JP2016512280A - 天然油ポリオールベースの新規ポリマーポリオール - Google Patents

天然油ポリオールベースの新規ポリマーポリオール Download PDF

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Publication number
JP2016512280A
JP2016512280A JP2016500813A JP2016500813A JP2016512280A JP 2016512280 A JP2016512280 A JP 2016512280A JP 2016500813 A JP2016500813 A JP 2016500813A JP 2016500813 A JP2016500813 A JP 2016500813A JP 2016512280 A JP2016512280 A JP 2016512280A
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polyol
natural oil
polyols
initiator
polymer polyol
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Pending
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JP2016500813A
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English (en)
Japanese (ja)
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JP2016512280A5 (enExample
Inventor
リック、アイ．アドキンス
ジョン、イングランド
ドン、エス．ウォーディウス
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Covestro LLC
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Bayer MaterialScience LLC
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Publication of JP2016512280A publication Critical patent/JP2016512280A/ja
Publication of JP2016512280A5 publication Critical patent/JP2016512280A5/ja
Pending legal-status Critical Current

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    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G71/00—Macromolecular compounds obtained by reactions forming a ureide or urethane link, otherwise, than from isocyanate radicals in the main chain of the macromolecule
    • C08G71/04—Polyurethanes
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/40—High-molecular-weight compounds
    • C08G18/48—Polyethers
    • C08G18/4829—Polyethers containing at least three hydroxy groups
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/08—Processes
    • C08G18/09—Processes comprising oligomerisation of isocyanates or isothiocyanates involving reaction of a part of the isocyanate or isothiocyanate groups with each other in the reaction mixture
    • C08G18/092—Processes comprising oligomerisation of isocyanates or isothiocyanates involving reaction of a part of the isocyanate or isothiocyanate groups with each other in the reaction mixture oligomerisation to isocyanurate groups
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/08—Processes
    • C08G18/16—Catalysts
    • C08G18/161—Catalysts containing two or more components to be covered by at least two of the groups C08G18/166, C08G18/18 or C08G18/22
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/08—Processes
    • C08G18/16—Catalysts
    • C08G18/18—Catalysts containing secondary or tertiary amines or salts thereof
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/08—Processes
    • C08G18/16—Catalysts
    • C08G18/22—Catalysts containing metal compounds
    • C08G18/225—Catalysts containing metal compounds of alkali or alkaline earth metals
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/40—High-molecular-weight compounds
    • C08G18/4009—Two or more macromolecular compounds not provided for in one single group of groups C08G18/42 - C08G18/64
    • C08G18/4072—Mixtures of compounds of group C08G18/63 with other macromolecular compounds
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/40—High-molecular-weight compounds
    • C08G18/48—Polyethers
    • C08G18/4804—Two or more polyethers of different physical or chemical nature
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/40—High-molecular-weight compounds
    • C08G18/48—Polyethers
    • C08G18/4891—Polyethers modified with higher fatty oils or their acids or by resin acids
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/40—High-molecular-weight compounds
    • C08G18/63—Block or graft polymers obtained by polymerising compounds having carbon-to-carbon double bonds on to polymers
    • C08G18/632—Block or graft polymers obtained by polymerising compounds having carbon-to-carbon double bonds on to polymers onto polyethers
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/40—High-molecular-weight compounds
    • C08G18/63—Block or graft polymers obtained by polymerising compounds having carbon-to-carbon double bonds on to polymers
    • C08G18/636—Block or graft polymers obtained by polymerising compounds having carbon-to-carbon double bonds on to polymers characterised by the presence of a dispersion-stabiliser
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
    • C08G18/81—Unsaturated isocyanates or isothiocyanates
    • C08G18/8108—Unsaturated isocyanates or isothiocyanates having only one isocyanate or isothiocyanate group
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J9/00—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof
    • C08J9/04—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof using blowing gases generated by a previously added blowing agent
    • C08J9/12—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof using blowing gases generated by a previously added blowing agent by a physical blowing agent
    • C08J9/14—Working-up of macromolecular substances to porous or cellular articles or materials; After-treatment thereof using blowing gases generated by a previously added blowing agent by a physical blowing agent organic
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G2110/00—Foam properties
    • C08G2110/0016—Foam properties semi-rigid
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G2115/00—Oligomerisation
    • C08G2115/02—Oligomerisation to isocyanurate groups
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G2350/00—Acoustic or vibration damping material
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2205/00—Foams characterised by their properties
    • C08J2205/10—Rigid foams
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J2375/00—Characterised by the use of polyureas or polyurethanes; Derivatives of such polymers
    • C08J2375/04—Polyurethanes

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  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Dispersion Chemistry (AREA)
  • Polyurethanes Or Polyureas (AREA)
  • Polymerisation Methods In General (AREA)
  • Graft Or Block Polymers (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Lubricants (AREA)
JP2016500813A 2013-03-14 2014-03-07 天然油ポリオールベースの新規ポリマーポリオール Pending JP2016512280A (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US13/826,911 2013-03-14
US13/826,911 US20140275310A1 (en) 2013-03-14 2013-03-14 Novel polymer polyols based on natural oils polyols
PCT/US2014/021704 WO2014159048A1 (en) 2013-03-14 2014-03-07 Novel polymer polyols based on natural oils polyols

Publications (2)

Publication Number Publication Date
JP2016512280A true JP2016512280A (ja) 2016-04-25
JP2016512280A5 JP2016512280A5 (enExample) 2017-04-13

Family

ID=51530048

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2016500813A Pending JP2016512280A (ja) 2013-03-14 2014-03-07 天然油ポリオールベースの新規ポリマーポリオール

Country Status (12)

Country Link
US (1) US20140275310A1 (enExample)
EP (1) EP2970553B1 (enExample)
JP (1) JP2016512280A (enExample)
KR (1) KR20150128978A (enExample)
CN (1) CN105452317B (enExample)
BR (1) BR112015021958A2 (enExample)
CA (1) CA2903015A1 (enExample)
ES (1) ES2717755T3 (enExample)
MX (1) MX2015012027A (enExample)
PL (1) PL2970553T3 (enExample)
SG (2) SG11201506884QA (enExample)
WO (1) WO2014159048A1 (enExample)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2023532875A (ja) * 2020-06-25 2023-08-01 ビーエーエスエフ ソシエタス・ヨーロピア 高圧縮強度、低熱伝導率、高表面品質を有するポリイソシアヌレート樹脂フォーム

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EP3250619B1 (en) * 2015-01-26 2024-04-24 Henkel AG & Co. KGaA Functionalized polyurethanes prepared from renewable materials
WO2017020124A1 (en) 2015-07-31 2017-02-09 The Governors Of The University Of Alberta Synthesis of polyols suitable for castor oil replacement
CN109642046B (zh) * 2016-06-28 2022-01-25 Ptt全球化学公众有限公司 基于天然油多元醇的杂化多元醇
US10975190B2 (en) * 2016-07-21 2021-04-13 Bionanofoam Llc Bio-based and hydrophilic polyurethane prepolymer and foam made therefrom
US10479862B2 (en) * 2017-12-07 2019-11-19 Covestro Llc Amine based polymer polyol stabilizers
SG11202004869PA (en) 2017-12-08 2020-06-29 Shell Int Research Antioxidant for low-density polyurethane foam
US10851239B2 (en) * 2018-11-07 2020-12-01 Covestro Llc Ethylenically unsaturated macromers produced from a residue of isocyanate manufacturing, related preformed stabilizers, polymer polyols, foam-forming compositions and foams
US11407874B2 (en) 2019-10-07 2022-08-09 Covestro Llc Polyol premixes, thermally insulating rigid polyurethane foams and methods for their production
WO2021145869A1 (en) * 2020-01-15 2021-07-22 Covestro Llc Methods of manufacturing short chain polyether polyols
US11993733B2 (en) * 2020-03-18 2024-05-28 Iowa State University Research Foundation, Inc. Bio-based coatings and adhesives using oils of Physaria fendleri and Euphorbia lagascae
CN111440180B (zh) * 2020-04-07 2021-04-20 万华化学集团股份有限公司 阻燃聚合物多元醇及其制备方法和用途
KR20230056674A (ko) 2020-08-24 2023-04-27 에보닉 오퍼레이션스 게엠베하 온화한 조건하에서 폴리우레탄의 탈중합
CN115989257B (zh) 2020-08-24 2026-03-03 赢创运营有限公司 聚氨酯解聚方法
CN115160555A (zh) * 2021-04-02 2022-10-11 常州强力先端电子材料有限公司 一种氧杂环丁烷类聚合物及其制备方法
US12428523B2 (en) 2021-05-05 2025-09-30 H.B. Fuller Company Polyurethanes and moisture curable compositions including the same
WO2023275031A1 (de) * 2021-07-02 2023-01-05 Evonik Operations Gmbh Herstellung von pu-schaumstoffen unter einsatz von recycling-polyolen
US12006413B2 (en) 2022-01-12 2024-06-11 Covestro Llc Polymer polyols, processes for their preparation, and the use thereof to produce foams exhibiting resistance to combustion
CN116178634B (zh) * 2023-02-01 2024-08-20 中国林业科学研究院林产化学工业研究所 一种桐油基聚合物及其制备方法和应用
US12679922B2 (en) 2023-06-15 2026-07-14 Covestro Llc Isocyanate-reactive compositions, rigid polyurethane foams and methods for their production

Citations (5)

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Publication number Priority date Publication date Assignee Title
JP2006045567A (ja) * 2004-08-02 2006-02-16 Bayer Material Science Llc 低粘度ポリマーポリオール
JP2007077396A (ja) * 2005-09-09 2007-03-29 Bayer Material Science Llc 高ヒドロキシル価を特徴とする低粘度ポリマーポリオール
JP2008121015A (ja) * 2006-11-13 2008-05-29 Bayer Materialscience Ag ポリエーテル−エステルポリオールの製造方法
JP2009538963A (ja) * 2006-05-31 2009-11-12 バイエル・マテリアルサイエンス・リミテッド・ライアビリティ・カンパニー 高固体および高ヒドロキシル価を特徴とするポリマーポリオールを用いる、少量のジイソシアネートによる硬質および半硬質のフォームの製造方法および得られるフォーム
JP2010150547A (ja) * 2008-12-23 2010-07-08 Bayer Material Science Llc 天然油ベースポリオールを含むポリマーポリオール、該ポリマーポリオールを含むポリウレタンフォーム、およびその製造方法

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EP2001921A2 (en) * 2006-03-23 2008-12-17 Dow Global Technologies Inc. Natural oil based polyols with intrinsic surpactancy for polyurethane foaming
ZA200709673B (en) * 2006-11-13 2009-09-30 Bayer Materialscience Ag Process for the preparation of polyether-ester polyols
US8097739B2 (en) * 2007-04-18 2012-01-17 BioBases Technologies, LLC Process for the manufacture of natural oil hydroxylates
EP2225194A4 (en) * 2007-11-29 2012-07-11 Univ Saskatchewan METHOD FOR PRODUCING POLYOL BASED CATALYSTS
DE102008051882A1 (de) * 2008-10-16 2010-04-29 Bayer Materialscience Ag Verfahren zur Herstellung von Polyetheresterpolyolen

Patent Citations (5)

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Publication number Priority date Publication date Assignee Title
JP2006045567A (ja) * 2004-08-02 2006-02-16 Bayer Material Science Llc 低粘度ポリマーポリオール
JP2007077396A (ja) * 2005-09-09 2007-03-29 Bayer Material Science Llc 高ヒドロキシル価を特徴とする低粘度ポリマーポリオール
JP2009538963A (ja) * 2006-05-31 2009-11-12 バイエル・マテリアルサイエンス・リミテッド・ライアビリティ・カンパニー 高固体および高ヒドロキシル価を特徴とするポリマーポリオールを用いる、少量のジイソシアネートによる硬質および半硬質のフォームの製造方法および得られるフォーム
JP2008121015A (ja) * 2006-11-13 2008-05-29 Bayer Materialscience Ag ポリエーテル−エステルポリオールの製造方法
JP2010150547A (ja) * 2008-12-23 2010-07-08 Bayer Material Science Llc 天然油ベースポリオールを含むポリマーポリオール、該ポリマーポリオールを含むポリウレタンフォーム、およびその製造方法

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2023532875A (ja) * 2020-06-25 2023-08-01 ビーエーエスエフ ソシエタス・ヨーロピア 高圧縮強度、低熱伝導率、高表面品質を有するポリイソシアヌレート樹脂フォーム
JP7749605B2 (ja) 2020-06-25 2025-10-06 ビーエーエスエフ ソシエタス・ヨーロピア 高圧縮強度、低熱伝導率、高表面品質を有するポリイソシアヌレート樹脂フォーム

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Publication number Publication date
KR20150128978A (ko) 2015-11-18
BR112015021958A2 (pt) 2017-07-18
PL2970553T3 (pl) 2019-07-31
US20140275310A1 (en) 2014-09-18
SG11201506884QA (en) 2015-09-29
CN105452317A (zh) 2016-03-30
CA2903015A1 (en) 2014-10-02
EP2970553A4 (en) 2016-10-26
EP2970553B1 (en) 2019-03-06
EP2970553A1 (en) 2016-01-20
CN105452317B (zh) 2018-02-16
MX2015012027A (es) 2015-11-18
WO2014159048A8 (en) 2015-12-23
WO2014159048A1 (en) 2014-10-02
ES2717755T3 (es) 2019-06-25
SG10201707482QA (en) 2017-10-30

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