JP2013507501A5 - - Google Patents
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- JP2013507501A5 JP2013507501A5 JP2012533605A JP2012533605A JP2013507501A5 JP 2013507501 A5 JP2013507501 A5 JP 2013507501A5 JP 2012533605 A JP2012533605 A JP 2012533605A JP 2012533605 A JP2012533605 A JP 2012533605A JP 2013507501 A5 JP2013507501 A5 JP 2013507501A5
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- JP
- Japan
- Prior art keywords
- component
- acid
- weight
- mixture
- polyester
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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- 239000000203 mixture Substances 0.000 claims description 20
- 229920000728 polyester Polymers 0.000 claims description 13
- -1 polypropylene carbonate Polymers 0.000 claims description 11
- 125000001931 aliphatic group Chemical group 0.000 claims description 9
- 150000001875 compounds Chemical class 0.000 claims description 9
- OFOBLEOULBTSOW-UHFFFAOYSA-N Malonic acid Chemical compound OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 claims description 7
- 150000002148 esters Chemical class 0.000 claims description 7
- 125000003118 aryl group Chemical group 0.000 claims description 5
- PBLZLIFKVPJDCO-UHFFFAOYSA-N 12-aminododecanoic acid Chemical compound NCCCCCCCCCCCC(O)=O PBLZLIFKVPJDCO-UHFFFAOYSA-N 0.000 claims description 4
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 claims description 4
- 239000002253 acid Substances 0.000 claims description 4
- 150000001718 carbodiimides Chemical class 0.000 claims description 4
- JBKVHLHDHHXQEQ-UHFFFAOYSA-N epsilon-caprolactam Chemical compound O=C1CCCCCN1 JBKVHLHDHHXQEQ-UHFFFAOYSA-N 0.000 claims description 4
- 239000000314 lubricant Substances 0.000 claims description 4
- 239000002667 nucleating agent Substances 0.000 claims description 4
- 125000002924 primary amino group Chemical group [H]N([H])* 0.000 claims description 4
- 238000006243 chemical reaction Methods 0.000 claims description 3
- 150000002009 diols Chemical class 0.000 claims description 3
- 150000002118 epoxides Chemical class 0.000 claims description 3
- 150000004893 oxazines Chemical class 0.000 claims description 3
- 150000002918 oxazolines Chemical class 0.000 claims description 3
- GUOSQNAUYHMCRU-UHFFFAOYSA-N 11-Aminoundecanoic acid Chemical compound NCCCCCCCCCCC(O)=O GUOSQNAUYHMCRU-UHFFFAOYSA-N 0.000 claims description 2
- SLXKOJJOQWFEFD-UHFFFAOYSA-N 6-aminohexanoic acid Chemical compound NCCCCCC(O)=O SLXKOJJOQWFEFD-UHFFFAOYSA-N 0.000 claims description 2
- 229910052582 BN Inorganic materials 0.000 claims description 2
- PZNSFCLAULLKQX-UHFFFAOYSA-N Boron nitride Chemical compound N#B PZNSFCLAULLKQX-UHFFFAOYSA-N 0.000 claims description 2
- UAUDZVJPLUQNMU-UHFFFAOYSA-N Erucasaeureamid Natural products CCCCCCCCC=CCCCCCCCCCCCC(N)=O UAUDZVJPLUQNMU-UHFFFAOYSA-N 0.000 claims description 2
- 229960002684 aminocaproic acid Drugs 0.000 claims description 2
- 229910000019 calcium carbonate Inorganic materials 0.000 claims description 2
- BVKZGUZCCUSVTD-UHFFFAOYSA-N carbonic acid Chemical compound OC(O)=O BVKZGUZCCUSVTD-UHFFFAOYSA-N 0.000 claims description 2
- UAUDZVJPLUQNMU-KTKRTIGZSA-N erucamide Chemical compound CCCCCCCC\C=C/CCCCCCCCCCCC(N)=O UAUDZVJPLUQNMU-KTKRTIGZSA-N 0.000 claims description 2
- 125000001033 ether group Chemical group 0.000 claims description 2
- 125000001495 ethyl group Chemical group [H]C([H])([H])C([H])([H])* 0.000 claims description 2
- 125000000524 functional group Chemical group 0.000 claims description 2
- 239000012948 isocyanate Substances 0.000 claims description 2
- 150000002513 isocyanates Chemical class 0.000 claims description 2
- 150000003951 lactams Chemical class 0.000 claims description 2
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims description 2
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 claims description 2
- 150000002978 peroxides Chemical class 0.000 claims description 2
- 125000000843 phenylene group Chemical group C1(=C(C=CC=C1)*)* 0.000 claims description 2
- 229920001707 polybutylene terephthalate Polymers 0.000 claims description 2
- 229920000139 polyethylene terephthalate Polymers 0.000 claims description 2
- 239000005020 polyethylene terephthalate Substances 0.000 claims description 2
- 125000001273 sulfonato group Chemical group [O-]S(*)(=O)=O 0.000 claims description 2
- 239000000454 talc Substances 0.000 claims description 2
- 229910052623 talc Inorganic materials 0.000 claims description 2
- 238000000034 method Methods 0.000 claims 19
- 229920000642 polymer Polymers 0.000 claims 7
- 239000003054 catalyst Substances 0.000 claims 4
- 238000005809 transesterification reaction Methods 0.000 claims 4
- 239000004970 Chain extender Substances 0.000 claims 3
- 229920000229 biodegradable polyester Polymers 0.000 claims 3
- 239000004622 biodegradable polyester Substances 0.000 claims 3
- 230000032050 esterification Effects 0.000 claims 3
- 238000005886 esterification reaction Methods 0.000 claims 3
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims 2
- 239000005057 Hexamethylene diisocyanate Substances 0.000 claims 2
- KKEYFWRCBNTPAC-UHFFFAOYSA-N Terephthalic acid Chemical compound OC(=O)C1=CC=C(C(O)=O)C=C1 KKEYFWRCBNTPAC-UHFFFAOYSA-N 0.000 claims 2
- WNLRTRBMVRJNCN-UHFFFAOYSA-N adipic acid Chemical compound OC(=O)CCCCC(O)=O WNLRTRBMVRJNCN-UHFFFAOYSA-N 0.000 claims 2
- WERYXYBDKMZEQL-UHFFFAOYSA-N butane-1,4-diol Chemical compound OCCCCO WERYXYBDKMZEQL-UHFFFAOYSA-N 0.000 claims 2
- 238000010924 continuous production Methods 0.000 claims 2
- RRAMGCGOFNQTLD-UHFFFAOYSA-N hexamethylene diisocyanate Chemical compound O=C=NCCCCCCN=C=O RRAMGCGOFNQTLD-UHFFFAOYSA-N 0.000 claims 2
- 239000011574 phosphorus Substances 0.000 claims 2
- 229910052698 phosphorus Inorganic materials 0.000 claims 2
- 229920000747 poly(lactic acid) Polymers 0.000 claims 2
- 239000004626 polylactic acid Substances 0.000 claims 2
- 229920002959 polymer blend Polymers 0.000 claims 2
- 239000002516 radical scavenger Substances 0.000 claims 2
- CXMXRPHRNRROMY-UHFFFAOYSA-N sebacic acid Chemical compound OC(=O)CCCCCCCCC(O)=O CXMXRPHRNRROMY-UHFFFAOYSA-N 0.000 claims 2
- DNIAPMSPPWPWGF-VKHMYHEASA-N (+)-propylene glycol Chemical compound C[C@H](O)CO DNIAPMSPPWPWGF-VKHMYHEASA-N 0.000 claims 1
- YPFDHNVEDLHUCE-UHFFFAOYSA-N 1,3-propanediol Substances OCCCO YPFDHNVEDLHUCE-UHFFFAOYSA-N 0.000 claims 1
- AEMRFAOFKBGASW-UHFFFAOYSA-N Glycolic acid Polymers OCC(O)=O AEMRFAOFKBGASW-UHFFFAOYSA-N 0.000 claims 1
- 229920000954 Polyglycolide Polymers 0.000 claims 1
- KDYFGRWQOYBRFD-UHFFFAOYSA-N Succinic acid Natural products OC(=O)CCC(O)=O KDYFGRWQOYBRFD-UHFFFAOYSA-N 0.000 claims 1
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 claims 1
- ZJCCRDAZUWHFQH-UHFFFAOYSA-N Trimethylolpropane Chemical compound CCC(CO)(CO)CO ZJCCRDAZUWHFQH-UHFFFAOYSA-N 0.000 claims 1
- 239000000654 additive Substances 0.000 claims 1
- 239000001361 adipic acid Substances 0.000 claims 1
- 235000011037 adipic acid Nutrition 0.000 claims 1
- 229920003232 aliphatic polyester Polymers 0.000 claims 1
- KDYFGRWQOYBRFD-NUQCWPJISA-N butanedioic acid Chemical group O[14C](=O)CC[14C](O)=O KDYFGRWQOYBRFD-NUQCWPJISA-N 0.000 claims 1
- 229920002301 cellulose acetate Polymers 0.000 claims 1
- 150000001991 dicarboxylic acids Chemical class 0.000 claims 1
- 239000011552 falling film Substances 0.000 claims 1
- 235000011187 glycerol Nutrition 0.000 claims 1
- 238000011065 in-situ storage Methods 0.000 claims 1
- 239000007788 liquid Substances 0.000 claims 1
- 238000004519 manufacturing process Methods 0.000 claims 1
- WXZMFSXDPGVJKK-UHFFFAOYSA-N pentaerythritol Chemical compound OCC(CO)(CO)CO WXZMFSXDPGVJKK-UHFFFAOYSA-N 0.000 claims 1
- 239000005014 poly(hydroxyalkanoate) Substances 0.000 claims 1
- 229920001610 polycaprolactone Polymers 0.000 claims 1
- 239000004632 polycaprolactone Substances 0.000 claims 1
- 238000006068 polycondensation reaction Methods 0.000 claims 1
- 229920000903 polyhydroxyalkanoate Polymers 0.000 claims 1
- 229920000379 polypropylene carbonate Polymers 0.000 claims 1
- 229920000166 polytrimethylene carbonate Polymers 0.000 claims 1
- 239000011541 reaction mixture Substances 0.000 claims 1
- 230000003068 static effect Effects 0.000 claims 1
- 229910052719 titanium Inorganic materials 0.000 claims 1
- 239000010936 titanium Substances 0.000 claims 1
- 210000000707 wrist Anatomy 0.000 claims 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP09173193.5 | 2009-10-15 | ||
| EP09173193 | 2009-10-15 | ||
| PCT/EP2010/065233 WO2011045293A1 (de) | 2009-10-15 | 2010-10-12 | Verfahren zur kontinuierlichen herstellung von polyestermischungen |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2013507501A JP2013507501A (ja) | 2013-03-04 |
| JP2013507501A5 true JP2013507501A5 (enExample) | 2013-11-28 |
| JP5680095B2 JP5680095B2 (ja) | 2015-03-04 |
Family
ID=43416885
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2012533605A Expired - Fee Related JP5680095B2 (ja) | 2009-10-15 | 2010-10-12 | ポリエステル混合物の連続的な製造法 |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US8754173B2 (enExample) |
| EP (1) | EP2488585B1 (enExample) |
| JP (1) | JP5680095B2 (enExample) |
| KR (1) | KR101760965B1 (enExample) |
| CN (1) | CN102549072B (enExample) |
| BR (1) | BR112012008514A2 (enExample) |
| WO (1) | WO2011045293A1 (enExample) |
Families Citing this family (44)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR101760965B1 (ko) | 2009-10-15 | 2017-07-24 | 바스프 에스이 | 폴리에스테르 혼합물의 연속 제조 방법 |
| CN102838856B (zh) * | 2011-06-23 | 2015-06-17 | 中国石油化工股份有限公司 | 一种生物可降解的复合物及其制备方法和一次性用品 |
| CN102838855B (zh) * | 2011-06-23 | 2015-06-17 | 中国石油化工股份有限公司 | 生物可降解的复合物及其制备方法和一次性用品 |
| US9096758B2 (en) | 2011-07-29 | 2015-08-04 | Basf Se | Biodegradable polyester foil |
| CN102358778B (zh) * | 2011-07-29 | 2014-06-18 | 上海载和实业投资有限公司 | 一种新型生物降解母料及其制备方法 |
| CN102924902A (zh) * | 2011-08-12 | 2013-02-13 | 中国石油化工股份有限公司 | 一种塑料制品及其制备方法 |
| CN102924676B (zh) * | 2011-08-12 | 2015-08-19 | 中国石油化工股份有限公司 | 一种透明共聚酯及其制备方法 |
| FI124410B (en) * | 2012-10-26 | 2014-08-15 | Stora Enso Oyj | Method for the production of biodegradable packaging material, biodegradable packaging material and packaging or container thereof |
| ES2599165T3 (es) * | 2012-10-29 | 2017-01-31 | Uhde Inventa-Fischer Gmbh | Procedimiento para la preparación de un poliéster o un copoliéster de alto peso molecular así como mezclas poliméricas que los contienen |
| WO2014075998A1 (de) * | 2012-11-15 | 2014-05-22 | Basf Se | Biologisch abbaubare polyestermischung |
| CN103087493B (zh) * | 2012-11-27 | 2015-09-09 | 山西省化工研究所 | 脂肪二羧酸二酰肼类成核剂的用途 |
| KR101992392B1 (ko) | 2012-12-12 | 2019-09-30 | (주)새한폴리머 | 생분해성 지방족/방향족 폴리에스테르 공중합체의 연속 제조방법 |
| KR20140076354A (ko) | 2012-12-12 | 2014-06-20 | 삼성정밀화학 주식회사 | 생분해성 지방족/방향족 폴리에스테르 공중합체의 연속 제조방법 |
| KR20140076355A (ko) | 2012-12-12 | 2014-06-20 | 삼성정밀화학 주식회사 | 생분해성 지방족/방향족 폴리에스테르 공중합체의 연속 제조방법 |
| CN103102477B (zh) * | 2013-01-05 | 2014-12-10 | 金发科技股份有限公司 | 一种聚酯、制备方法及其应用 |
| EP2759569B1 (en) * | 2013-01-24 | 2019-10-16 | So.F.Ter. Tecnopolimeri Srl | A polyactic acid-based composition, a process for processing a polylactic acid based composition into a moulded article |
| KR20150047939A (ko) * | 2013-10-25 | 2015-05-06 | 삼성정밀화학 주식회사 | 생분해성 폴리에스테르 수지 컴파운드 및 그로부터 얻어진 발포체 |
| US9139505B2 (en) | 2013-11-08 | 2015-09-22 | Eastman Chemical Company | Production of terephthalic acid di-esters using alcohol-amine promoters |
| WO2016130575A1 (en) | 2015-02-13 | 2016-08-18 | Boston Scientific Neuromodulation Corporation | Retractor and tools for implantation of electrical stimulation leads |
| WO2016176211A1 (en) | 2015-04-28 | 2016-11-03 | Boston Scientific Neuromodulation Corporation | Systems and methods for making and using a lead introducer with a seal for an electrical stimulation system |
| CN105295321A (zh) * | 2015-07-13 | 2016-02-03 | 中国石油大学(北京) | 油气田作业用的可降解材料及其制备方法 |
| KR102644022B1 (ko) | 2015-12-28 | 2024-03-08 | 주식회사 안코바이오플라스틱스 | 생분해성 폴리에스테르 수지의 반연속식 제조 방법 |
| KR101658521B1 (ko) * | 2016-04-29 | 2016-09-21 | 문창영 | 생분해성 폐그물의 재생 방법 |
| CN106009571B (zh) * | 2016-07-15 | 2018-05-04 | 扬州大学 | 一种聚己内酯/纤维素纳米晶体复合材料的制备方法 |
| CN107459784B (zh) * | 2016-12-13 | 2020-05-19 | 金发科技股份有限公司 | 一种可生物降解聚酯组合物 |
| EP3559081B1 (en) * | 2016-12-22 | 2023-11-22 | Solvay SA | Glycolic acid polymer |
| PT3630869T (pt) | 2017-05-31 | 2021-05-18 | Basf Se | Poliéster alifático-aromático com elevado índice de brancura |
| CN108219390A (zh) * | 2017-12-05 | 2018-06-29 | 湖北光合生物科技有限公司 | 聚己二酸-对苯二甲酸丁二醇酯复合材料及其制备方法 |
| US10683399B2 (en) | 2018-06-26 | 2020-06-16 | Intrinsic Advanced Materials, LLC | Biodegradable textiles, masterbatches, and method of making biodegradable fibers |
| PT3891208T (pt) | 2018-12-06 | 2023-05-02 | Basf Se | Processo para produzir um (co) poliéster |
| CN113453749B (zh) | 2019-02-19 | 2024-09-20 | 波士顿科学神经调制公司 | 引线引入器以及包括该引线引入器的系统和方法 |
| KR20210145182A (ko) * | 2019-03-19 | 2021-12-01 | 바스프 에스이 | 적어도 2개의 중합체 용융물의 조합된 가공 방법 |
| EP3941963B1 (en) * | 2019-03-19 | 2023-03-01 | Basf Se | A method for the combined production of at least two target products |
| CN110183617B (zh) * | 2019-07-01 | 2021-09-07 | 黄山正杰新材料有限公司 | 一种耐磨性优的透明粉用50：50聚酯树脂及其制备方法与应用 |
| FR3098519B1 (fr) * | 2019-07-10 | 2021-07-23 | Carbiolice | Matiere plastique à haute teneur en pla comprenant du ppgdge |
| KR20220114578A (ko) | 2019-12-10 | 2022-08-17 | 티코나 엘엘씨 | 블룸-저항성 또는 바이오-기반 가소제를 함유하는 셀룰로오스 에스테르 조성물 |
| CN111393665A (zh) * | 2020-05-04 | 2020-07-10 | 常州市五好新材料科技有限公司 | 一种钙金属有机骨架材料的制备方法和应用 |
| CN113136033B (zh) * | 2021-04-30 | 2022-08-19 | 成都新晨新材科技有限公司 | 一种pbo预聚合工艺的控制方法 |
| CN114763429B (zh) * | 2021-05-17 | 2024-01-26 | 瑞拓峰高新科技有限公司 | 一种具有高度相容性的生物降解聚酯合金的合成方法 |
| CN113846423B (zh) * | 2021-10-15 | 2023-02-28 | 嘉兴学院 | 一种生物全降解复合纤维膜的制备方法 |
| CN114057996A (zh) * | 2021-12-14 | 2022-02-18 | 中国天辰工程有限公司 | 一种对苯二甲酸基聚酯的高效合成方法 |
| CN117050486A (zh) * | 2022-05-07 | 2023-11-14 | 深圳市裕同包装科技股份有限公司 | 用于制造阻隔层的组合物、阻隔层及其制造方法和包装材料 |
| CN114835871B (zh) * | 2022-06-06 | 2024-06-18 | 惠州博科环保新材料有限公司 | 一种可生物降解的嵌段共聚酯的合成方法以及嵌段共聚酯 |
| CN119330652B (zh) * | 2024-12-23 | 2025-02-25 | 山东招和环保建材有限责任公司 | 一种工业废渣生态环保透水砖及其制备方法 |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE4440858A1 (de) | 1994-11-15 | 1996-05-23 | Basf Ag | Biologisch abbaubare Polymere, Verfahren zu deren Herstellung sowie deren Verwendung zur Herstellung bioabbaubarer Formkörper |
| DE4440837A1 (de) * | 1994-11-15 | 1996-05-23 | Basf Ag | Biologisch abbaubare Polymere, Verfahren zu deren Herstellung sowie deren Verwendung zur Herstellung bioabbaubarer Formkörper |
| ES2130526T3 (es) | 1994-12-30 | 1999-07-01 | Fischer Karl Ind Gmbh | Dispositivo de reactor para medios poco viscosos y medios de mayor viscosidad. |
| DE19509551A1 (de) | 1995-03-16 | 1996-09-19 | Basf Ag | Verfahren zur kontinuierlichen Herstellung von thermoplastischen Polyestern |
| CN1211312C (zh) | 1996-07-01 | 2005-07-20 | 宇部兴产株式会社 | 陶瓷复合材料和多孔陶瓷材料及其生产方法 |
| DE19929790A1 (de) * | 1999-06-29 | 2001-01-04 | Basf Ag | Verfahren zur kontinuierlichen Herstellung von Polybutylenterephthalat aus Terephthalsäure und Butandiol |
| US20040014883A1 (en) * | 2000-09-18 | 2004-01-22 | Motonori Yamamoto | Polyester film |
| DE10155419B4 (de) * | 2001-11-12 | 2005-06-16 | Inventa-Fischer Gmbh & Co. Kg | Verfahren zur kontinuierlichen Herstellung von hochmolekularem Polyester sowie Vorrichtung zur Durchführung des Verfahrens |
| DE10351085A1 (de) | 2003-10-31 | 2005-06-16 | Inventa-Fischer Gmbh & Co. Kg | Turmreaktor sowie dessen Verwendung zur kontinuierlichen Herstellung von hochmolekularem Polyester |
| WO2006074815A1 (de) | 2005-01-12 | 2006-07-20 | Basf Aktiengesellschaft | Biologisch abbaubare polyestermischung |
| DE102005053068B4 (de) | 2005-11-04 | 2017-05-11 | Basf Se | Sebazinsäurehaltige Polyester und Polyestermischung, Verfahren zu deren Herstellung sowie ein Verzweigerbatch und die Verwendung der Polyestermischung |
| US20090234042A1 (en) | 2006-04-27 | 2009-09-17 | Basf Se | Transparent blends of polypropylene carbonate |
| ES2397765T3 (es) * | 2008-04-15 | 2013-03-11 | Basf Se | Proceso para la producción continua de poliésteres biodegradables |
| CN102007160B (zh) | 2008-04-15 | 2013-05-29 | 巴斯夫欧洲公司 | 连续生产生物降解聚酯的方法 |
| CN102165012A (zh) | 2008-08-01 | 2011-08-24 | 巴斯夫欧洲公司 | 提高生物降解聚酯耐水解性的方法 |
| KR101760965B1 (ko) | 2009-10-15 | 2017-07-24 | 바스프 에스이 | 폴리에스테르 혼합물의 연속 제조 방법 |
| KR20130141425A (ko) | 2010-07-19 | 2013-12-26 | 바스프 에스이 | 폴리에스테르의 분자량 증가 방법 |
| US20120016090A1 (en) | 2010-07-19 | 2012-01-19 | Basf Se | Process for increasing the molecular weight of polyesters |
-
2010
- 2010-10-12 KR KR1020127012339A patent/KR101760965B1/ko not_active Expired - Fee Related
- 2010-10-12 WO PCT/EP2010/065233 patent/WO2011045293A1/de not_active Ceased
- 2010-10-12 JP JP2012533605A patent/JP5680095B2/ja not_active Expired - Fee Related
- 2010-10-12 BR BR112012008514A patent/BR112012008514A2/pt not_active IP Right Cessation
- 2010-10-12 EP EP10770765.5A patent/EP2488585B1/de not_active Not-in-force
- 2010-10-12 US US13/501,978 patent/US8754173B2/en not_active Expired - Fee Related
- 2010-10-12 CN CN201080045769.5A patent/CN102549072B/zh not_active Expired - Fee Related
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