JP2014088387A5 - - Google Patents
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- Publication number
- JP2014088387A5 JP2014088387A5 JP2013247358A JP2013247358A JP2014088387A5 JP 2014088387 A5 JP2014088387 A5 JP 2014088387A5 JP 2013247358 A JP2013247358 A JP 2013247358A JP 2013247358 A JP2013247358 A JP 2013247358A JP 2014088387 A5 JP2014088387 A5 JP 2014088387A5
- Authority
- JP
- Japan
- Prior art keywords
- phosphonium catalyst
- catalyst
- phosphonium
- purified
- reaction zone
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000003054 catalyst Substances 0.000 claims description 22
- XYFCBTPGUUZFHI-UHFFFAOYSA-O phosphonium Chemical compound [PH4+] XYFCBTPGUUZFHI-UHFFFAOYSA-O 0.000 claims description 18
- 239000000203 mixture Substances 0.000 claims description 2
- 238000000034 method Methods 0.000 claims 12
- 238000006243 chemical reaction Methods 0.000 claims 9
- -1 phosphonium halide Chemical class 0.000 claims 8
- 238000004519 manufacturing process Methods 0.000 claims 3
- 239000000047 product Substances 0.000 claims 3
- 239000002904 solvent Substances 0.000 claims 3
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims 2
- 125000002947 alkylene group Chemical group 0.000 claims 2
- 125000004209 (C1-C8) alkyl group Chemical group 0.000 claims 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 claims 1
- 229910052799 carbon Inorganic materials 0.000 claims 1
- 229910002092 carbon dioxide Inorganic materials 0.000 claims 1
- 239000001569 carbon dioxide Substances 0.000 claims 1
- 150000004649 carbonic acid derivatives Chemical class 0.000 claims 1
- 239000007857 degradation product Substances 0.000 claims 1
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 claims 1
- 150000004820 halides Chemical class 0.000 claims 1
- 125000000959 isobutyl group Chemical group [H]C([H])([H])C([H])(C([H])([H])[H])C([H])([H])* 0.000 claims 1
- 125000001449 isopropyl group Chemical group [H]C([H])([H])C([H])(*)C([H])([H])[H] 0.000 claims 1
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims 1
- 125000004108 n-butyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])([H])* 0.000 claims 1
- 125000004123 n-propyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])* 0.000 claims 1
- AUONHKJOIZSQGR-UHFFFAOYSA-N oxophosphane Chemical compound P=O AUONHKJOIZSQGR-UHFFFAOYSA-N 0.000 claims 1
- 238000002360 preparation method Methods 0.000 claims 1
- 239000011541 reaction mixture Substances 0.000 claims 1
- 125000000999 tert-butyl group Chemical group [H]C([H])([H])C(*)(C([H])([H])[H])C([H])([H])[H] 0.000 claims 1
- RKHXQBLJXBGEKF-UHFFFAOYSA-M tetrabutylphosphanium;bromide Chemical group [Br-].CCCC[P+](CCCC)(CCCC)CCCC RKHXQBLJXBGEKF-UHFFFAOYSA-M 0.000 claims 1
- 238000005809 transesterification reaction Methods 0.000 claims 1
- 238000004821 distillation Methods 0.000 description 6
- 239000000356 contaminant Substances 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP06110999 | 2006-03-13 | ||
| EP06110999.7 | 2006-03-13 |
Related Parent Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2008558796A Division JP5551876B2 (ja) | 2006-03-13 | 2007-03-12 | アルキレンカーボネートの製造方法ならびにこのように製造されたアルキレンカーボネートの、アルカンジオールおよびジアルキルカーボネートの製造における使用 |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2014088387A JP2014088387A (ja) | 2014-05-15 |
| JP2014088387A5 true JP2014088387A5 (enExample) | 2014-08-14 |
| JP5726278B2 JP5726278B2 (ja) | 2015-05-27 |
Family
ID=36838664
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2008558796A Expired - Fee Related JP5551876B2 (ja) | 2006-03-13 | 2007-03-12 | アルキレンカーボネートの製造方法ならびにこのように製造されたアルキレンカーボネートの、アルカンジオールおよびジアルキルカーボネートの製造における使用 |
| JP2013247358A Expired - Fee Related JP5726278B2 (ja) | 2006-03-13 | 2013-11-29 | アルキレンカーボネートの製造方法ならびにこのように製造されたアルキレンカーボネートの、アルカンジオールおよびジアルキルカーボネートの製造における使用 |
Family Applications Before (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2008558796A Expired - Fee Related JP5551876B2 (ja) | 2006-03-13 | 2007-03-12 | アルキレンカーボネートの製造方法ならびにこのように製造されたアルキレンカーボネートの、アルカンジオールおよびジアルキルカーボネートの製造における使用 |
Country Status (13)
| Country | Link |
|---|---|
| US (1) | US20070213542A1 (enExample) |
| EP (1) | EP1994018B1 (enExample) |
| JP (2) | JP5551876B2 (enExample) |
| KR (1) | KR20080110782A (enExample) |
| CN (1) | CN101553479B (enExample) |
| AU (1) | AU2007224469A1 (enExample) |
| BR (1) | BRPI0708285A2 (enExample) |
| CA (1) | CA2641997A1 (enExample) |
| ES (1) | ES2396866T3 (enExample) |
| MX (1) | MX2008011415A (enExample) |
| RU (1) | RU2008140313A (enExample) |
| TW (1) | TWI387584B (enExample) |
| WO (1) | WO2007104730A1 (enExample) |
Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| TW200906774A (en) * | 2007-04-23 | 2009-02-16 | Shell Int Research | Process for the preparation of an 1,2-alkylene diol and a dialkylcarbonate |
| WO2009141377A1 (en) * | 2008-05-20 | 2009-11-26 | Shell Internationale Research Maatschappij B.V. | Process for preparing an 1,2-alkylene carbonate |
| TWI457317B (zh) | 2008-05-20 | 2014-10-21 | Shell Int Research | 碳酸伸烷酯之製造方法 |
| DE102010042937A1 (de) * | 2010-10-08 | 2012-04-12 | Bayer Materialscience Aktiengesellschaft | Verfahren zur Herstellung von Diarylcarbonaten aus Dialkylcarbonaten |
| CN103028440B (zh) * | 2011-09-29 | 2015-06-10 | 中国石油化工股份有限公司 | 用于制备碳酸亚烷酯的大孔型树脂催化剂 |
| TWI623525B (zh) * | 2013-07-19 | 2018-05-11 | Maruzen Petrochemical Co Ltd | Continuous manufacturing method of cyclic carbonate |
| AU2014317208B2 (en) * | 2013-09-03 | 2018-11-01 | Basf Se | Amorphous material and the use thereof |
| WO2024214491A1 (ja) * | 2023-04-14 | 2024-10-17 | 信越化学工業株式会社 | フェノール部位を有する固定化第四級ホスホニウム塩およびその製造方法、並びにこれを用いた環状カーボネートの製造方法 |
Family Cites Families (37)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2873282A (en) * | 1952-04-05 | 1959-02-10 | Jefferson Chem Co Inc | Catalytic process for producing alkylene carbonates |
| US2773070A (en) * | 1952-10-31 | 1956-12-04 | Jefferson Chem Co Inc | Catalytic process for producing alkylene carbonates |
| US2924608A (en) * | 1957-12-30 | 1960-02-09 | Olin Mathieson | Ethylene carbonates |
| US2994705A (en) * | 1958-12-08 | 1961-08-01 | Pure Oil Co | Preparation of cyclic alkylene carbonates in the presence of organic phosphonium compounds |
| DE1274578B (de) * | 1965-01-21 | 1968-08-08 | Bayer Ag | Verfahren zur Herstellung von Cycloalkylaminverbindungen |
| US3803201A (en) * | 1971-02-22 | 1974-04-09 | Dow Chemical Co | Synthesis of dimethyl carbonate |
| US3748345A (en) * | 1971-07-02 | 1973-07-24 | Shell Oil Co | Preparation of alkylene carbonates by reaction of alkylene oxides with carbon dioxide |
| DE2748718A1 (de) * | 1977-10-29 | 1979-05-03 | Bayer Ag | Verfahren zur herstellung von dialkylcarbonaten |
| US4314945A (en) * | 1977-12-22 | 1982-02-09 | Union Carbide Corporation | Alkylene carbonate process |
| CA1224793A (en) * | 1981-12-02 | 1987-07-28 | Halcon Sd Group, Inc. (The) | Preparation of alkylene carbonates |
| US4400559A (en) * | 1982-06-14 | 1983-08-23 | The Halcon Sd Group, Inc. | Process for preparing ethylene glycol |
| US4508927A (en) * | 1983-08-02 | 1985-04-02 | The Halcon Sd Group, Inc. | Preparation of glycols from ethylene oxide |
| US4691041A (en) * | 1986-01-03 | 1987-09-01 | Texaco Inc. | Process for production of ethylene glycol and dimethyl carbonate |
| DE4030283A1 (de) * | 1990-09-25 | 1992-03-26 | Ruetgerswerke Ag | Verfahren zur herstellung cyclischer carbonate |
| JP3079560B2 (ja) * | 1990-11-07 | 2000-08-21 | 松下電器産業株式会社 | プリプラ式射出成形機およびその制御方法 |
| GB2255972A (en) * | 1991-04-12 | 1992-11-25 | Davy Res & Dev Ltd | Production of diaryl carbonates. |
| DE4129316A1 (de) * | 1991-09-03 | 1993-03-04 | Bayer Ag | Verfahren zur kontinuierlichen herstellung von dialkylcarbonaten |
| DE4216121A1 (de) * | 1992-05-15 | 1993-11-18 | Bayer Ag | Verfahren zur kontinuierlichen Herstellung von Dialkylcarbonaten |
| DE4318893A1 (de) * | 1993-06-07 | 1994-12-08 | Bayer Ag | Reaktor und damit durchzuführendes kontinuierliches Verfahren zur Herstellung von Ethylenglykolcarbonat bzw. Propylenglykolcarbonat |
| DE4318892A1 (de) * | 1993-06-07 | 1994-12-08 | Bayer Ag | Verfahren zur Herstellung von Propylenglykolcarbonat |
| DE4342713A1 (de) * | 1993-12-15 | 1995-06-22 | Bayer Ag | Verfahren zur Abtrennung von Methanol aus einem Gemisch von Dimethylcarbonat und Methanol |
| DE69620470T2 (de) * | 1995-12-22 | 2002-11-21 | Asahi Kasei Kabushiki Kaisha, Osaka | Verfahren zur kontinuierlichen herstellung von dialkylcarbonaten und diolen |
| SG77264A1 (en) * | 1998-08-10 | 2000-12-19 | Mitsubishi Chem Corp | Process for producing an alkylene glycol |
| US6156160A (en) * | 1998-10-07 | 2000-12-05 | Huntsman Petrochemical Corporation | Alkylene carbonate process |
| JP3659038B2 (ja) * | 1998-12-22 | 2005-06-15 | 三菱化学株式会社 | エチレングリコールの製造方法 |
| AU2827900A (en) * | 1999-03-03 | 2000-09-21 | Asahi Kasei Kabushiki Kaisha | Process for continuously producing dialkyl carbonate and diol |
| US6407279B1 (en) * | 1999-11-19 | 2002-06-18 | Exxonmobil Chemical Patents Inc. | Integrated process for preparing dialkyl carbonates and diols |
| US6294684B1 (en) * | 1999-12-08 | 2001-09-25 | General Electric Company | Method and apparatus for the continuous production of diaryl carbonates |
| JP3659109B2 (ja) * | 2000-01-19 | 2005-06-15 | 三菱化学株式会社 | エチレングリコールと炭酸エステルの併産方法 |
| US6392078B1 (en) * | 2000-06-12 | 2002-05-21 | Catalytic Distillation Technologies | Process and catalyst for making dialkyl carbonates |
| US6774256B2 (en) * | 2001-06-22 | 2004-08-10 | Exxonmobil Chemical Patents Inc. | Low corrosive integrated process for preparing dialkyl carbonates |
| US6573396B2 (en) * | 2001-10-12 | 2003-06-03 | Exxonmobil Chemical Patents Inc. | Co-production of dialkyl carbonates and diols with treatment of hydroxy alkyl carbonate |
| JP2003267970A (ja) * | 2002-03-13 | 2003-09-25 | Mitsubishi Chemicals Corp | エチレンカーボネートの製造方法 |
| JP2004099554A (ja) * | 2002-09-11 | 2004-04-02 | Mitsubishi Chemicals Corp | アルキレングリコール及びジアルキルカーボネートの併産方法 |
| TW200503997A (en) * | 2002-12-20 | 2005-02-01 | Shell Int Research | Process for the preparation of alkylene glycol |
| ES2293327T3 (es) * | 2003-06-30 | 2008-03-16 | Shell Internationale Research Maatschappij B.V. | Procedimiento para la preparacion de carbonato de propileno. |
| TWI382979B (zh) * | 2006-02-22 | 2013-01-21 | Shell Int Research | 碳酸伸烷酯之生產方法及由此生產的碳酸伸烷酯於烷二醇及碳酸二烷酯之製造中的用途 |
-
2007
- 2007-03-09 TW TW096108219A patent/TWI387584B/zh not_active IP Right Cessation
- 2007-03-12 BR BRPI0708285-1A patent/BRPI0708285A2/pt not_active Application Discontinuation
- 2007-03-12 WO PCT/EP2007/052270 patent/WO2007104730A1/en not_active Ceased
- 2007-03-12 JP JP2008558796A patent/JP5551876B2/ja not_active Expired - Fee Related
- 2007-03-12 RU RU2008140313/04A patent/RU2008140313A/ru not_active Application Discontinuation
- 2007-03-12 MX MX2008011415A patent/MX2008011415A/es not_active Application Discontinuation
- 2007-03-12 EP EP07726784A patent/EP1994018B1/en not_active Not-in-force
- 2007-03-12 CN CN2007800075665A patent/CN101553479B/zh not_active Expired - Fee Related
- 2007-03-12 US US11/684,873 patent/US20070213542A1/en not_active Abandoned
- 2007-03-12 CA CA002641997A patent/CA2641997A1/en not_active Abandoned
- 2007-03-12 ES ES07726784T patent/ES2396866T3/es active Active
- 2007-03-12 KR KR1020087024405A patent/KR20080110782A/ko not_active Withdrawn
- 2007-03-12 AU AU2007224469A patent/AU2007224469A1/en not_active Abandoned
-
2013
- 2013-11-29 JP JP2013247358A patent/JP5726278B2/ja not_active Expired - Fee Related
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