JP2020073662A - 潤滑剤組成物 - Google Patents
潤滑剤組成物 Download PDFInfo
- Publication number
- JP2020073662A JP2020073662A JP2019228197A JP2019228197A JP2020073662A JP 2020073662 A JP2020073662 A JP 2020073662A JP 2019228197 A JP2019228197 A JP 2019228197A JP 2019228197 A JP2019228197 A JP 2019228197A JP 2020073662 A JP2020073662 A JP 2020073662A
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- Prior art keywords
- solvent
- solvent composition
- oil
- cleaning
- mass
- Prior art date
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- Granted
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- 239000000203 mixture Substances 0.000 title claims abstract description 184
- 239000000314 lubricant Substances 0.000 title description 55
- 239000002904 solvent Substances 0.000 claims abstract description 239
- 238000004140 cleaning Methods 0.000 claims abstract description 88
- 239000003381 stabilizer Substances 0.000 claims abstract description 41
- 238000009835 boiling Methods 0.000 claims abstract description 21
- LDTMPQQAWUMPKS-UPHRSURJSA-N (z)-1-chloro-3,3,3-trifluoroprop-1-ene Chemical compound FC(F)(F)\C=C/Cl LDTMPQQAWUMPKS-UPHRSURJSA-N 0.000 claims abstract description 6
- 239000011248 coating agent Substances 0.000 claims description 58
- 238000000576 coating method Methods 0.000 claims description 56
- 238000000034 method Methods 0.000 claims description 52
- 239000003921 oil Substances 0.000 claims description 30
- 239000012855 volatile organic compound Substances 0.000 claims description 17
- 239000010730 cutting oil Substances 0.000 claims description 13
- 238000012545 processing Methods 0.000 claims description 8
- OHMHBGPWCHTMQE-UHFFFAOYSA-N 2,2-dichloro-1,1,1-trifluoroethane Chemical class FC(F)(F)C(Cl)Cl OHMHBGPWCHTMQE-UHFFFAOYSA-N 0.000 claims description 5
- UJIGKESMIPTWJH-UHFFFAOYSA-N 1,3-dichloro-1,1,2,2,3-pentafluoropropane Chemical compound FC(Cl)C(F)(F)C(F)(F)Cl UJIGKESMIPTWJH-UHFFFAOYSA-N 0.000 claims description 3
- VRVIDSRWPUGFBU-UHFFFAOYSA-N 2-chloro-1,1,1-trifluoropropane Chemical group CC(Cl)C(F)(F)F VRVIDSRWPUGFBU-UHFFFAOYSA-N 0.000 claims description 3
- ZPIFKCVYZBVZIV-UHFFFAOYSA-N 3-chloro-1,1,1-trifluoropropane Chemical compound FC(F)(F)CCCl ZPIFKCVYZBVZIV-UHFFFAOYSA-N 0.000 claims description 3
- 239000010687 lubricating oil Substances 0.000 claims description 3
- 239000010721 machine oil Substances 0.000 claims description 3
- 238000004080 punching Methods 0.000 claims description 3
- 238000010791 quenching Methods 0.000 claims description 3
- 230000000171 quenching effect Effects 0.000 claims description 3
- 239000010731 rolling oil Substances 0.000 claims description 3
- 229910052751 metal Inorganic materials 0.000 abstract description 29
- 239000002184 metal Substances 0.000 abstract description 29
- 239000000243 solution Substances 0.000 abstract description 15
- 230000007797 corrosion Effects 0.000 abstract description 13
- 238000005260 corrosion Methods 0.000 abstract description 13
- 230000002411 adverse Effects 0.000 abstract description 12
- 238000001035 drying Methods 0.000 abstract description 10
- 150000002739 metals Chemical class 0.000 abstract description 10
- 239000000126 substance Substances 0.000 abstract description 10
- 229920003023 plastic Polymers 0.000 abstract description 8
- 239000004033 plastic Substances 0.000 abstract description 8
- 229920001971 elastomer Polymers 0.000 abstract description 7
- 239000000806 elastomer Substances 0.000 abstract description 7
- 239000000463 material Substances 0.000 abstract description 7
- 238000010790 dilution Methods 0.000 abstract description 5
- 239000012895 dilution Substances 0.000 abstract description 5
- 231100000989 no adverse effect Toxicity 0.000 abstract description 3
- 238000012360 testing method Methods 0.000 description 23
- -1 chlorine radicals Chemical class 0.000 description 19
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 19
- 238000011156 evaluation Methods 0.000 description 15
- 150000001875 compounds Chemical class 0.000 description 13
- 239000000047 product Substances 0.000 description 12
- 125000004432 carbon atom Chemical group C* 0.000 description 11
- 230000000694 effects Effects 0.000 description 11
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 10
- CBENFWSGALASAD-UHFFFAOYSA-N Ozone Chemical compound [O-][O+]=O CBENFWSGALASAD-UHFFFAOYSA-N 0.000 description 10
- 238000000354 decomposition reaction Methods 0.000 description 10
- 238000005108 dry cleaning Methods 0.000 description 10
- 238000005406 washing Methods 0.000 description 10
- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 description 9
- 238000004821 distillation Methods 0.000 description 9
- 229910052731 fluorine Inorganic materials 0.000 description 9
- 239000003795 chemical substances by application Substances 0.000 description 8
- 239000007788 liquid Substances 0.000 description 8
- 238000000926 separation method Methods 0.000 description 8
- 239000000344 soap Substances 0.000 description 8
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 description 7
- 229910052801 chlorine Inorganic materials 0.000 description 7
- 230000000052 comparative effect Effects 0.000 description 7
- 238000001816 cooling Methods 0.000 description 7
- 235000014113 dietary fatty acids Nutrition 0.000 description 7
- 150000002148 esters Chemical class 0.000 description 7
- 229930195729 fatty acid Natural products 0.000 description 7
- 239000000194 fatty acid Substances 0.000 description 7
- 239000011737 fluorine Substances 0.000 description 7
- 229920001296 polysiloxane Polymers 0.000 description 7
- ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-Butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 description 6
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 6
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 description 6
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 6
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 6
- IMNFDUFMRHMDMM-UHFFFAOYSA-N N-Heptane Chemical compound CCCCCCC IMNFDUFMRHMDMM-UHFFFAOYSA-N 0.000 description 6
- 239000000460 chlorine Substances 0.000 description 6
- 125000004122 cyclic group Chemical group 0.000 description 6
- 238000007865 diluting Methods 0.000 description 6
- 239000011521 glass Substances 0.000 description 6
- 150000002576 ketones Chemical class 0.000 description 6
- 239000004215 Carbon black (E152) Substances 0.000 description 5
- 239000007795 chemical reaction product Substances 0.000 description 5
- NEHMKBQYUWJMIP-UHFFFAOYSA-N chloromethane Chemical compound ClC NEHMKBQYUWJMIP-UHFFFAOYSA-N 0.000 description 5
- 229930195733 hydrocarbon Natural products 0.000 description 5
- 150000002430 hydrocarbons Chemical class 0.000 description 5
- JEIPFZHSYJVQDO-UHFFFAOYSA-N iron(III) oxide Inorganic materials O=[Fe]O[Fe]=O JEIPFZHSYJVQDO-UHFFFAOYSA-N 0.000 description 5
- 229920006395 saturated elastomer Polymers 0.000 description 5
- LDTMPQQAWUMPKS-OWOJBTEDSA-N (e)-1-chloro-3,3,3-trifluoroprop-1-ene Chemical compound FC(F)(F)\C=C\Cl LDTMPQQAWUMPKS-OWOJBTEDSA-N 0.000 description 4
- JVSWJIKNEAIKJW-UHFFFAOYSA-N 2-Methylheptane Chemical compound CCCCCC(C)C JVSWJIKNEAIKJW-UHFFFAOYSA-N 0.000 description 4
- RGSFGYAAUTVSQA-UHFFFAOYSA-N Cyclopentane Chemical compound C1CCCC1 RGSFGYAAUTVSQA-UHFFFAOYSA-N 0.000 description 4
- OFBQJSOFQDEBGM-UHFFFAOYSA-N Pentane Chemical compound CCCCC OFBQJSOFQDEBGM-UHFFFAOYSA-N 0.000 description 4
- 230000015572 biosynthetic process Effects 0.000 description 4
- 239000000919 ceramic Substances 0.000 description 4
- 238000001704 evaporation Methods 0.000 description 4
- 238000004519 manufacturing process Methods 0.000 description 4
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 4
- ZWRUINPWMLAQRD-UHFFFAOYSA-N nonan-1-ol Chemical compound CCCCCCCCCO ZWRUINPWMLAQRD-UHFFFAOYSA-N 0.000 description 4
- 230000003287 optical effect Effects 0.000 description 4
- 238000001139 pH measurement Methods 0.000 description 4
- 238000002360 preparation method Methods 0.000 description 4
- 230000003449 preventive effect Effects 0.000 description 4
- 238000013020 steam cleaning Methods 0.000 description 4
- 238000003860 storage Methods 0.000 description 4
- 238000010792 warming Methods 0.000 description 4
- XJSRKJAHJGCPGC-UHFFFAOYSA-N 1,1,1,2,2,3,3,4,4,5,5,6,6-tridecafluorohexane Chemical compound FC(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)F XJSRKJAHJGCPGC-UHFFFAOYSA-N 0.000 description 3
- OKIYQFLILPKULA-UHFFFAOYSA-N 1,1,1,2,2,3,3,4,4-nonafluoro-4-methoxybutane Chemical compound COC(F)(F)C(F)(F)C(F)(F)C(F)(F)F OKIYQFLILPKULA-UHFFFAOYSA-N 0.000 description 3
- RIQRGMUSBYGDBL-UHFFFAOYSA-N 1,1,1,2,2,3,4,5,5,5-decafluoropentane Chemical compound FC(F)(F)C(F)C(F)C(F)(F)C(F)(F)F RIQRGMUSBYGDBL-UHFFFAOYSA-N 0.000 description 3
- CWIFAKBLLXGZIC-UHFFFAOYSA-N 1,1,2,2-tetrafluoro-1-(2,2,2-trifluoroethoxy)ethane Chemical compound FC(F)C(F)(F)OCC(F)(F)F CWIFAKBLLXGZIC-UHFFFAOYSA-N 0.000 description 3
- UBOXGVDOUJQMTN-UHFFFAOYSA-N 1,1,2-trichloroethane Chemical compound ClCC(Cl)Cl UBOXGVDOUJQMTN-UHFFFAOYSA-N 0.000 description 3
- QPRQEDXDYOZYLA-UHFFFAOYSA-N 2-methylbutan-1-ol Chemical compound CCC(C)CO QPRQEDXDYOZYLA-UHFFFAOYSA-N 0.000 description 3
- COAUHYBSXMIJDK-UHFFFAOYSA-N 3,3-dichloro-1,1,1,2,2-pentafluoropropane Chemical compound FC(F)(F)C(F)(F)C(Cl)Cl COAUHYBSXMIJDK-UHFFFAOYSA-N 0.000 description 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 3
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 description 3
- KDLHZDBZIXYQEI-UHFFFAOYSA-N Palladium Chemical compound [Pd] KDLHZDBZIXYQEI-UHFFFAOYSA-N 0.000 description 3
- XBDQKXXYIPTUBI-UHFFFAOYSA-M Propionate Chemical compound CCC([O-])=O XBDQKXXYIPTUBI-UHFFFAOYSA-M 0.000 description 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- DKGAVHZHDRPRBM-UHFFFAOYSA-N Tert-Butanol Chemical compound CC(C)(C)O DKGAVHZHDRPRBM-UHFFFAOYSA-N 0.000 description 3
- ZMANZCXQSJIPKH-UHFFFAOYSA-N Triethylamine Chemical compound CCN(CC)CC ZMANZCXQSJIPKH-UHFFFAOYSA-N 0.000 description 3
- 230000003373 anti-fouling effect Effects 0.000 description 3
- 239000012298 atmosphere Substances 0.000 description 3
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 3
- 229910052799 carbon Inorganic materials 0.000 description 3
- 125000001309 chloro group Chemical group Cl* 0.000 description 3
- 125000001153 fluoro group Chemical group F* 0.000 description 3
- 239000007789 gas Substances 0.000 description 3
- 238000007654 immersion Methods 0.000 description 3
- 238000002156 mixing Methods 0.000 description 3
- TVMXDCGIABBOFY-UHFFFAOYSA-N octane Chemical compound CCCCCCCC TVMXDCGIABBOFY-UHFFFAOYSA-N 0.000 description 3
- 150000002894 organic compounds Chemical class 0.000 description 3
- 239000001301 oxygen Substances 0.000 description 3
- 229910052760 oxygen Inorganic materials 0.000 description 3
- 238000000746 purification Methods 0.000 description 3
- 230000008929 regeneration Effects 0.000 description 3
- 238000011069 regeneration method Methods 0.000 description 3
- 238000003786 synthesis reaction Methods 0.000 description 3
- CXWXQJXEFPUFDZ-UHFFFAOYSA-N tetralin Chemical compound C1=CC=C2CCCCC2=C1 CXWXQJXEFPUFDZ-UHFFFAOYSA-N 0.000 description 3
- GRWFGVWFFZKLTI-IUCAKERBSA-N (-)-α-pinene Chemical compound CC1=CC[C@@H]2C(C)(C)[C@H]1C2 GRWFGVWFFZKLTI-IUCAKERBSA-N 0.000 description 2
- RTGGFPLAKRCINA-UHFFFAOYSA-N 1,1,1,2,2,3,3,4,4-nonafluorohexane Chemical compound CCC(F)(F)C(F)(F)C(F)(F)C(F)(F)F RTGGFPLAKRCINA-UHFFFAOYSA-N 0.000 description 2
- KDWQLICBSFIDRM-UHFFFAOYSA-N 1,1,1-trifluoropropane Chemical compound CCC(F)(F)F KDWQLICBSFIDRM-UHFFFAOYSA-N 0.000 description 2
- QPFMBZIOSGYJDE-UHFFFAOYSA-N 1,1,2,2-tetrachloroethane Chemical compound ClC(Cl)C(Cl)Cl QPFMBZIOSGYJDE-UHFFFAOYSA-N 0.000 description 2
- FRCHKSNAZZFGCA-UHFFFAOYSA-N 1,1-dichloro-1-fluoroethane Chemical compound CC(F)(Cl)Cl FRCHKSNAZZFGCA-UHFFFAOYSA-N 0.000 description 2
- NDKGUMMLYBINOC-UHFFFAOYSA-N 1,2-dichloro-1-fluoroethane Chemical compound FC(Cl)CCl NDKGUMMLYBINOC-UHFFFAOYSA-N 0.000 description 2
- KBPLFHHGFOOTCA-UHFFFAOYSA-N 1-Octanol Chemical compound CCCCCCCCO KBPLFHHGFOOTCA-UHFFFAOYSA-N 0.000 description 2
- VEZJSKSPVQQGIS-UHFFFAOYSA-N 1-chloro-2-fluoroethane Chemical compound FCCCl VEZJSKSPVQQGIS-UHFFFAOYSA-N 0.000 description 2
- AFFLGGQVNFXPEV-UHFFFAOYSA-N 1-decene Chemical compound CCCCCCCCC=C AFFLGGQVNFXPEV-UHFFFAOYSA-N 0.000 description 2
- BBMCTIGTTCKYKF-UHFFFAOYSA-N 1-heptanol Chemical compound CCCCCCCO BBMCTIGTTCKYKF-UHFFFAOYSA-N 0.000 description 2
- LIKMAJRDDDTEIG-UHFFFAOYSA-N 1-hexene Chemical compound CCCCC=C LIKMAJRDDDTEIG-UHFFFAOYSA-N 0.000 description 2
- JRZJOMJEPLMPRA-UHFFFAOYSA-N 1-nonene Chemical compound CCCCCCCC=C JRZJOMJEPLMPRA-UHFFFAOYSA-N 0.000 description 2
- KWKAKUADMBZCLK-UHFFFAOYSA-N 1-octene Chemical compound CCCCCCC=C KWKAKUADMBZCLK-UHFFFAOYSA-N 0.000 description 2
- HNRMPXKDFBEGFZ-UHFFFAOYSA-N 2,2-dimethylbutane Chemical compound CCC(C)(C)C HNRMPXKDFBEGFZ-UHFFFAOYSA-N 0.000 description 2
- FLTJDUOFAQWHDF-UHFFFAOYSA-N 2,2-dimethylhexane Chemical compound CCCCC(C)(C)C FLTJDUOFAQWHDF-UHFFFAOYSA-N 0.000 description 2
- UHUGFVKSZJCZEY-UHFFFAOYSA-N 2,3,3-trichloro-1,1,1-trifluoropropane Chemical compound FC(F)(F)C(Cl)C(Cl)Cl UHUGFVKSZJCZEY-UHFFFAOYSA-N 0.000 description 2
- ZFFMLCVRJBZUDZ-UHFFFAOYSA-N 2,3-dimethylbutane Chemical compound CC(C)C(C)C ZFFMLCVRJBZUDZ-UHFFFAOYSA-N 0.000 description 2
- BZHMBWZPUJHVEE-UHFFFAOYSA-N 2,4-dimethylpentane Chemical compound CC(C)CC(C)C BZHMBWZPUJHVEE-UHFFFAOYSA-N 0.000 description 2
- UWNADWZGEHDQAB-UHFFFAOYSA-N 2,5-dimethylhexane Chemical compound CC(C)CCC(C)C UWNADWZGEHDQAB-UHFFFAOYSA-N 0.000 description 2
- OJVAMHKKJGICOG-UHFFFAOYSA-N 2,5-hexanedione Chemical compound CC(=O)CCC(C)=O OJVAMHKKJGICOG-UHFFFAOYSA-N 0.000 description 2
- AFABGHUZZDYHJO-UHFFFAOYSA-N 2-Methylpentane Chemical compound CCCC(C)C AFABGHUZZDYHJO-UHFFFAOYSA-N 0.000 description 2
- RXGUIWHIADMCFC-UHFFFAOYSA-N 2-Methylpropyl 2-methylpropionate Chemical compound CC(C)COC(=O)C(C)C RXGUIWHIADMCFC-UHFFFAOYSA-N 0.000 description 2
- QQZOPKMRPOGIEB-UHFFFAOYSA-N 2-Oxohexane Chemical compound CCCCC(C)=O QQZOPKMRPOGIEB-UHFFFAOYSA-N 0.000 description 2
- JYNCTFQDWJMJDI-UHFFFAOYSA-N 2-chloro-1,1,1,3,3-pentafluoropropane Chemical compound FC(F)C(Cl)C(F)(F)F JYNCTFQDWJMJDI-UHFFFAOYSA-N 0.000 description 2
- CETWDUZRCINIHU-UHFFFAOYSA-N 2-heptanol Chemical compound CCCCCC(C)O CETWDUZRCINIHU-UHFFFAOYSA-N 0.000 description 2
- PFNHSEQQEPMLNI-UHFFFAOYSA-N 2-methyl-1-pentanol Chemical compound CCCC(C)CO PFNHSEQQEPMLNI-UHFFFAOYSA-N 0.000 description 2
- GXDHCNNESPLIKD-UHFFFAOYSA-N 2-methylhexane Chemical compound CCCCC(C)C GXDHCNNESPLIKD-UHFFFAOYSA-N 0.000 description 2
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- PLTIOZOVDUUXDQ-UHFFFAOYSA-N 3,3-dichloro-1,1,1-trifluoropropane Chemical compound FC(F)(F)CC(Cl)Cl PLTIOZOVDUUXDQ-UHFFFAOYSA-N 0.000 description 2
- KUMXLFIBWFCMOJ-UHFFFAOYSA-N 3,3-dimethylhexane Chemical compound CCCC(C)(C)CC KUMXLFIBWFCMOJ-UHFFFAOYSA-N 0.000 description 2
- LAIUFBWHERIJIH-UHFFFAOYSA-N 3-Methylheptane Chemical compound CCCCC(C)CC LAIUFBWHERIJIH-UHFFFAOYSA-N 0.000 description 2
- DUPUVYJQZSLSJB-UHFFFAOYSA-N 3-ethyl-2-methylpentane Chemical compound CCC(CC)C(C)C DUPUVYJQZSLSJB-UHFFFAOYSA-N 0.000 description 2
- MXLMTQWGSQIYOW-UHFFFAOYSA-N 3-methyl-2-butanol Chemical compound CC(C)C(C)O MXLMTQWGSQIYOW-UHFFFAOYSA-N 0.000 description 2
- HTSABYAWKQAHBT-UHFFFAOYSA-N 3-methylcyclohexanol Chemical compound CC1CCCC(O)C1 HTSABYAWKQAHBT-UHFFFAOYSA-N 0.000 description 2
- VLJXXKKOSFGPHI-UHFFFAOYSA-N 3-methylhexane Chemical compound CCCC(C)CC VLJXXKKOSFGPHI-UHFFFAOYSA-N 0.000 description 2
- YEJRWHAVMIAJKC-UHFFFAOYSA-N 4-Butyrolactone Chemical compound O=C1CCCO1 YEJRWHAVMIAJKC-UHFFFAOYSA-N 0.000 description 2
- HCFAJYNVAYBARA-UHFFFAOYSA-N 4-heptanone Chemical compound CCCC(=O)CCC HCFAJYNVAYBARA-UHFFFAOYSA-N 0.000 description 2
- MQWCXKGKQLNYQG-UHFFFAOYSA-N 4-methylcyclohexan-1-ol Chemical compound CC1CCC(O)CC1 MQWCXKGKQLNYQG-UHFFFAOYSA-N 0.000 description 2
- CHBAWFGIXDBEBT-UHFFFAOYSA-N 4-methylheptane Chemical compound CCCC(C)CCC CHBAWFGIXDBEBT-UHFFFAOYSA-N 0.000 description 2
- KWOLFJPFCHCOCG-UHFFFAOYSA-N Acetophenone Chemical compound CC(=O)C1=CC=CC=C1 KWOLFJPFCHCOCG-UHFFFAOYSA-N 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical group [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- XDTMQSROBMDMFD-UHFFFAOYSA-N Cyclohexane Chemical compound C1CCCCC1 XDTMQSROBMDMFD-UHFFFAOYSA-N 0.000 description 2
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- NIQCNGHVCWTJSM-UHFFFAOYSA-N Dimethyl phthalate Chemical compound COC(=O)C1=CC=CC=C1C(=O)OC NIQCNGHVCWTJSM-UHFFFAOYSA-N 0.000 description 2
- RZKSECIXORKHQS-UHFFFAOYSA-N Heptan-3-ol Chemical compound CCCCC(O)CC RZKSECIXORKHQS-UHFFFAOYSA-N 0.000 description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
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- JKRZOJADNVOXPM-UHFFFAOYSA-N Oxalic acid dibutyl ester Chemical compound CCCCOC(=O)C(=O)OCCCC JKRZOJADNVOXPM-UHFFFAOYSA-N 0.000 description 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 2
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- KXKVLQRXCPHEJC-UHFFFAOYSA-N acetic acid trimethyl ester Natural products COC(C)=O KXKVLQRXCPHEJC-UHFFFAOYSA-N 0.000 description 2
- YRKCREAYFQTBPV-UHFFFAOYSA-N acetylacetone Chemical compound CC(=O)CC(C)=O YRKCREAYFQTBPV-UHFFFAOYSA-N 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- XXROGKLTLUQVRX-UHFFFAOYSA-N allyl alcohol Chemical compound OCC=C XXROGKLTLUQVRX-UHFFFAOYSA-N 0.000 description 2
- 229910052782 aluminium Inorganic materials 0.000 description 2
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 2
- 239000002280 amphoteric surfactant Substances 0.000 description 2
- 239000003945 anionic surfactant Substances 0.000 description 2
- QUKGYYKBILRGFE-UHFFFAOYSA-N benzyl acetate Chemical compound CC(=O)OCC1=CC=CC=C1 QUKGYYKBILRGFE-UHFFFAOYSA-N 0.000 description 2
- SESFRYSPDFLNCH-UHFFFAOYSA-N benzyl benzoate Chemical compound C=1C=CC=CC=1C(=O)OCC1=CC=CC=C1 SESFRYSPDFLNCH-UHFFFAOYSA-N 0.000 description 2
- BTANRVKWQNVYAZ-UHFFFAOYSA-N butan-2-ol Chemical compound CCC(C)O BTANRVKWQNVYAZ-UHFFFAOYSA-N 0.000 description 2
- XSIFPSYPOVKYCO-UHFFFAOYSA-N butyl benzoate Chemical compound CCCCOC(=O)C1=CC=CC=C1 XSIFPSYPOVKYCO-UHFFFAOYSA-N 0.000 description 2
- XUPYJHCZDLZNFP-UHFFFAOYSA-N butyl butanoate Chemical compound CCCCOC(=O)CCC XUPYJHCZDLZNFP-UHFFFAOYSA-N 0.000 description 2
- NMJJFJNHVMGPGM-UHFFFAOYSA-N butyl formate Chemical compound CCCCOC=O NMJJFJNHVMGPGM-UHFFFAOYSA-N 0.000 description 2
- 239000003054 catalyst Substances 0.000 description 2
- 239000003093 cationic surfactant Substances 0.000 description 2
- 230000008859 change Effects 0.000 description 2
- 150000008280 chlorinated hydrocarbons Chemical class 0.000 description 2
- JHIVVAPYMSGYDF-UHFFFAOYSA-N cyclohexanone Chemical compound O=C1CCCCC1 JHIVVAPYMSGYDF-UHFFFAOYSA-N 0.000 description 2
- HGCIXCUEYOPUTN-UHFFFAOYSA-N cyclohexene Chemical compound C1CCC=CC1 HGCIXCUEYOPUTN-UHFFFAOYSA-N 0.000 description 2
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Abstract
Description
なお、本明細書においては、特に断りのない限り飽和のハイドロクロロフルオロカーボンをHCFCといい、HCFOとは区別して用いる。また、HCFCを飽和のハイドロクロロフルオロカーボンのように明記する場合もある。また、本明細書において、ハロゲン化炭化水素については、化合物名の後の括弧内にその化合物の略称を記し、必要に応じて化合物名に代えてその略称を用いる。また、幾何異性体を有する化合物の略称に付けられた(E)は、E体(トランス体)を示し、(Z)はZ体(シス体)を示す。該化合物の名称、略称において、E体、Z体の明記がない場合、該名称、略称は、E体、Z体、およびE体とZ体の混合物を含む総称を意味する。
[2]前記溶剤の含有量に対する、前記安定剤の含有量の割合が1質量ppm〜1質量%である、[1]に記載の溶剤組成物。
[3]前記1233zd(Z)の含有量に対する前記安定剤の含有量の割合が1質量ppm〜1質量%である、[1]または[2]に記載の溶剤組成物。
[4]前記溶剤全量に対する前記1233zd(Z)の含有量の割合が、80〜100質量%である、[1]〜[3]のいずれかに記載の溶剤組成物。
[5]前記常圧における沸点が30℃以上60℃以下の飽和のHCFCが、2−クロロ−3,3,3−トリフルオロプロパン(CF3−CHCl−CH3、HCFC−253db、以下「253db」ともいう。)、1−クロロ−3,3,3−トリフルオロプロパン(CF3−CH2−CH2Cl、HCFC−253fb、以下「253fb」ともいう。)、1,1−ジクロロ−2,2,3,3,3−ペンタフルオロプロパン(CF3−CF2−CHCl2、HCFC−225ca、以下「225ca」ともいう。)および1,3−ジクロロ−1,1,2,2,3−ペンタフルオロプロパン(CClF2−CF2−CClFHH、HCFC−225cb、以下「225cb」ともいう。)からなる群より選ばれる1種以上である、[1]〜[4]のいずれかに記載の溶剤組成物。
[7]前記被洗浄物品に付着した加工油を洗浄する、[6]に記載の洗浄方法。
[8]前記加工油が、切削油、焼き入れ油、圧延油、潤滑油、機械油、プレス加工油、打ち抜き油、引き抜き油、組立油および線引き油からなる群より選ばれる1種以上である、[7]に記載の洗浄方法。
[9]前記被洗浄物品が衣類である、[6]に記載の洗浄方法。
[10]前記[1]〜[5]のいずれかに記載の溶剤組成物に不揮発性有機化合物を溶解させて塗膜形成用組成物を作製し、該塗膜形成用組成物を被塗布物上に塗布した後、前記溶剤組成物を蒸発させて、前記不揮発性有機化合物からなる塗膜を形成することを特徴とする、塗膜の形成方法。
本発明の溶剤組成物は、以下の溶剤(A)および安定剤(B)を含有する。
溶剤(A):1233zd(Z)を含む溶剤
安定剤(B):常圧における沸点が30〜60℃のHCFCからなる安定剤
なお、本明細書において「常圧」とは760mmHgである。また、特に断りのない限り本明細書における「沸点」は、常圧における沸点である。
本発明の溶剤組成物は、1233zd(Z)を含有する溶剤(A)を含有する。溶剤(A)は1233zd(Z)のみで構成されてもよく、1233zd(Z)の有する上記特徴を害しない範囲で、溶質となる各種の物質の溶解性を高める、揮発速度を調節する等の目的に応じて、1233zd(Z)以外の溶剤(以下「溶剤(a1)」という。)を含有していてもよい。
本発明の溶剤組成物は、安定剤(B)として、常圧における沸点が30〜60℃のHCFCからなる安定剤を含む。本発明における安定剤とは、1233zd(Z)の酸素による分解を抑制する能力を有する化合物をいう。
HCFCとは、分子内に塩素原子、フッ素原子、水素原子および炭素原子をそれぞれ少なくとも一つ以上有する飽和化合物であり、下記一般式(1)で表わすことができる。
CwHxClyFz ……(1)
(但し、上記式中、x、y、z、wはいずれも整数であり、w≧1、x≧1、y≧1、z≧1、x+y+z=2w+2を満たす数である。)
本発明の洗浄方法は、上記本発明の溶剤組成物によって被洗浄物品に付着された付着物を洗浄する方法であり、本発明の溶剤組成物と被洗浄物品とを接触させることを特徴とする。
次に、本発明の溶剤組成物を、各種衣類の汚れの除去洗浄に用いる場合について説明する。
本発明の溶剤組成物は、不揮発性有機化合物の希釈塗付用の溶剤(希釈塗布溶剤)に使用できる。すなわち本発明の塗膜の形成方法は、上記本発明の溶剤組成物に不揮発性有機化合物を溶解させて塗膜形成用組成物を作製し、該塗膜形成用組成物を被塗布物上に塗布した後、前記溶剤組成物を蒸発させて、前記不揮発性有機化合物からなる塗膜を形成することを特徴とする。
(1233zd(Z)の合成)
国際公開2014/175403号の実施例3の方法により得られた蒸留後釜残分をさらに蒸留精製することで、純度99.9質量%の1233zd(Z)を含む組成物(以下「1233zd(Z)組成物」という。)を得る。すなわち、テトラn−ブチルアンモニウムクロリド(TBAC)の存在下、243faと243fbを含み、243faと243fbの合計に対して243fbが5モル%以下である原料組成物に水酸化ナトリウムを加えて反応生成物を得、これを蒸留精製して1233zd(Z)組成物を得る。1233zd(Z)組成物中の、1233zd(Z)以外の0.1質量%の成分は(E)−1−クロロ−3,3,3−トリフルオロ−1−プロペン(1233zd(E))である。
US公開2015−0045590のExample5 StepA、StepB記載の方法で253fbを含む粗液を得、さらに蒸留精製することで、純度100.0質量%の253fbを得る。すなわち、2質量%のパラジウム(Pd)を担持させたカーボン(C)触媒の存在下、3,3,3−トリフルオロプロペンと水素を反応させて3,3,3−トリフルオロプロパンを得る。該3,3,3−トリフルオロプロパンと塩素を加熱下で反応させて、253fbを含む粗液を得、これを蒸留精製することで、純度100.0質量%の253fbを得る。
非特許文献Journal of OrganicChemistry 1989, Vol54, No6, p1433に記載の方法で純度100.0質量%の253dbを得る。すなわち、トリエチルアミン存在下ジクロロメタン中で希釈した1,1,1−トリフルオロ−2−プロパノールとノナフルオロブタンスルホン酸フロリドを反応させて、1,1,1−トリフルオロイソプロピルノナフレートを得る。該1,1,1−トリフルオロイソプロピルノナフレートをアセトルアセトン中リチウムクロライドと反応させて、253dbを含む粗液を得、これを蒸留精製することで、純度100.0質量%の253dbを得る。
旭硝子社製、アサヒクリンAK−225(商品名、225caおよび225cbの混合物)を蒸留精製することで純度100.0%の225caおよび225cbをそれぞれ得る。
上記それぞれの純度が100.0%である225caと225cbを同質量混合することで、225caの50.0質量%と225cbの50.0質量%からなる225ca/cb混合品を得る。
1233zd(Z)組成物に、溶剤組成物とした際に表1に示す質量割合となるように安定剤(B)を添加して、例1〜35の溶剤組成物を51kgずつ調製する。また、表1に示す、HCFO−1233zd(Z)組成物は含有するが安定剤(B)を含有しない例36の溶剤組成物を51kg調製する。なお、表1に示す安定剤(B)の質量割合(質量ppm)は、溶剤組成物中の1233zd(Z)の含有量に対する安定剤(B)の含有量の質量割合である。
1.安定性試験・金属耐食試験
上記例1〜36の溶剤組成物の100gを、一般用冷間圧延鋼板(SPCC)の試験片を入れた耐熱ガラス瓶に入れ、HCFO−1233zd(Z)の沸点(40℃)で7日間保存する。調製直後と7日間保存後のpHを測定し、また7日間保存後(試験後)のSPCC表面の外観観察を行う。評価結果を表1に示す。
各例の溶剤組成物40gとpH7に調製した40gの純水とを、200ml容分液漏斗に入れ、1分間振盪する。その後、静置して2層分離した上層の水層を分取し、その水層のpHをpHメーター(型番:HM−30R、東亜ディーケーケー株式会社製)で測定する。
A:光沢が失われる。
B:表面がわずかに錆びている。
×:表面の全面に錆びが認められる。
上記例1〜36を図1に示すのと同様な洗浄装置10に適用して洗浄試験を行う。洗浄装置10の洗浄槽1、リンス槽2、蒸気発生槽3に例1〜36の溶剤組成物の50kgを入れて、それぞれ300時間循環運転する。運転開始前(初期)、運転開始後10時間、100時間、300時間後に蒸気発生槽3、洗浄槽1、水分離槽5の溶剤を100g採取し、塩素イオン濃度とpHを下記方法で測定する。結果を表2、3に示す。表2、3において、槽3とは蒸気発生槽3を、槽1とは洗浄槽1を、槽5とは水分離槽5をそれぞれ意味する。
採取して得られる溶剤組成物40gとpH7に調製した40gの純水とを、200mL容分液漏斗に入れ、1分間振盪する。その後、静置して2層分離した上層の水層を分取し、その水層のpHを上記同様のpHメーターで測定する。
採取して得られる溶剤組成物50gを100mLのサンプル瓶に入れた後、50gのイオン交換水を加えて、30秒間手で振り混ぜることにより、溶剤組成物中に含まれる塩素イオンをイオン交換水中に抽出する。静置してイオン交換水を分離後、イオン交換水中に含まれる塩素イオン濃度(ppm)をイオンクロマトグラフィー(ICS−1000、日本ダイオネクス社製)により測定する。
上記の例1〜35(実施例)および例36(比較例)の溶剤組成物をさらに作製し、以下の各洗浄試験を行う。
ステンレス鋼SUS304の試験片(25mm×30mm×2mm)を、切削油である製品名「ダフニーマーグプラスHT−10」(出光興産株式会社製)中に浸漬した後、各例の溶剤組成物50mL中に1分間浸漬し、引き上げて切削油が除去された度合を観察する。洗浄性の評価は以下の基準で行う。
「S(優良)」:切削油が完全に除去される。
「A(良好)」:切削油がほぼ除去される。
「B(やや不良)」:切削油が微量に残存する。
「×(不良)」:切削油がかなり残存する。
切削油として製品名「ダフニーマーグプラスAM20」(出光興産株式会社製)を使用する以外は洗浄試験Aと同様に試験し、同じ基準で洗浄性を評価する。
切削油として製品名「ダフニーマーグプラスHM25」(出光興産株式会社製)を使用する以外は洗浄試験Aと同様に試験し、同じ基準で洗浄性を評価する。
切削油として製品名「G−6318FK」(日本工作油株式会社製)を使用する以外は洗浄試験Aと同様に試験し、同じ基準で洗浄性を評価する。
上記の例1〜35(実施例)および例36(比較例)の溶剤組成物をさらに作製し、各溶剤組成物とフッ素系潤滑剤である製品名「クライトックス(登録商標)GPL102」(デュポン株式会社製、フッ素系オイル)を混合し、該フッ素系潤滑剤の含有量の割合が溶液全量に対して0.5質量%である潤滑剤溶液を調製する。
(溶解状態)
各例の溶剤組成物を用いた潤滑剤溶液の溶解状態を目視で確認し、以下の基準で評価する。
「S(優良)」:直ちに均一に溶解し、透明になる。
「A(良好)」:振盪すれば均一に溶解し、透明になる。
「B(やや不良)」:若干白濁する。
「×(不良)」:白濁もしくは相分離する。
各例の溶剤組成物を用いた潤滑剤溶液による潤滑剤塗膜の状態を目視で確認して以下の基準で評価する。
「S(優良)」:均一な塗膜である。
「A(良好)」:ほぼ均一な塗膜である。
「B(やや不良)」:塗膜に部分的にムラが見られる。
「×(不良)」:塗膜にかなりムラが見られる。
各例の溶剤組成物を用いた潤滑剤溶液による潤滑剤塗膜の形成時の潤滑剤溶液の乾燥性を以下の基準で乾燥性を評価する。
「S(優良)」:直ちに溶剤が蒸発する。
「A(良好)」:10分間以内に溶剤が蒸発する。
「B(可)」:10分超1時間以内で溶剤が蒸発する。
「×(不良)」:1時間経過しても溶剤が残存している。
Claims (10)
- (Z)−1−クロロ−3,3,3−トリフルオロ−1−プロペンを含む溶剤と、常圧における沸点が30℃以上60℃以下の飽和のハイドロクロロフルオロカーボンからなる安定剤とを含む溶剤組成物。
- 前記溶剤の含有量に対する、前記安定剤の含有量の割合が1質量ppm〜1質量%である、請求項1に記載の溶剤組成物。
- 前記(Z)−1−クロロ−3,3,3−トリフルオロ−1−プロペンの含有量に対する前記安定剤の含有量の割合が1質量ppm〜1質量%である、請求項1または2に記載の溶剤組成物。
- 前記溶剤全量に対する前記(Z)−1−クロロ−3,3,3−トリフルオロ−1−プロペンの含有量の割合が、80〜100質量%である、請求項1〜3のいずれか1項に記載の溶剤組成物。
- 前記常圧における沸点が30℃以上60℃以下の飽和のハイドロクロロフルオロカーボンが、2−クロロ−3,3,3−トリフルオロプロパン、1−クロロ−3,3,3−トリフルオロプロパン、1,1−ジクロロ−2,2,3,3,3−ペンタフルオロプロパンおよび1,3−ジクロロ−1,1,2,2,3−ペンタフルオロプロパンからなる群より選ばれる1種以上である請求項1〜4のいずれか1項に記載の溶剤組成物。
- 請求項1〜5のいずれか1項に記載の溶剤組成物と被洗浄物品とを接触させることを特徴とする洗浄方法。
- 前記被洗浄物品に付着した加工油を洗浄する、請求項6に記載の洗浄方法。
- 前記加工油が、切削油、焼き入れ油、圧延油、潤滑油、機械油、プレス加工油、打ち抜き油、引き抜き油、組立油および線引き油からなる群より選ばれる1種以上である、請求項7に記載の洗浄方法。
- 前記被洗浄物品が衣類である、請求項6に記載の洗浄方法。
- 請求項1〜5のいずれか1項に記載の溶剤組成物に不揮発性有機化合物を溶解させて塗膜形成用組成物を作製し、該塗膜形成用組成物を被塗布物上に塗布した後、前記溶剤組成物を蒸発させて、前記不揮発性有機化合物からなる塗膜を形成することを特徴とする、塗膜の形成方法。
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WO2019039521A1 (ja) * | 2017-08-25 | 2019-02-28 | Agc株式会社 | 溶剤組成物、洗浄方法、塗膜付き基材の製造方法及び熱移動媒体 |
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