0.000 description 2
- 229920002472 Starch Polymers 0.000 description 2
- 235000010724 Wisteria floribunda Nutrition 0.000 description 2
- 239000000654 additive Substances 0.000 description 2
- TZCXTZWJZNENPQ-UHFFFAOYSA-L barium sulfate Chemical compound [Ba+2].[O-]S([O-])(=O)=O TZCXTZWJZNENPQ-UHFFFAOYSA-L 0.000 description 2
- 239000011230 binding agent Substances 0.000 description 2
- 239000000839 emulsion Substances 0.000 description 2
- 239000008187 granular material Substances 0.000 description 2
- 238000007645 offset printing Methods 0.000 description 2
- 239000008188 pellet Substances 0.000 description 2
- 239000002244 precipitate Substances 0.000 description 2
- 239000002243 precursor Substances 0.000 description 2
- 150000003839 salts Chemical class 0.000 description 2
- 239000008107 starch Substances 0.000 description 2
- 235000019698 starch Nutrition 0.000 description 2
- 239000007858 starting material Substances 0.000 description 2
- 239000010414 supernatant solution Substances 0.000 description 2
- 230000000007 visual effect Effects 0.000 description 2
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonium chloride Substances [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 description 1
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 description 1
- CWYNVVGOOAEACU-UHFFFAOYSA-N Fe2+ Chemical class [Fe+2] CWYNVVGOOAEACU-UHFFFAOYSA-N 0.000 description 1
- 239000004115 Sodium Silicate Substances 0.000 description 1
- WGLPBDUCMAPZCE-UHFFFAOYSA-N Trioxochromium Chemical compound O=[Cr](=O)=O WGLPBDUCMAPZCE-UHFFFAOYSA-N 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 150000008044 alkali metal hydroxides Chemical class 0.000 description 1
- QGZKDVFQNNGYKY-UHFFFAOYSA-N ammonia Natural products N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 1
- 235000011114 ammonium hydroxide Nutrition 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 239000007900 aqueous suspension Substances 0.000 description 1
- 239000002585 base Substances 0.000 description 1
- 239000000378 calcium silicate Substances 0.000 description 1
- 229910052918 calcium silicate Inorganic materials 0.000 description 1
- OYACROKNLOSFPA-UHFFFAOYSA-N calcium;dioxido(oxo)silane Chemical compound [Ca+2].[O-][Si]([O-])=O OYACROKNLOSFPA-UHFFFAOYSA-N 0.000 description 1
- 239000006229 carbon black Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 229910000423 chromium oxide Inorganic materials 0.000 description 1
- 239000003086 colorant Substances 0.000 description 1
- 238000004040 coloring Methods 0.000 description 1
- 238000005034 decoration Methods 0.000 description 1
- IJKVHSBPTUYDLN-UHFFFAOYSA-N dihydroxy(oxo)silane Chemical compound O[Si](O)=O IJKVHSBPTUYDLN-UHFFFAOYSA-N 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 238000004945 emulsification Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 239000000499 gel Substances 0.000 description 1
- 238000007646 gravure printing Methods 0.000 description 1
- 238000009499 grossing Methods 0.000 description 1
- 239000008269 hand cream Substances 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- 230000003301 hydrolyzing effect Effects 0.000 description 1
- 229910021331 inorganic silicon compound Inorganic materials 0.000 description 1
- QGPQTSCLUYMZHL-UHFFFAOYSA-N iron(3+);oxygen(2-);hydrate Chemical compound O.[O-2].[O-2].[O-2].[Fe+3].[Fe+3] QGPQTSCLUYMZHL-UHFFFAOYSA-N 0.000 description 1
- 229910021506 iron(II) hydroxide Inorganic materials 0.000 description 1
- NCNCGGDMXMBVIA-UHFFFAOYSA-L iron(ii) hydroxide Chemical compound [OH-].[OH-].[Fe+2] NCNCGGDMXMBVIA-UHFFFAOYSA-L 0.000 description 1
- -1 lipsticks Substances 0.000 description 1
- 239000010445 mica Substances 0.000 description 1
- 229910052618 mica group Inorganic materials 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 229920000620 organic polymer Polymers 0.000 description 1
- 239000006072 paste Substances 0.000 description 1
- 238000009702 powder compression Methods 0.000 description 1
- 239000012266 salt solution Substances 0.000 description 1
- 238000007650 screen-printing Methods 0.000 description 1
- 239000002453 shampoo Substances 0.000 description 1
- 239000002356 single layer Substances 0.000 description 1
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 description 1
- 229910052911 sodium silicate Inorganic materials 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000004448 titration Methods 0.000 description 1
- 239000000606 toothpaste Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
- C09C1/0081—Composite particulate pigments or fillers, i.e. containing at least two solid phases, except those consisting of coated particles of one compound
- C09C1/0084—Composite particulate pigments or fillers, i.e. containing at least two solid phases, except those consisting of coated particles of one compound containing titanium dioxide
- C09C1/0087—Composite particulate pigments or fillers, i.e. containing at least two solid phases, except those consisting of coated particles of one compound containing titanium dioxide only containing titanium dioxide and silica or silicate
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
- C09C1/28—Compounds of silicon
- C09C1/30—Silicic acid
- C09C1/3045—Treatment with inorganic compounds
- C09C1/3054—Coating
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/30—Particle morphology extending in three dimensions
- C01P2004/32—Spheres
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/60—Particles characterised by their size
- C01P2004/61—Micrometer sized, i.e. from 1-100 micrometer
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/80—Particles consisting of a mixture of two or more inorganic phases
- C01P2004/82—Particles consisting of a mixture of two or more inorganic phases two phases having the same anion, e.g. both oxidic phases
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/60—Optical properties, e.g. expressed in CIELAB-values
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/60—Optical properties, e.g. expressed in CIELAB-values
- C01P2006/62—L* (lightness axis)
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/60—Optical properties, e.g. expressed in CIELAB-values
- C01P2006/66—Hue (H*)
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Composite Materials (AREA)
- Cosmetics (AREA)
- Pigments, Carbon Blacks, Or Wood Stains (AREA)
- Paints Or Removers (AREA)
- Inks, Pencil-Leads, Or Crayons (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19842134A DE19842134A1 (de) | 1998-09-14 | 1998-09-14 | Pigment mit hoher Lichtdiffusion |
| DE19842134.6 | 1998-09-14 | ||
| PCT/EP1999/006751 WO2000015720A1 (de) | 1998-09-14 | 1999-09-13 | Pigmentgemisch mit hoher lichtdiffusion |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2002524647A JP2002524647A (ja) | 2002-08-06 |
| JP2002524647A5 JP2002524647A5 (enExample) | 2006-11-09 |
| JP4137383B2 true JP4137383B2 (ja) | 2008-08-20 |
Family
ID=7880982
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2000570251A Expired - Lifetime JP4137383B2 (ja) | 1998-09-14 | 1999-09-13 | 高光拡散性顔料混合物 |
Country Status (7)
| Country | Link |
|---|---|
| EP (1) | EP1115796B1 (enExample) |
| JP (1) | JP4137383B2 (enExample) |
| CN (1) | CN1158358C (enExample) |
| AU (1) | AU5747099A (enExample) |
| DE (2) | DE19842134A1 (enExample) |
| ES (1) | ES2190249T3 (enExample) |
| WO (1) | WO2000015720A1 (enExample) |
Families Citing this family (21)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE10024466A1 (de) | 2000-05-18 | 2001-11-22 | Merck Patent Gmbh | Pigmente mit Opalstruktur |
| WO2001096635A2 (en) | 2000-06-15 | 2001-12-20 | Merck Patent Gmbh | A method for producing sphere-based crystals |
| WO2002044301A2 (en) | 2000-11-30 | 2002-06-06 | Merck Patent Gmbh | Particles with opalescent effect |
| DE10259246A1 (de) * | 2002-12-17 | 2004-07-01 | Merck Patent Gmbh | Anorganische sphärische Absorptionspigmente |
| FR2862534A1 (fr) * | 2003-11-26 | 2005-05-27 | Oreal | Composition cosmetique comprenant des particules de durete differente |
| DE10357679A1 (de) * | 2003-12-10 | 2005-07-07 | Merck Patent Gmbh | Effektfarbmittel enthaltend Kern-Mantel-Partikel |
| DE102007062945A1 (de) | 2007-12-21 | 2009-06-25 | Rehau Ag + Co. | Karosserie-Kunststoffbauteil für ein Kraftfahrzeug sowie dessen Verwendung |
| DE102008020440A1 (de) * | 2008-04-23 | 2009-10-29 | Merck Patent Gmbh | Reaktiv oberflächenmodifizierte Partikel |
| DE102008045308A1 (de) | 2008-09-02 | 2010-03-04 | Merck Patent Gmbh | Dispersionen |
| DE102009029763A1 (de) | 2009-06-18 | 2010-12-23 | Rehau Ag + Co. | Karosserie-Kunststoffbauteil für ein Kraftfahrzeug |
| DE102009051171A1 (de) * | 2009-10-29 | 2011-05-05 | Merck Patent Gmbh | Pigmente |
| US9603784B2 (en) | 2010-09-30 | 2017-03-28 | Merck Patent Gmbh | Process for treating sol-gel capsules |
| CN102634067B (zh) * | 2012-04-17 | 2013-12-25 | 上海大学 | 光扩散剂、光分散材料及其制备方法 |
| DE102013012023A1 (de) * | 2013-07-19 | 2015-01-22 | Merck Patent Gmbh | Pigmentgemisch |
| WO2015024615A1 (de) * | 2013-08-22 | 2015-02-26 | Merck Patent Gmbh | Diffusionspigmente in der phototherapie |
| WO2016015148A1 (en) | 2014-07-28 | 2016-02-04 | The Royal Institution For The Advancement Of Learning/Mcgill University | Method for producing functionalized nanocrystalline cellulose and functionalized nanocrystalline cellulose thereby produced |
| WO2017075773A1 (en) * | 2015-11-04 | 2017-05-11 | Dow Global Technologies Llc | Polycaprolactone-polyurethane microparticles coated with inorganic metal oxides and methods for the preparation thereof |
| WO2017091893A1 (en) | 2015-11-30 | 2017-06-08 | Anomera Inc. | Cellulose-based organic pigments |
| DE102016004164A1 (de) * | 2016-04-11 | 2017-10-12 | Merck Patent Gmbh | Pigmentgemisch |
| DE102017200921A1 (de) * | 2017-01-20 | 2018-07-26 | Beiersdorf Ag | Kosmetische oder dermatologische Zubereitungen mit einem Gehalt an sphärischen Silicapartikeln, welche mit Titandioxid und Eisenoxiden beschichtet sind und mittelkettigen aliphatischen Diolen |
| KR101876199B1 (ko) * | 2017-04-21 | 2018-08-03 | 씨큐브 주식회사 | 복합 백색 안료 및 그 제조 방법 |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP3018126B2 (ja) * | 1992-02-19 | 2000-03-13 | 花王株式会社 | 複合体質顔料及びこれを含有してなる化粧料 |
| DE4219287A1 (de) * | 1992-06-12 | 1993-12-16 | Merck Patent Gmbh | Anorganische Füllstoffe und organische Matrixmaterialien mit Brechungsindex-Anpassung |
| EP0803550B1 (en) * | 1996-04-22 | 2003-07-09 | MERCK PATENT GmbH | Coated SiO2 particles |
| DE19618569A1 (de) * | 1996-05-09 | 1997-11-13 | Merck Patent Gmbh | Mehrschichtige Interferenzpigmente |
-
1998
- 1998-09-14 DE DE19842134A patent/DE19842134A1/de not_active Withdrawn
-
1999
- 1999-09-13 DE DE59904056T patent/DE59904056D1/de not_active Expired - Lifetime
- 1999-09-13 ES ES99944642T patent/ES2190249T3/es not_active Expired - Lifetime
- 1999-09-13 EP EP99944642A patent/EP1115796B1/de not_active Expired - Lifetime
- 1999-09-13 CN CNB998108561A patent/CN1158358C/zh not_active Expired - Fee Related
- 1999-09-13 JP JP2000570251A patent/JP4137383B2/ja not_active Expired - Lifetime
- 1999-09-13 AU AU57470/99A patent/AU5747099A/en not_active Abandoned
- 1999-09-13 WO PCT/EP1999/006751 patent/WO2000015720A1/de not_active Ceased
Also Published As
| Publication number | Publication date |
|---|---|
| CN1318092A (zh) | 2001-10-17 |
| WO2000015720A1 (de) | 2000-03-23 |
| ES2190249T3 (es) | 2003-07-16 |
| DE19842134A1 (de) | 2000-04-13 |
| JP2002524647A (ja) | 2002-08-06 |
| AU5747099A (en) | 2000-04-03 |
| DE59904056D1 (de) | 2003-02-20 |
| EP1115796A1 (de) | 2001-07-18 |
| CN1158358C (zh) | 2004-07-21 |
| EP1115796B1 (de) | 2003-01-15 |
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