JP2021127282A5 - - Google Patents
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- Publication number
- JP2021127282A5 JP2021127282A5 JP2020024294A JP2020024294A JP2021127282A5 JP 2021127282 A5 JP2021127282 A5 JP 2021127282A5 JP 2020024294 A JP2020024294 A JP 2020024294A JP 2020024294 A JP2020024294 A JP 2020024294A JP 2021127282 A5 JP2021127282 A5 JP 2021127282A5
- Authority
- JP
- Japan
- Prior art keywords
- lithium
- liquid
- containing liquid
- ion exchange
- lithium hydroxide
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- WMFOQBRAJBCJND-UHFFFAOYSA-M Lithium hydroxide Chemical compound [Li+].[OH-] WMFOQBRAJBCJND-UHFFFAOYSA-M 0.000 claims description 66
- KWGKDLIKAYFUFQ-UHFFFAOYSA-M lithium chloride Chemical compound [Li+].[Cl-] KWGKDLIKAYFUFQ-UHFFFAOYSA-M 0.000 claims description 40
- 239000007788 liquid Substances 0.000 claims description 36
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 claims description 18
- 229910052744 lithium Inorganic materials 0.000 claims description 18
- 238000006386 neutralization reaction Methods 0.000 claims description 17
- QHGJSLXSVXVKHZ-UHFFFAOYSA-N dilithium;dioxido(dioxo)manganese Chemical compound [Li+].[Li+].[O-][Mn]([O-])(=O)=O QHGJSLXSVXVKHZ-UHFFFAOYSA-N 0.000 claims description 14
- 238000004519 manufacturing process Methods 0.000 claims description 14
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 claims description 12
- 238000005342 ion exchange Methods 0.000 claims description 12
- 239000003456 ion exchange resin Substances 0.000 claims description 12
- 229920003303 ion-exchange polymer Polymers 0.000 claims description 12
- 238000001179 sorption measurement Methods 0.000 claims description 12
- 239000013522 chelant Substances 0.000 claims description 11
- NBZBKCUXIYYUSX-UHFFFAOYSA-N iminodiacetic acid Chemical compound OC(=O)CNCC(O)=O NBZBKCUXIYYUSX-UHFFFAOYSA-N 0.000 claims description 11
- 239000011347 resin Substances 0.000 claims description 11
- 229920005989 resin Polymers 0.000 claims description 11
- 238000007254 oxidation reaction Methods 0.000 claims description 9
- 238000010828 elution Methods 0.000 claims description 8
- 239000003463 adsorbent Substances 0.000 claims description 7
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 6
- 239000003513 alkali Substances 0.000 claims description 6
- 238000006243 chemical reaction Methods 0.000 claims description 5
- 238000000034 method Methods 0.000 claims description 5
- 230000003647 oxidation Effects 0.000 claims description 5
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 4
- 238000000909 electrodialysis Methods 0.000 claims description 4
- 229910052708 sodium Inorganic materials 0.000 claims description 4
- 239000011734 sodium Substances 0.000 claims description 4
- 125000000524 functional group Chemical group 0.000 claims description 3
- 239000007800 oxidant agent Substances 0.000 claims description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 2
- 150000003839 salts Chemical class 0.000 claims 2
- RSWGJHLUYNHPMX-UHFFFAOYSA-N 1,4a-dimethyl-7-propan-2-yl-2,3,4,4b,5,6,10,10a-octahydrophenanthrene-1-carboxylic acid Chemical compound C12CCC(C(C)C)=CC2=CCC2C1(C)CCCC2(C)C(O)=O RSWGJHLUYNHPMX-UHFFFAOYSA-N 0.000 claims 1
- 229910052748 manganese Inorganic materials 0.000 description 6
- 239000011572 manganese Substances 0.000 description 6
- PWHULOQIROXLJO-UHFFFAOYSA-N Manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 description 4
- 229910052751 metal Inorganic materials 0.000 description 3
- 239000002184 metal Substances 0.000 description 3
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 2
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 description 2
- 229910052791 calcium Inorganic materials 0.000 description 2
- 239000011575 calcium Substances 0.000 description 2
- 150000002500 ions Chemical class 0.000 description 2
- 229910052749 magnesium Inorganic materials 0.000 description 2
- 239000011777 magnesium Substances 0.000 description 2
- 150000002696 manganese Chemical class 0.000 description 2
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 125000004435 hydrogen atom Chemical group [H]* 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- 230000003472 neutralizing effect Effects 0.000 description 1
Priority Applications (8)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2020024294A JP7156322B2 (ja) | 2020-02-17 | 2020-02-17 | 水酸化リチウムの製造方法 |
| US17/797,397 US20230079295A1 (en) | 2020-02-17 | 2021-01-08 | Method for producing lithium hydroxide |
| PCT/JP2021/000466 WO2021166479A1 (ja) | 2020-02-17 | 2021-01-08 | 水酸化リチウムの製造方法 |
| CN202180012969.9A CN115052836B (zh) | 2020-02-17 | 2021-01-08 | 氢氧化锂的制造方法 |
| AU2021222916A AU2021222916B2 (en) | 2020-02-17 | 2021-01-08 | Lithium hydroxide production method |
| EP21756744.5A EP4108633A4 (en) | 2020-02-17 | 2021-01-08 | METHOD FOR PRODUCING LITHIUM HYDROXIDE |
| ARP210100369A AR121327A1 (es) | 2020-02-17 | 2021-02-12 | Método para producir hidróxido de litio |
| CL2022002100A CL2022002100A1 (es) | 2020-02-17 | 2022-08-04 | Método para producir hidróxido de litio |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2020024294A JP7156322B2 (ja) | 2020-02-17 | 2020-02-17 | 水酸化リチウムの製造方法 |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2021127282A JP2021127282A (ja) | 2021-09-02 |
| JP2021127282A5 true JP2021127282A5 (https=) | 2021-11-11 |
| JP7156322B2 JP7156322B2 (ja) | 2022-10-19 |
Family
ID=77391779
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2020024294A Active JP7156322B2 (ja) | 2020-02-17 | 2020-02-17 | 水酸化リチウムの製造方法 |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US20230079295A1 (https=) |
| EP (1) | EP4108633A4 (https=) |
| JP (1) | JP7156322B2 (https=) |
| CN (1) | CN115052836B (https=) |
| AR (1) | AR121327A1 (https=) |
| AU (1) | AU2021222916B2 (https=) |
| CL (1) | CL2022002100A1 (https=) |
| WO (1) | WO2021166479A1 (https=) |
Families Citing this family (18)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20190072667A (ko) | 2016-11-14 | 2019-06-25 | 리락 솔루션즈, 인크. | 코팅된 이온 교환 입자를 이용한 리튬 추출 |
| US11253848B2 (en) | 2017-08-02 | 2022-02-22 | Lilac Solutions, Inc. | Lithium extraction with porous ion exchange beads |
| EP3661620A4 (en) | 2017-08-02 | 2021-05-12 | Lilac Solutions, Inc. | Ion exchange system for lithium extraction |
| AR114412A1 (es) | 2018-02-28 | 2020-09-02 | Lilac Solutions Inc | Reactor de intercambio iónico con trampas de partículas para la extracción de litio |
| JP2023529444A (ja) | 2020-06-09 | 2023-07-10 | ライラック ソリューションズ，インク． | スケール物質存在下におけるリチウム抽出 |
| JP7124917B1 (ja) * | 2021-03-31 | 2022-08-24 | 住友金属鉱山株式会社 | リチウム含有溶液の製造方法 |
| WO2022226219A1 (en) | 2021-04-23 | 2022-10-27 | Lilac Solutions, Inc. | Ion exchange devices for lithium extraction |
| JP7518481B2 (ja) * | 2021-09-30 | 2024-07-18 | 住友金属鉱山株式会社 | 水酸化リチウムの製造方法 |
| JP7698239B2 (ja) * | 2021-10-28 | 2025-06-25 | 住友金属鉱山株式会社 | リチウム含有溶液の製造方法および水酸化リチウムの製造方法 |
| JP2023092624A (ja) * | 2021-12-22 | 2023-07-04 | 住友金属鉱山株式会社 | 水酸化リチウムの製造方法 |
| JPWO2023136195A1 (https=) * | 2022-01-14 | 2023-07-20 | ||
| WO2023192192A1 (en) | 2022-03-28 | 2023-10-05 | Lilac Solutions, Inc. | Lithium extraction enhanced by an alternate phase |
| WO2023192623A2 (en) | 2022-04-01 | 2023-10-05 | Lilac Solutions, Inc. | Extraction of lithium with chemical additives |
| WO2024043228A1 (ja) * | 2022-08-22 | 2024-02-29 | 株式会社アサカ理研 | 水酸化リチウム水溶液の製造方法 |
| JP7713736B2 (ja) * | 2023-06-28 | 2025-07-28 | 株式会社アサカ理研 | リチウム膜電解後の淡塩水の処理方法 |
| WO2025253801A1 (ja) * | 2024-06-06 | 2025-12-11 | 住友化学株式会社 | リチウム塩の製造方法、及びリチウム塩の製造システム |
| CN118634868B (zh) * | 2024-08-15 | 2025-04-04 | 西安金沃泰环保科技有限公司 | 一种离子交换树脂分离重金属离子的方法和装置 |
| CN121044630B (zh) * | 2025-10-31 | 2026-02-24 | 湖南岳阳三湘化工有限公司 | 一种利用回收氯化锰溶液制备工业级碳酸锰的工艺 |
Family Cites Families (25)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP3968678B2 (ja) | 1998-10-26 | 2007-08-29 | オルガノ株式会社 | テトラアルキルアンモニウムイオン含有液の処理方法 |
| CN102016123A (zh) * | 2008-04-22 | 2011-04-13 | 凯米涛弗特公司 | 制备高纯度氢氧化锂和盐酸的方法 |
| JP2009269810A (ja) | 2008-05-07 | 2009-11-19 | Kee:Kk | 高純度水酸化リチウムの製造法 |
| JP2009270188A (ja) | 2008-05-07 | 2009-11-19 | Kee:Kk | 高純度水酸化リチウムの製造方法 |
| JP2012504190A (ja) * | 2008-09-29 | 2012-02-16 | 韓国地質資源研究院 | 分離膜貯留層を用いるリチウム回収装置、これを用いるリチウム回収方法、及びこれを用いるリチウム吸脱着システム |
| JP4723629B2 (ja) * | 2008-11-13 | 2011-07-13 | Ｊｘ日鉱日石金属株式会社 | 陰イオン交換樹脂を用いた銀の回収方法 |
| US9034294B1 (en) * | 2009-04-24 | 2015-05-19 | Simbol, Inc. | Preparation of lithium carbonate from lithium chloride containing brines |
| JP2011032151A (ja) * | 2009-08-04 | 2011-02-17 | Kee:Kk | 炭酸リチウムの水酸化リチウムへの転換方法 |
| WO2012065361A1 (zh) * | 2010-11-19 | 2012-05-24 | 中南大学 | 一种盐湖卤水镁锂分离及富集锂的方法和装置 |
| KR101047986B1 (ko) * | 2010-11-26 | 2011-07-13 | 한국지질자원연구원 | Ｃｃｄ 공정을 이용한 리튬 이온의 흡착/탈착 장치 및 그 방법 |
| AR084006A1 (es) * | 2010-12-01 | 2013-04-17 | Toray Industries | Procedimiento para la separacion y recuperacion de una sal de metal alcalino purificada |
| JP2012121780A (ja) | 2010-12-10 | 2012-06-28 | Sumitomo Metal Mining Co Ltd | 酸化リチウムの製造方法 |
| JPWO2013153692A1 (ja) | 2012-04-13 | 2015-12-17 | 旭化成株式会社 | リチウム回収方法 |
| EP4424408A3 (en) * | 2013-03-15 | 2025-04-09 | Nemaska Lithium Inc. | Processes for preparing lithium hydroxide |
| CN103272554B (zh) * | 2013-06-03 | 2015-08-19 | 长沙矿冶研究院有限责任公司 | 锂锰氧化物型锂吸附剂的制备方法 |
| KR101700684B1 (ko) * | 2015-04-30 | 2017-01-31 | 재단법인 포항산업과학연구원 | 수산화리튬, 및 탄산리튬의 제조 방법 및 그 장치 |
| KR101711854B1 (ko) * | 2015-05-13 | 2017-03-03 | 재단법인 포항산업과학연구원 | 수산화리튬 및 탄산리튬의 제조 방법 |
| CN107298450B (zh) * | 2016-08-31 | 2019-11-29 | 江苏力泰锂能科技有限公司 | 利用可溶性锂盐溶液制备氢氧化锂和碳酸锂的方法 |
| US11253848B2 (en) * | 2017-08-02 | 2022-02-22 | Lilac Solutions, Inc. | Lithium extraction with porous ion exchange beads |
| CN108658101A (zh) * | 2017-08-10 | 2018-10-16 | 青海盐湖工业股份有限公司 | 一种盐湖卤水生产高纯度氯化锂的新工艺 |
| US10648090B2 (en) * | 2018-02-17 | 2020-05-12 | Lilac Solutions, Inc. | Integrated system for lithium extraction and conversion |
| WO2020115948A1 (ja) * | 2018-12-07 | 2020-06-11 | 住友金属鉱山株式会社 | リチウム含有溶液の製造方法 |
| CN110065958B (zh) * | 2019-03-27 | 2022-03-18 | 浙江工业大学 | 一种集成选择性电渗析和选择性双极膜电渗析处理盐湖卤水制备氢氧化锂的方法 |
| CN109850927B (zh) * | 2019-03-29 | 2021-04-20 | 四川顺应动力电池材料有限公司 | 一种制取高纯氢氧化锂的方法 |
| CN110743516A (zh) * | 2019-10-28 | 2020-02-04 | 湖北凯旭企业管理咨询有限公司 | 一种适用于卤水提锂吸附剂的造粒技术 |
-
2020
- 2020-02-17 JP JP2020024294A patent/JP7156322B2/ja active Active
-
2021
- 2021-01-08 US US17/797,397 patent/US20230079295A1/en active Pending
- 2021-01-08 WO PCT/JP2021/000466 patent/WO2021166479A1/ja not_active Ceased
- 2021-01-08 AU AU2021222916A patent/AU2021222916B2/en active Active
- 2021-01-08 EP EP21756744.5A patent/EP4108633A4/en active Pending
- 2021-01-08 CN CN202180012969.9A patent/CN115052836B/zh active Active
- 2021-02-12 AR ARP210100369A patent/AR121327A1/es active IP Right Grant
-
2022
- 2022-08-04 CL CL2022002100A patent/CL2022002100A1/es unknown
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