JP2019502022A5 - - Google Patents
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- Publication number
- JP2019502022A5 JP2019502022A5 JP2018530051A JP2018530051A JP2019502022A5 JP 2019502022 A5 JP2019502022 A5 JP 2019502022A5 JP 2018530051 A JP2018530051 A JP 2018530051A JP 2018530051 A JP2018530051 A JP 2018530051A JP 2019502022 A5 JP2019502022 A5 JP 2019502022A5
- Authority
- JP
- Japan
- Prior art keywords
- acid
- group
- dispersion
- silver
- reducing agent
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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- 238000000034 method Methods 0.000 claims 17
- 239000006185 dispersion Substances 0.000 claims 12
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 claims 11
- 239000002055 nanoplate Substances 0.000 claims 8
- 229910052709 silver Inorganic materials 0.000 claims 8
- 239000004332 silver Substances 0.000 claims 8
- 239000003638 chemical reducing agent Substances 0.000 claims 7
- 229910000510 noble metal Inorganic materials 0.000 claims 7
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims 6
- -1 hydroxide compound Chemical class 0.000 claims 6
- 239000000203 mixture Substances 0.000 claims 5
- 238000010521 absorption reaction Methods 0.000 claims 4
- 150000001450 anions Chemical class 0.000 claims 4
- 238000000576 coating method Methods 0.000 claims 4
- 230000031700 light absorption Effects 0.000 claims 4
- 229920005646 polycarboxylate Polymers 0.000 claims 4
- 229920000642 polymer Polymers 0.000 claims 4
- FEWJPZIEWOKRBE-JCYAYHJZSA-N Dextrotartaric acid Chemical compound OC(=O)[C@H](O)[C@@H](O)C(O)=O FEWJPZIEWOKRBE-JCYAYHJZSA-N 0.000 claims 3
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims 3
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 claims 3
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims 3
- 239000007864 aqueous solution Substances 0.000 claims 3
- 238000006243 chemical reaction Methods 0.000 claims 3
- 239000003795 chemical substances by application Substances 0.000 claims 3
- 239000011248 coating agent Substances 0.000 claims 3
- 150000002500 ions Chemical class 0.000 claims 3
- 239000000243 solution Substances 0.000 claims 3
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 claims 2
- KRKNYBCHXYNGOX-UHFFFAOYSA-K Citrate Chemical compound [O-]C(=O)CC(O)(CC([O-])=O)C([O-])=O KRKNYBCHXYNGOX-UHFFFAOYSA-K 0.000 claims 2
- KCXVZYZYPLLWCC-UHFFFAOYSA-N EDTA Chemical compound OC(=O)CN(CC(O)=O)CCN(CC(O)=O)CC(O)=O KCXVZYZYPLLWCC-UHFFFAOYSA-N 0.000 claims 2
- OFOBLEOULBTSOW-UHFFFAOYSA-L Malonate Chemical compound [O-]C(=O)CC([O-])=O OFOBLEOULBTSOW-UHFFFAOYSA-L 0.000 claims 2
- FOIXSVOLVBLSDH-UHFFFAOYSA-N Silver ion Chemical compound [Ag+] FOIXSVOLVBLSDH-UHFFFAOYSA-N 0.000 claims 2
- 239000002253 acid Substances 0.000 claims 2
- 125000003172 aldehyde group Chemical group 0.000 claims 2
- 125000003368 amide group Chemical group 0.000 claims 2
- 125000003277 amino group Chemical group 0.000 claims 2
- 230000015572 biosynthetic process Effects 0.000 claims 2
- 125000002843 carboxylic acid group Chemical group 0.000 claims 2
- GTZCVFVGUGFEME-IWQZZHSRSA-N cis-aconitic acid Chemical compound OC(=O)C\C(C(O)=O)=C\C(O)=O GTZCVFVGUGFEME-IWQZZHSRSA-N 0.000 claims 2
- XFTRTWQBIOMVPK-UHFFFAOYSA-L citramalate(2-) Chemical compound [O-]C(=O)C(O)(C)CC([O-])=O XFTRTWQBIOMVPK-UHFFFAOYSA-L 0.000 claims 2
- 239000002131 composite material Substances 0.000 claims 2
- SWXVUIWOUIDPGS-UHFFFAOYSA-N diacetone alcohol Chemical compound CC(=O)CC(C)(C)O SWXVUIWOUIDPGS-UHFFFAOYSA-N 0.000 claims 2
- WJJMNDUMQPNECX-UHFFFAOYSA-N dipicolinic acid Chemical compound OC(=O)C1=CC=CC(C(O)=O)=N1 WJJMNDUMQPNECX-UHFFFAOYSA-N 0.000 claims 2
- 125000004185 ester group Chemical group 0.000 claims 2
- 125000001033 ether group Chemical group 0.000 claims 2
- LZCLXQDLBQLTDK-UHFFFAOYSA-N ethyl 2-hydroxypropanoate Chemical compound CCOC(=O)C(C)O LZCLXQDLBQLTDK-UHFFFAOYSA-N 0.000 claims 2
- 125000000623 heterocyclic group Chemical group 0.000 claims 2
- 125000002887 hydroxy group Chemical group [H]O* 0.000 claims 2
- ODBLHEXUDAPZAU-UHFFFAOYSA-N isocitric acid Chemical compound OC(=O)C(O)C(C(O)=O)CC(O)=O ODBLHEXUDAPZAU-UHFFFAOYSA-N 0.000 claims 2
- 125000000468 ketone group Chemical group 0.000 claims 2
- 239000003446 ligand Substances 0.000 claims 2
- BDAGIHXWWSANSR-UHFFFAOYSA-N methanoic acid Natural products OC=O BDAGIHXWWSANSR-UHFFFAOYSA-N 0.000 claims 2
- SIOXPEMLGUPBBT-UHFFFAOYSA-N picolinic acid Chemical compound OC(=O)C1=CC=CC=N1 SIOXPEMLGUPBBT-UHFFFAOYSA-N 0.000 claims 2
- KDYFGRWQOYBRFD-UHFFFAOYSA-L succinate(2-) Chemical compound [O-]C(=O)CCC([O-])=O KDYFGRWQOYBRFD-UHFFFAOYSA-L 0.000 claims 2
- 238000003786 synthesis reaction Methods 0.000 claims 2
- 229940095064 tartrate Drugs 0.000 claims 2
- VILCJCGEZXAXTO-UHFFFAOYSA-N 2,2,2-tetramine Chemical compound NCCNCCNCCN VILCJCGEZXAXTO-UHFFFAOYSA-N 0.000 claims 1
- YITYVXUAFSMRJI-UHFFFAOYSA-N 2-(carboxymethylamino)pentanedioic acid Chemical compound OC(=O)CCC(C(O)=O)NCC(O)=O YITYVXUAFSMRJI-UHFFFAOYSA-N 0.000 claims 1
- DMQQXDPCRUGSQB-UHFFFAOYSA-N 2-[3-[bis(carboxymethyl)amino]propyl-(carboxymethyl)amino]acetic acid Chemical compound OC(=O)CN(CC(O)=O)CCCN(CC(O)=O)CC(O)=O DMQQXDPCRUGSQB-UHFFFAOYSA-N 0.000 claims 1
- XWSGEVNYFYKXCP-UHFFFAOYSA-N 2-[carboxymethyl(methyl)amino]acetic acid Chemical compound OC(=O)CN(C)CC(O)=O XWSGEVNYFYKXCP-UHFFFAOYSA-N 0.000 claims 1
- OSWFIVFLDKOXQC-UHFFFAOYSA-N 4-(3-methoxyphenyl)aniline Chemical compound COC1=CC=CC(C=2C=CC(N)=CC=2)=C1 OSWFIVFLDKOXQC-UHFFFAOYSA-N 0.000 claims 1
- CPELXLSAUQHCOX-UHFFFAOYSA-M Bromide Chemical compound [Br-] CPELXLSAUQHCOX-UHFFFAOYSA-M 0.000 claims 1
- PIICEJLVQHRZGT-UHFFFAOYSA-N Ethylenediamine Chemical compound NCCN PIICEJLVQHRZGT-UHFFFAOYSA-N 0.000 claims 1
- AVXURJPOCDRRFD-UHFFFAOYSA-N Hydroxylamine Chemical compound ON AVXURJPOCDRRFD-UHFFFAOYSA-N 0.000 claims 1
- HNDVDQJCIGZPNO-YFKPBYRVSA-N L-histidine Chemical compound OC(=O)[C@@H](N)CC1=CN=CN1 HNDVDQJCIGZPNO-YFKPBYRVSA-N 0.000 claims 1
- QPCDCPDFJACHGM-UHFFFAOYSA-N N,N-bis{2-[bis(carboxymethyl)amino]ethyl}glycine Chemical compound OC(=O)CN(CC(O)=O)CCN(CC(=O)O)CCN(CC(O)=O)CC(O)=O QPCDCPDFJACHGM-UHFFFAOYSA-N 0.000 claims 1
- 229910002651 NO3 Inorganic materials 0.000 claims 1
- NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 claims 1
- LSNNMFCWUKXFEE-UHFFFAOYSA-N Sulfurous acid Chemical compound OS(O)=O LSNNMFCWUKXFEE-UHFFFAOYSA-N 0.000 claims 1
- FEWJPZIEWOKRBE-UHFFFAOYSA-N Tartaric acid Natural products [H+].[H+].[O-]C(=O)C(O)C(O)C([O-])=O FEWJPZIEWOKRBE-UHFFFAOYSA-N 0.000 claims 1
- YDONNITUKPKTIG-UHFFFAOYSA-N [Nitrilotris(methylene)]trisphosphonic acid Chemical compound OP(O)(=O)CN(CP(O)(O)=O)CP(O)(O)=O YDONNITUKPKTIG-UHFFFAOYSA-N 0.000 claims 1
- 125000000217 alkyl group Chemical group 0.000 claims 1
- 235000010323 ascorbic acid Nutrition 0.000 claims 1
- 229960005070 ascorbic acid Drugs 0.000 claims 1
- 239000011668 ascorbic acid Substances 0.000 claims 1
- 125000004432 carbon atom Chemical group C* 0.000 claims 1
- 239000008139 complexing agent Substances 0.000 claims 1
- 239000012045 crude solution Substances 0.000 claims 1
- HPNMFZURTQLUMO-UHFFFAOYSA-N diethylamine Chemical compound CCNCC HPNMFZURTQLUMO-UHFFFAOYSA-N 0.000 claims 1
- 229940116333 ethyl lactate Drugs 0.000 claims 1
- 235000019253 formic acid Nutrition 0.000 claims 1
- 125000000524 functional group Chemical group 0.000 claims 1
- 229910052737 gold Inorganic materials 0.000 claims 1
- 239000010931 gold Substances 0.000 claims 1
- HNDVDQJCIGZPNO-UHFFFAOYSA-N histidine Natural products OC(=O)C(N)CC1=CN=CN1 HNDVDQJCIGZPNO-UHFFFAOYSA-N 0.000 claims 1
- NBZBKCUXIYYUSX-UHFFFAOYSA-N iminodiacetic acid Chemical compound OC(=O)CNCC(O)=O NBZBKCUXIYYUSX-UHFFFAOYSA-N 0.000 claims 1
- 229910052751 metal Inorganic materials 0.000 claims 1
- 239000002184 metal Substances 0.000 claims 1
- MGFYIUFZLHCRTH-UHFFFAOYSA-N nitrilotriacetic acid Chemical compound OC(=O)CN(CC(O)=O)CC(O)=O MGFYIUFZLHCRTH-UHFFFAOYSA-N 0.000 claims 1
- 235000006408 oxalic acid Nutrition 0.000 claims 1
- 229960003330 pentetic acid Drugs 0.000 claims 1
- 150000002978 peroxides Chemical class 0.000 claims 1
- 229940081066 picolinic acid Drugs 0.000 claims 1
- 229910052697 platinum Inorganic materials 0.000 claims 1
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Substances [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 claims 1
- 239000001267 polyvinylpyrrolidone Substances 0.000 claims 1
- 235000013855 polyvinylpyrrolidone Nutrition 0.000 claims 1
- 229920000036 polyvinylpyrrolidone Polymers 0.000 claims 1
- 239000010970 precious metal Substances 0.000 claims 1
- 239000011541 reaction mixture Substances 0.000 claims 1
- 150000003839 salts Chemical class 0.000 claims 1
- 230000003595 spectral effect Effects 0.000 claims 1
- 230000002194 synthesizing effect Effects 0.000 claims 1
- 235000002906 tartaric acid Nutrition 0.000 claims 1
- 239000011975 tartaric acid Substances 0.000 claims 1
- DHCDFWKWKRSZHF-UHFFFAOYSA-L thiosulfate(2-) Chemical compound [O-]S([S-])(=O)=O DHCDFWKWKRSZHF-UHFFFAOYSA-L 0.000 claims 1
- KQTIIICEAUMSDG-UHFFFAOYSA-N tricarballylic acid Chemical compound OC(=O)CC(C(O)=O)CC(O)=O KQTIIICEAUMSDG-UHFFFAOYSA-N 0.000 claims 1
- MBYLVOKEDDQJDY-UHFFFAOYSA-N tris(2-aminoethyl)amine Chemical compound NCCN(CCN)CCN MBYLVOKEDDQJDY-UHFFFAOYSA-N 0.000 claims 1
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2022091525A JP7412024B2 (ja) | 2015-12-09 | 2022-06-06 | 銀ナノプレート上への貴金属コーティングの適用方法 |
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US14/963,974 | 2015-12-09 | ||
| US14/963,974 US10147512B2 (en) | 2015-12-09 | 2015-12-09 | Methods for synthesizing silver nanoplates and noble metal coated silver nanoplates and their use in transparent films for control of light hue |
| PCT/US2016/064558 WO2017100086A1 (en) | 2015-12-09 | 2016-12-02 | Methods for synthesizing silver nanoplates and noble metal coated silver nanoplates and their use in transparent films |
Related Child Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2022091525A Division JP7412024B2 (ja) | 2015-12-09 | 2022-06-06 | 銀ナノプレート上への貴金属コーティングの適用方法 |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2019502022A JP2019502022A (ja) | 2019-01-24 |
| JP2019502022A5 true JP2019502022A5 (https=) | 2020-01-16 |
| JP7153922B2 JP7153922B2 (ja) | 2022-10-17 |
Family
ID=59014112
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2018530051A Active JP7153922B2 (ja) | 2015-12-09 | 2016-12-02 | 銀ナノプレートの合成方法 |
| JP2022091525A Active JP7412024B2 (ja) | 2015-12-09 | 2022-06-06 | 銀ナノプレート上への貴金属コーティングの適用方法 |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2022091525A Active JP7412024B2 (ja) | 2015-12-09 | 2022-06-06 | 銀ナノプレート上への貴金属コーティングの適用方法 |
Country Status (6)
| Country | Link |
|---|---|
| US (3) | US10147512B2 (https=) |
| JP (2) | JP7153922B2 (https=) |
| KR (1) | KR102568165B1 (https=) |
| CN (2) | CN114255906B (https=) |
| TW (1) | TWI733720B (https=) |
| WO (1) | WO2017100086A1 (https=) |
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| KR101930385B1 (ko) * | 2014-11-05 | 2018-12-18 | 씨에이엠 홀딩 코포레이션 | 은 나노와이어-기반 투명 전도성 필름을 형성하기 위한 아이오다이드 첨가제를 갖는 단쇄 플루오로계면활성제 |
| JP6663079B2 (ja) * | 2017-03-31 | 2020-03-11 | 富士フイルム株式会社 | 金被覆銀平板状粒子、金被覆銀平板状粒子分散液及びその製造方法、塗布膜、並びに、反射防止光学部材 |
| CN107984839A (zh) * | 2017-12-04 | 2018-05-04 | 京东方科技集团股份有限公司 | 一种复合保护层及柔性显示装置 |
| US10714230B2 (en) | 2017-12-06 | 2020-07-14 | C3Nano Inc. | Thin and uniform silver nanowires, method of synthesis and transparent conductive films formed from the nanowires |
| KR102050042B1 (ko) * | 2018-03-15 | 2019-11-28 | 경희대학교 산학협력단 | 이방성 2d 은 나노 플레이트 및 이의 제조방법 |
| CN109243677B (zh) * | 2018-07-27 | 2021-04-23 | 深圳市华科创智技术有限公司 | 一种透明导电膜 |
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| CN111755146B (zh) * | 2020-06-28 | 2022-02-22 | 深圳市华科创智技术有限公司 | 一种低b*值高透过率导电膜 |
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| CN116213745B (zh) * | 2023-01-03 | 2025-08-15 | 中国乐凯集团有限公司 | 薄膜状银粉及其制备方法和应用 |
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| CN117862520B (zh) * | 2024-03-11 | 2024-05-10 | 云南师范大学 | 一种使用紫胶制备片状银粉的方法 |
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| CA2889423A1 (en) | 2012-10-26 | 2014-05-01 | Nanocomposix, Inc. | Metastable silver nanoparticle composites |
| US9441301B2 (en) | 2012-12-06 | 2016-09-13 | Nanyang Technological University | Method for forming a bimetallic core-shell nanostructure |
| US10020807B2 (en) | 2013-02-26 | 2018-07-10 | C3Nano Inc. | Fused metal nanostructured networks, fusing solutions with reducing agents and methods for forming metal networks |
| US11274223B2 (en) | 2013-11-22 | 2022-03-15 | C3 Nano, Inc. | Transparent conductive coatings based on metal nanowires and polymer binders, solution processing thereof, and patterning approaches |
| US9183968B1 (en) | 2014-07-31 | 2015-11-10 | C3Nano Inc. | Metal nanowire inks for the formation of transparent conductive films with fused networks |
| US20160096967A1 (en) | 2014-10-03 | 2016-04-07 | C3Nano Inc. | Property enhancing fillers for transparent coatings and transparent conductive films |
| CN104263303B (zh) * | 2014-10-13 | 2016-05-18 | 中国科学院理化技术研究所 | 一种直接涂覆使用的柔性导电胶及其制备方法 |
| US11111396B2 (en) | 2014-10-17 | 2021-09-07 | C3 Nano, Inc. | Transparent films with control of light hue using nanoscale colorants |
| US20160122562A1 (en) | 2014-10-29 | 2016-05-05 | C3Nano Inc. | Stable transparent conductive elements based on sparse metal conductive layers |
| US20160369104A1 (en) | 2015-06-16 | 2016-12-22 | C3Nano Inc. | Transparent polymer hardcoats and corresponding transparent films |
| CN105140341B (zh) * | 2015-07-28 | 2017-05-10 | 李嘉诚 | 一种薄膜太阳能电池前电极的制备方法 |
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