JP2013212952A - 炭化珪素単結晶の製造方法 - Google Patents
炭化珪素単結晶の製造方法 Download PDFInfo
- Publication number
- JP2013212952A JP2013212952A JP2012083613A JP2012083613A JP2013212952A JP 2013212952 A JP2013212952 A JP 2013212952A JP 2012083613 A JP2012083613 A JP 2012083613A JP 2012083613 A JP2012083613 A JP 2012083613A JP 2013212952 A JP2013212952 A JP 2013212952A
- Authority
- JP
- Japan
- Prior art keywords
- silicon carbide
- single crystal
- raw material
- carbide single
- seed substrate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- HBMJWWWQQXIZIP-UHFFFAOYSA-N silicon carbide Chemical compound [Si+]#[C-] HBMJWWWQQXIZIP-UHFFFAOYSA-N 0.000 title claims abstract description 280
- 229910010271 silicon carbide Inorganic materials 0.000 title claims abstract description 280
- 239000013078 crystal Substances 0.000 title claims abstract description 171
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 52
- 238000000034 method Methods 0.000 title abstract description 21
- 239000002994 raw material Substances 0.000 claims abstract description 105
- 239000000758 substrate Substances 0.000 claims abstract description 84
- 238000005092 sublimation method Methods 0.000 claims abstract description 7
- 238000010438 heat treatment Methods 0.000 claims description 12
- 238000000859 sublimation Methods 0.000 claims description 10
- 230000008022 sublimation Effects 0.000 claims description 10
- 230000005855 radiation Effects 0.000 claims description 6
- 230000000052 comparative effect Effects 0.000 description 8
- 238000009826 distribution Methods 0.000 description 8
- 239000000463 material Substances 0.000 description 7
- 238000001953 recrystallisation Methods 0.000 description 4
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 3
- 229910052799 carbon Inorganic materials 0.000 description 3
- 230000004048 modification Effects 0.000 description 3
- 238000012986 modification Methods 0.000 description 3
- 238000002360 preparation method Methods 0.000 description 3
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 2
- 230000007423 decrease Effects 0.000 description 2
- 239000004065 semiconductor Substances 0.000 description 2
- 229910052710 silicon Inorganic materials 0.000 description 2
- 239000010703 silicon Substances 0.000 description 2
- 238000003763 carbonization Methods 0.000 description 1
- 230000015556 catabolic process Effects 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 230000006866 deterioration Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000002050 diffraction method Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000006698 induction Effects 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B23/00—Single-crystal growth by condensing evaporated or sublimed materials
- C30B23/02—Epitaxial-layer growth
- C30B23/06—Heating of the deposition chamber, the substrate or the materials to be evaporated
- C30B23/066—Heating of the material to be evaporated
-
- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B23/00—Single-crystal growth by condensing evaporated or sublimed materials
- C30B23/02—Epitaxial-layer growth
- C30B23/025—Epitaxial-layer growth characterised by the substrate
-
- C—CHEMISTRY; METALLURGY
- C30—CRYSTAL GROWTH
- C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
- C30B29/00—Single crystals or homogeneous polycrystalline material with defined structure characterised by the material or by their shape
- C30B29/10—Inorganic compounds or compositions
- C30B29/36—Carbides
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Crystallography & Structural Chemistry (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Crystals, And After-Treatments Of Crystals (AREA)
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2012083613A JP2013212952A (ja) | 2012-04-02 | 2012-04-02 | 炭化珪素単結晶の製造方法 |
| US13/780,127 US20130255568A1 (en) | 2012-04-02 | 2013-02-28 | Method for manufacturing silicon carbide single crystal |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2012083613A JP2013212952A (ja) | 2012-04-02 | 2012-04-02 | 炭化珪素単結晶の製造方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JP2013212952A true JP2013212952A (ja) | 2013-10-17 |
| JP2013212952A5 JP2013212952A5 (https=) | 2015-02-19 |
Family
ID=49233158
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2012083613A Pending JP2013212952A (ja) | 2012-04-02 | 2012-04-02 | 炭化珪素単結晶の製造方法 |
Country Status (2)
| Country | Link |
|---|---|
| US (1) | US20130255568A1 (https=) |
| JP (1) | JP2013212952A (https=) |
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2015212207A (ja) * | 2014-05-02 | 2015-11-26 | 新日鐵住金株式会社 | 炭化珪素単結晶インゴットの製造方法 |
| JP2016088801A (ja) * | 2014-11-04 | 2016-05-23 | 住友電気工業株式会社 | 炭化珪素単結晶の製造装置および炭化珪素単結晶の製造方法 |
| JP2016088789A (ja) * | 2014-10-31 | 2016-05-23 | 住友電気工業株式会社 | 炭化珪素単結晶の製造装置および炭化珪素単結晶の製造方法 |
| JP2016088812A (ja) * | 2014-11-06 | 2016-05-23 | 新日鐵住金株式会社 | 炭化珪素単結晶インゴットの製造方法及び製造装置 |
| JP2019073441A (ja) * | 2019-02-20 | 2019-05-16 | 住友電気工業株式会社 | 炭化珪素単結晶の製造装置および炭化珪素単結晶の製造方法 |
| KR102187449B1 (ko) * | 2019-05-28 | 2020-12-11 | 에스케이씨 주식회사 | 탄화규소 잉곳의 제조방법, 탄화규소 잉곳 및 이의 성장 시스템 |
| JP2021104912A (ja) * | 2019-12-26 | 2021-07-26 | 昭和電工株式会社 | 単結晶製造装置 |
| US11359306B2 (en) | 2019-10-29 | 2022-06-14 | Senic Inc. | Method for preparing a SiC ingot and device for preparing a SiC ingot wherein electrical resistance of crucible body is 2.9 ohms or more |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US10724151B2 (en) * | 2014-10-31 | 2020-07-28 | Sumitomo Electric Industries, Ltd. | Device of manufacturing silicon carbide single crystal |
| EP4407079A3 (en) | 2015-09-24 | 2024-10-30 | Pallidus, Inc. | Vapor deposition apparatus and techniques using high purity polymer derived silicon carbide |
| CN113652740A (zh) * | 2021-08-27 | 2021-11-16 | 宁波合盛新材料有限公司 | 一种碳化硅单晶的制备方法及一种单晶长晶炉、单晶长晶炉的加热装置 |
| EP4431643A1 (en) * | 2023-03-15 | 2024-09-18 | SiCrystal GmbH | Sublimation system and method of growing at least one single crystal |
| CN116676661B (zh) * | 2023-08-03 | 2023-10-17 | 北京青禾晶元半导体科技有限责任公司 | 一种在溶液法生长碳化硅过程中防止籽晶掉落的方法 |
Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2005112637A (ja) * | 2003-10-02 | 2005-04-28 | Bridgestone Corp | 炭化ケイ素単結晶製造装置 |
| JP2006096578A (ja) * | 2004-09-28 | 2006-04-13 | Nippon Steel Corp | 炭化珪素単結晶の製造方法及び炭化珪素単結晶インゴット |
| JP2006143497A (ja) * | 2004-11-17 | 2006-06-08 | Bridgestone Corp | 炭化ケイ素単結晶製造装置 |
| JP2008074662A (ja) * | 2006-09-21 | 2008-04-03 | Nippon Steel Corp | 炭化珪素単結晶製造装置 |
| JP2011219287A (ja) * | 2010-04-06 | 2011-11-04 | Nippon Steel Corp | 炭化珪素単結晶インゴットの製造方法及び炭化珪素単結晶インゴット |
| JP2011219295A (ja) * | 2010-04-07 | 2011-11-04 | Nippon Steel Corp | 炭化珪素単結晶インゴットの製造装置 |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6863728B2 (en) * | 2001-02-14 | 2005-03-08 | The Fox Group, Inc. | Apparatus for growing low defect density silicon carbide |
| DE102008063129B4 (de) * | 2008-12-24 | 2013-05-16 | Sicrystal Ag | Herstellungsverfahren für einen codotierten SiC-Volumeneinkristall und hochohmiges SiC-Substrat |
-
2012
- 2012-04-02 JP JP2012083613A patent/JP2013212952A/ja active Pending
-
2013
- 2013-02-28 US US13/780,127 patent/US20130255568A1/en not_active Abandoned
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2005112637A (ja) * | 2003-10-02 | 2005-04-28 | Bridgestone Corp | 炭化ケイ素単結晶製造装置 |
| JP2006096578A (ja) * | 2004-09-28 | 2006-04-13 | Nippon Steel Corp | 炭化珪素単結晶の製造方法及び炭化珪素単結晶インゴット |
| JP2006143497A (ja) * | 2004-11-17 | 2006-06-08 | Bridgestone Corp | 炭化ケイ素単結晶製造装置 |
| JP2008074662A (ja) * | 2006-09-21 | 2008-04-03 | Nippon Steel Corp | 炭化珪素単結晶製造装置 |
| JP2011219287A (ja) * | 2010-04-06 | 2011-11-04 | Nippon Steel Corp | 炭化珪素単結晶インゴットの製造方法及び炭化珪素単結晶インゴット |
| JP2011219295A (ja) * | 2010-04-07 | 2011-11-04 | Nippon Steel Corp | 炭化珪素単結晶インゴットの製造装置 |
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2015212207A (ja) * | 2014-05-02 | 2015-11-26 | 新日鐵住金株式会社 | 炭化珪素単結晶インゴットの製造方法 |
| JP2016088789A (ja) * | 2014-10-31 | 2016-05-23 | 住友電気工業株式会社 | 炭化珪素単結晶の製造装置および炭化珪素単結晶の製造方法 |
| JP2016088801A (ja) * | 2014-11-04 | 2016-05-23 | 住友電気工業株式会社 | 炭化珪素単結晶の製造装置および炭化珪素単結晶の製造方法 |
| JP2016088812A (ja) * | 2014-11-06 | 2016-05-23 | 新日鐵住金株式会社 | 炭化珪素単結晶インゴットの製造方法及び製造装置 |
| JP2019073441A (ja) * | 2019-02-20 | 2019-05-16 | 住友電気工業株式会社 | 炭化珪素単結晶の製造装置および炭化珪素単結晶の製造方法 |
| KR102187449B1 (ko) * | 2019-05-28 | 2020-12-11 | 에스케이씨 주식회사 | 탄화규소 잉곳의 제조방법, 탄화규소 잉곳 및 이의 성장 시스템 |
| US11359306B2 (en) | 2019-10-29 | 2022-06-14 | Senic Inc. | Method for preparing a SiC ingot and device for preparing a SiC ingot wherein electrical resistance of crucible body is 2.9 ohms or more |
| JP2021104912A (ja) * | 2019-12-26 | 2021-07-26 | 昭和電工株式会社 | 単結晶製造装置 |
| JP7351219B2 (ja) | 2019-12-26 | 2023-09-27 | 株式会社レゾナック | 単結晶製造装置 |
Also Published As
| Publication number | Publication date |
|---|---|
| US20130255568A1 (en) | 2013-10-03 |
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