JP2015515963A - 高純度で、黄変しない（メタ）アクリル酸の製造方法 - Google Patents

高純度で、黄変しない（メタ）アクリル酸の製造方法 Download PDF

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Publication number
JP2015515963A
JP2015515963A JP2015509367A JP2015509367A JP2015515963A JP 2015515963 A JP2015515963 A JP 2015515963A JP 2015509367 A JP2015509367 A JP 2015509367A JP 2015509367 A JP2015509367 A JP 2015509367A JP 2015515963 A JP2015515963 A JP 2015515963A
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Japan
Prior art keywords
meth
acrylic acid
pure
crude
ion exchange
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JP2015509367A
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Japanese (ja)
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JP2015515963A5 (enExample
Inventor
ジャン ジェンフェン
ジャン ジェンフェン
ケルブル ゲアハート
ケルブル ゲアハート
サルトレッリ ロレンツァ
サルトレッリ ロレンツァ
ヒルトナー ホアスト
ヒルトナー ホアスト
ワン フイシェン
ワン フイシェン
ミヒェル ミルコ
ミヒェル ミルコ
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Evonik Industries AG
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Evonik Industries AG
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Publication of JP2015515963A publication Critical patent/JP2015515963A/ja
Publication of JP2015515963A5 publication Critical patent/JP2015515963A5/ja
Pending legal-status Critical Current

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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/47—Separation; Purification; Stabilisation; Use of additives by solid-liquid treatment; by chemisorption
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • C07C51/44—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/48—Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
JP2015509367A 2012-05-03 2013-04-22 高純度で、黄変しない（メタ）アクリル酸の製造方法 Pending JP2015515963A (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
PCT/CN2012/075033 WO2013163806A1 (en) 2012-05-03 2012-05-03 Process for preparation of highly pure, non-yellowing methacrylic acid
CNPCT/CN2012/075033 2012-05-03
PCT/EP2013/058289 WO2013164216A1 (en) 2012-05-03 2013-04-22 Process for preparation of highly pure, non-yellowing (meth)acrylic acid

Publications (2)

Publication Number Publication Date
JP2015515963A true JP2015515963A (ja) 2015-06-04
JP2015515963A5 JP2015515963A5 (enExample) 2016-06-16

Family

ID=48142804

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2015509367A Pending JP2015515963A (ja) 2012-05-03 2013-04-22 高純度で、黄変しない（メタ）アクリル酸の製造方法

Country Status (8)

Country Link
US (1) US9290431B2 (enExample)
EP (1) EP2844633A1 (enExample)
JP (1) JP2015515963A (enExample)
KR (1) KR20150005938A (enExample)
SG (1) SG11201407133UA (enExample)
TW (1) TW201406717A (enExample)
WO (2) WO2013163806A1 (enExample)
ZA (1) ZA201407984B (enExample)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2023525210A (ja) * 2020-05-08 2023-06-15 ズルツァー・マネージメント・アーゲー スチレン含有供給原料から精製スチレン組成物を調製するための方法および装置

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR3008899B1 (fr) * 2013-07-25 2017-04-21 Arkema France Methode et systeme pour la distribution d'un liquide dans des capacites pour la preparation de monomeres (meth)acryliques

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS55129239A (en) * 1979-03-28 1980-10-06 Mitsubishi Rayon Co Ltd Purification of methacrylic acid
JPS5948437A (ja) * 1982-09-14 1984-03-19 Mitsubishi Rayon Co Ltd メタクリル酸の精製法
JPH1087551A (ja) * 1996-09-13 1998-04-07 Mitsubishi Rayon Co Ltd メタクリル酸の精製法
JPH1160536A (ja) * 1997-08-11 1999-03-02 Mitsubishi Rayon Co Ltd メタクリル酸の精製方法
JP2001213839A (ja) * 2000-02-03 2001-08-07 Nippon Shokubai Co Ltd （メタ）アクリル酸の製造方法
JP2003160530A (ja) * 2001-11-27 2003-06-03 Mitsubishi Chemicals Corp （メタ）アクリル酸の精製方法
JP2005179352A (ja) * 2003-11-28 2005-07-07 Mitsubishi Chemicals Corp （メタ）アクリル酸の精製方法
JP2008161848A (ja) * 2007-01-04 2008-07-17 Mitsubishi Rayon Co Ltd 縦型多段翼反応槽及び（メタ）アクリル酸の精製方法
JP2011514311A (ja) * 2008-01-30 2011-05-06 エボニック レーム ゲゼルシャフト ミット ベシュレンクテル ハフツング 高純度メタクリル酸の製造方法

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DE1668362B2 (de) 1968-02-17 1976-11-11 Hoechst Ag, 6000 Frankfurt Verfahren zur herstellung aliphatischer acrylsaeureester
BE786398A (fr) 1971-07-21 1973-01-18 Basf Ag Procede de preparation de l'acide acrylique anhydre
JPS55124734A (en) 1979-03-22 1980-09-26 Nippon Kayaku Co Ltd Preparation of methacrylic acid
JPS56108735A (en) 1980-02-01 1981-08-28 Sumitomo Chem Co Ltd Treating method of waste water in preparation of methacrylic acid
DE3467340D1 (en) 1984-07-21 1987-12-17 Mitsubishi Petrochemical Co Process for purification of 1,2-unsaturated carboxylic acids and/or esters thereof
US4879412A (en) 1985-03-14 1989-11-07 Mitsui Toatsu Chemicals, Inc. Purification process of methacrylic acid
JPS63122642A (ja) 1986-11-11 1988-05-26 Mitsubishi Rayon Co Ltd メタクロレイン及びメタクリル酸の製造法
CA1308737C (en) 1987-04-16 1992-10-13 Syoichi Matsumoto Process for producing methacrylic ester
CA1316545C (en) 1987-06-27 1993-04-20 Morimasa Kuragano Quenching process of reaction product gas containing methacrylic acid and treatment method of quenched liquid
JPS646233A (en) 1987-06-27 1989-01-10 Mitsui Toatsu Chemicals Purification of methacrylic acid
DE3721865A1 (de) 1987-07-02 1989-01-12 Basf Ag Verfahren zur herstellung von methacrylsaeure
JPH01193240A (ja) 1988-01-29 1989-08-03 Mitsui Toatsu Chem Inc メタクリル酸メチルの製造法
JPH0764776B2 (ja) 1988-03-23 1995-07-12 三井東圧化学株式会社 メタクロレインの吸収方法
JPH0684326B2 (ja) 1988-06-03 1994-10-26 株式会社日本触媒 メタクロレインの回収方法
DE3844087A1 (de) 1988-12-28 1990-07-05 Basf Ag Verfahren zur herstellung von methacrylsaeure durch oxidation von methacrolein
EP0608917B1 (en) 1989-12-06 1999-04-21 Nippon Shokubai Co., Ltd. Process for producing methacrolein and methacrylic acid
US5198579A (en) 1990-11-14 1993-03-30 Mitsui Toatsu Chemicals, Inc. Catalyst for oxidizing methacrolein and method for preparing methacrylic acid
DE4132684A1 (de) 1991-10-01 1993-04-08 Basf Ag Verfahren zur katalytischen gasphasenoxidation von methacrolein zu methacrylsaeure
TW305830B (enExample) 1993-03-26 1997-05-21 Sulzer Chemtech Ag
DE4405059A1 (de) 1994-02-17 1995-08-24 Basf Ag Multimetalloxidmassen
JPH08134011A (ja) 1994-11-04 1996-05-28 Mitsui Toatsu Chem Inc メタクリル酸の精製方法
DE19627847A1 (de) 1996-07-10 1998-01-15 Basf Ag Verfahren zur Herstellung von Acrylsäure
DE19740252A1 (de) 1997-09-12 1999-03-18 Basf Ag Verfahren zur Herstellung von Acrylsäure und Methacrylsäure
DE19838817A1 (de) 1998-08-26 2000-03-02 Basf Ag Verfahren zur kontinuierlichen Gewinnung von (Meth)acrylsäure
JP3702710B2 (ja) 1999-06-15 2005-10-05 住友化学株式会社 メタクリル酸製造用触媒およびメタクリル酸の製造方法
JP4960562B2 (ja) 2000-04-11 2012-06-27 ビーエーエスエフ ソシエタス・ヨーロピア 粗製アクリル酸溶融物の精製法
US7803969B2 (en) 2001-01-12 2010-09-28 Evonik Stockhausen Gmbh Continuous process for the production and purification of acrylic acid
DE10131479B4 (de) 2001-06-29 2005-05-19 Röhm GmbH & Co. KG Farbstabilisierung von grundstabilisierten ethylenisch ungesättigten Monomeren, insbesondere von grundstabilisierten Hydroxyalkyl(meth)acrylaten
DE10138150A1 (de) 2001-08-03 2003-02-13 Basf Ag Verfahren zur Herstellung wasserabsorbierender Harze
DE102008043609A1 (de) * 2008-11-10 2010-05-12 Evonik Röhm Gmbh Verfahren zur Reduzierung des Wassergehalts in (Meth)acrylsäure

Patent Citations (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS55129239A (en) * 1979-03-28 1980-10-06 Mitsubishi Rayon Co Ltd Purification of methacrylic acid
JPS5948437A (ja) * 1982-09-14 1984-03-19 Mitsubishi Rayon Co Ltd メタクリル酸の精製法
JPH1087551A (ja) * 1996-09-13 1998-04-07 Mitsubishi Rayon Co Ltd メタクリル酸の精製法
JPH1160536A (ja) * 1997-08-11 1999-03-02 Mitsubishi Rayon Co Ltd メタクリル酸の精製方法
JP2001213839A (ja) * 2000-02-03 2001-08-07 Nippon Shokubai Co Ltd （メタ）アクリル酸の製造方法
JP2003160530A (ja) * 2001-11-27 2003-06-03 Mitsubishi Chemicals Corp （メタ）アクリル酸の精製方法
JP2005179352A (ja) * 2003-11-28 2005-07-07 Mitsubishi Chemicals Corp （メタ）アクリル酸の精製方法
JP2008161848A (ja) * 2007-01-04 2008-07-17 Mitsubishi Rayon Co Ltd 縦型多段翼反応槽及び（メタ）アクリル酸の精製方法
JP2011514311A (ja) * 2008-01-30 2011-05-06 エボニック レーム ゲゼルシャフト ミット ベシュレンクテル ハフツング 高純度メタクリル酸の製造方法

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2023525210A (ja) * 2020-05-08 2023-06-15 ズルツァー・マネージメント・アーゲー スチレン含有供給原料から精製スチレン組成物を調製するための方法および装置

Also Published As

Publication number Publication date
US9290431B2 (en) 2016-03-22
KR20150005938A (ko) 2015-01-15
TW201406717A (zh) 2014-02-16
WO2013163806A1 (en) 2013-11-07
WO2013164216A1 (en) 2013-11-07
EP2844633A1 (en) 2015-03-11
US20150126777A1 (en) 2015-05-07
SG11201407133UA (en) 2014-11-27
ZA201407984B (en) 2015-12-23

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