JP2012533413A5 - - Google Patents
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- Publication number
- JP2012533413A5 JP2012533413A5 JP2012520819A JP2012520819A JP2012533413A5 JP 2012533413 A5 JP2012533413 A5 JP 2012533413A5 JP 2012520819 A JP2012520819 A JP 2012520819A JP 2012520819 A JP2012520819 A JP 2012520819A JP 2012533413 A5 JP2012533413 A5 JP 2012533413A5
- Authority
- JP
- Japan
- Prior art keywords
- catalyst
- catalyst precursor
- precursor composition
- composition
- magnesium
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000000203 mixture Substances 0.000 claims description 72
- 239000012018 catalyst precursor Substances 0.000 claims description 41
- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Substances [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 36
- 229910052742 iron Inorganic materials 0.000 claims description 14
- 229910052751 metal Inorganic materials 0.000 claims description 14
- 239000002184 metal Substances 0.000 claims description 14
- 229910052750 molybdenum Inorganic materials 0.000 claims description 9
- 150000002736 metal compounds Chemical class 0.000 claims description 5
- VTHJTEIRLNZDEV-UHFFFAOYSA-L magnesium dihydroxide Chemical compound [OH-].[OH-].[Mg+2] VTHJTEIRLNZDEV-UHFFFAOYSA-L 0.000 claims description 3
- 239000000347 magnesium hydroxide Substances 0.000 claims description 3
- 229910001862 magnesium hydroxide Inorganic materials 0.000 claims description 3
- 239000003054 catalyst Substances 0.000 claims 26
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims 18
- 239000002245 particle Substances 0.000 claims 16
- 239000010941 cobalt Substances 0.000 claims 12
- 229910017052 cobalt Inorganic materials 0.000 claims 12
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 claims 12
- 229910003455 mixed metal oxide Inorganic materials 0.000 claims 11
- 229910052749 magnesium Inorganic materials 0.000 claims 9
- 239000011777 magnesium Substances 0.000 claims 9
- CPLXHLVBOLITMK-UHFFFAOYSA-N magnesium oxide Inorganic materials [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 claims 9
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 claims 8
- 239000000395 magnesium oxide Substances 0.000 claims 8
- 239000011733 molybdenum Substances 0.000 claims 8
- AXZKOIWUVFPNLO-UHFFFAOYSA-N magnesium;oxygen(2-) Chemical compound [O-2].[Mg+2] AXZKOIWUVFPNLO-UHFFFAOYSA-N 0.000 claims 7
- FYYHWMGAXLPEAU-UHFFFAOYSA-N Magnesium Chemical compound [Mg] FYYHWMGAXLPEAU-UHFFFAOYSA-N 0.000 claims 5
- -1 magnesium aluminate Chemical class 0.000 claims 4
- QIJNJJZPYXGIQM-UHFFFAOYSA-N 1lambda4,2lambda4-dimolybdacyclopropa-1,2,3-triene Chemical compound [Mo]=C=[Mo] QIJNJJZPYXGIQM-UHFFFAOYSA-N 0.000 claims 3
- 229910039444 MoC Inorganic materials 0.000 claims 3
- WNROFYMDJYEPJX-UHFFFAOYSA-K aluminium hydroxide Chemical compound [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 claims 3
- 229910001567 cementite Inorganic materials 0.000 claims 3
- 150000002681 magnesium compounds Chemical class 0.000 claims 3
- 238000001354 calcination Methods 0.000 claims 2
- 150000001875 compounds Chemical class 0.000 claims 2
- 238000001035 drying Methods 0.000 claims 2
- 229910020068 MgAl Inorganic materials 0.000 claims 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 5
- 239000002041 carbon nanotube Substances 0.000 description 5
- 229910021393 carbon nanotube Inorganic materials 0.000 description 5
- 239000002048 multi walled nanotube Substances 0.000 description 5
- 238000005325 percolation Methods 0.000 description 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 description 2
- 229940011182 cobalt acetate Drugs 0.000 description 2
- QAHREYKOYSIQPH-UHFFFAOYSA-L cobalt(II) acetate Chemical compound [Co+2].CC([O-])=O.CC([O-])=O QAHREYKOYSIQPH-UHFFFAOYSA-L 0.000 description 2
- 239000002131 composite material Substances 0.000 description 2
- MVFCKEFYUDZOCX-UHFFFAOYSA-N iron(2+);dinitrate Chemical compound [Fe+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O MVFCKEFYUDZOCX-UHFFFAOYSA-N 0.000 description 2
- YIXJRHPUWRPCBB-UHFFFAOYSA-N magnesium nitrate Chemical compound [Mg+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O YIXJRHPUWRPCBB-UHFFFAOYSA-N 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 239000002071 nanotube Substances 0.000 description 2
- MXRIRQGCELJRSN-UHFFFAOYSA-N O.O.O.[Al] Chemical compound O.O.O.[Al] MXRIRQGCELJRSN-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- XUFUCDNVOXXQQC-UHFFFAOYSA-L azane;hydroxy-(hydroxy(dioxo)molybdenio)oxy-dioxomolybdenum Chemical compound N.N.O[Mo](=O)(=O)O[Mo](O)(=O)=O XUFUCDNVOXXQQC-UHFFFAOYSA-L 0.000 description 1
- 230000003197 catalytic effect Effects 0.000 description 1
- 150000001869 cobalt compounds Chemical class 0.000 description 1
- UFMZWBIQTDUYBN-UHFFFAOYSA-N cobalt dinitrate Chemical compound [Co+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O UFMZWBIQTDUYBN-UHFFFAOYSA-N 0.000 description 1
- 229910001981 cobalt nitrate Inorganic materials 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 150000002506 iron compounds Chemical class 0.000 description 1
- PVFSDGKDKFSOTB-UHFFFAOYSA-K iron(3+);triacetate Chemical compound [Fe+3].CC([O-])=O.CC([O-])=O.CC([O-])=O PVFSDGKDKFSOTB-UHFFFAOYSA-K 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 239000005078 molybdenum compound Substances 0.000 description 1
- 150000002752 molybdenum compounds Chemical class 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US22643809P | 2009-07-17 | 2009-07-17 | |
| US61/226,438 | 2009-07-17 | ||
| PCT/US2010/042321 WO2011009071A1 (en) | 2009-07-17 | 2010-07-16 | Catalyst and methods for producing multi-wall carbon nanotubes |
Related Child Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2014255341A Division JP5932010B2 (ja) | 2009-07-17 | 2014-12-17 | 多層カーボンナノチューブ製造のための触媒および方法 |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2012533413A JP2012533413A (ja) | 2012-12-27 |
| JP2012533413A5 true JP2012533413A5 (https=) | 2013-08-29 |
| JP5670451B2 JP5670451B2 (ja) | 2015-02-18 |
Family
ID=43449832
Family Applications (3)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2012520819A Active JP5670451B2 (ja) | 2009-07-17 | 2010-07-16 | 多層カーボンナノチューブ製造のための触媒および方法 |
| JP2014255341A Active JP5932010B2 (ja) | 2009-07-17 | 2014-12-17 | 多層カーボンナノチューブ製造のための触媒および方法 |
| JP2016088743A Active JP6310956B2 (ja) | 2009-07-17 | 2016-04-27 | 多層カーボンナノチューブ製造のための触媒および方法 |
Family Applications After (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2014255341A Active JP5932010B2 (ja) | 2009-07-17 | 2014-12-17 | 多層カーボンナノチューブ製造のための触媒および方法 |
| JP2016088743A Active JP6310956B2 (ja) | 2009-07-17 | 2016-04-27 | 多層カーボンナノチューブ製造のための触媒および方法 |
Country Status (6)
| Country | Link |
|---|---|
| US (2) | US9084990B2 (https=) |
| EP (1) | EP2454015B1 (https=) |
| JP (3) | JP5670451B2 (https=) |
| CN (1) | CN106829925A (https=) |
| CA (1) | CA2768474A1 (https=) |
| WO (1) | WO2011009071A1 (https=) |
Families Citing this family (35)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2851505B2 (ja) | 1993-02-26 | 1999-01-27 | 信越化学工業株式会社 | シリコーン系防水処理剤およびこれによる防水処理方法 |
| PE20121017A1 (es) | 2009-04-17 | 2012-08-08 | Seerstone Llc | Metodo para la produccion de carbono solido mediante la reduccion de oxidos de carbono |
| CN106829925A (zh) * | 2009-07-17 | 2017-06-13 | 西南纳米科技公司 | 用于制备多壁碳纳米管的催化剂和方法 |
| KR101424910B1 (ko) * | 2012-01-11 | 2014-07-31 | 주식회사 엘지화학 | 카본나노튜브 및 그 제조방법 |
| NO2749379T3 (https=) | 2012-04-16 | 2018-07-28 | ||
| EP2838844A4 (en) | 2012-04-16 | 2015-10-28 | Seerstone Llc | METHOD FOR TREATING A GAS CLEARANCE CONTAINING CARBON OXIDES |
| EP2838837A4 (en) | 2012-04-16 | 2015-12-23 | Seerstone Llc | METHOD AND STRUCTURES FOR REDUCING CARBON OXIDES WITH IRON-FREE CATALYSTS |
| WO2013158160A1 (en) | 2012-04-16 | 2013-10-24 | Seerstone Llc | Method for producing solid carbon by reducing carbon dioxide |
| CN104302576B (zh) | 2012-04-16 | 2017-03-08 | 赛尔斯通股份有限公司 | 用于捕捉和封存碳并且用于减少废气流中碳氧化物的质量的方法和系统 |
| US9896341B2 (en) | 2012-04-23 | 2018-02-20 | Seerstone Llc | Methods of forming carbon nanotubes having a bimodal size distribution |
| US10815124B2 (en) | 2012-07-12 | 2020-10-27 | Seerstone Llc | Solid carbon products comprising carbon nanotubes and methods of forming same |
| US9604848B2 (en) | 2012-07-12 | 2017-03-28 | Seerstone Llc | Solid carbon products comprising carbon nanotubes and methods of forming same |
| CN107215882A (zh) | 2012-07-13 | 2017-09-29 | 赛尔斯通股份有限公司 | 用于形成氨和固体碳产物的方法和系统 |
| US9779845B2 (en) | 2012-07-18 | 2017-10-03 | Seerstone Llc | Primary voltaic sources including nanofiber Schottky barrier arrays and methods of forming same |
| WO2014085378A1 (en) | 2012-11-29 | 2014-06-05 | Seerstone Llc | Reactors and methods for producing solid carbon materials |
| WO2014150944A1 (en) | 2013-03-15 | 2014-09-25 | Seerstone Llc | Methods of producing hydrogen and solid carbon |
| WO2014151119A2 (en) | 2013-03-15 | 2014-09-25 | Seerstone Llc | Electrodes comprising nanostructured carbon |
| WO2014151144A1 (en) | 2013-03-15 | 2014-09-25 | Seerstone Llc | Carbon oxide reduction with intermetallic and carbide catalysts |
| US9586823B2 (en) | 2013-03-15 | 2017-03-07 | Seerstone Llc | Systems for producing solid carbon by reducing carbon oxides |
| WO2014151138A1 (en) | 2013-03-15 | 2014-09-25 | Seerstone Llc | Reactors, systems, and methods for forming solid products |
| EP2883609B1 (en) * | 2013-07-10 | 2023-01-11 | LG Chem, Ltd. | Supported catalyst, carbon nanotube assembly, and preparation method therefor |
| KR101535388B1 (ko) | 2013-07-19 | 2015-07-08 | 주식회사 엘지화학 | 담지촉매, 이의 제조방법 및 이를 이용하여 제조된 탄소나노구조체의 2차구조물 |
| CA2930040C (en) * | 2013-12-18 | 2019-04-30 | Halliburton Energy Services, Inc. | Earth-boring drill bits with nanotube carpets |
| KR20170012745A (ko) * | 2015-07-23 | 2017-02-03 | 에스케이이노베이션 주식회사 | 다중벽 탄소나노튜브 제조용 촉매 및 이를 이용한 다중벽 탄소나노튜브의 제조 방법 |
| WO2018022999A1 (en) | 2016-07-28 | 2018-02-01 | Seerstone Llc. | Solid carbon products comprising compressed carbon nanotubes in a container and methods of forming same |
| WO2018168833A1 (ja) * | 2017-03-15 | 2018-09-20 | 東洋インキＳｃホールディングス株式会社 | 多層カーボンナノチューブ、多層カーボンナノチューブの製造方法、分散液、樹脂組成物、および塗膜 |
| JP6380588B1 (ja) * | 2017-03-15 | 2018-08-29 | 東洋インキＳｃホールディングス株式会社 | 多層カーボンナノチューブおよび多層カーボンナノチューブの製造方法 |
| JP7052336B2 (ja) * | 2017-12-20 | 2022-04-12 | 東洋インキＳｃホールディングス株式会社 | 多層カーボンナノチューブおよび多層カーボンナノチューブの製造方法 |
| US10759663B2 (en) | 2017-05-23 | 2020-09-01 | Indian Oil Corporation Limited | Multi-metal catalyst composition for production of morphology controlled CNT's and process thereof |
| JP6590034B1 (ja) * | 2018-06-28 | 2019-10-16 | 東洋インキＳｃホールディングス株式会社 | カーボンナノチューブ分散液およびその利用 |
| CN111135788A (zh) * | 2019-09-18 | 2020-05-12 | 青岛农业大学 | 一种磁性掺氮碳纳米管水处理吸附剂及其制备方法 |
| KR20240126027A (ko) * | 2021-10-01 | 2024-08-20 | 캐즘 어드밴스드 머티리얼스, 인크. | 촉매 화학 증착을 통한 탄소 나노튜브 및 하이브리드 물질 합성 시스템 및 방법 |
| JP7844056B2 (ja) * | 2021-10-13 | 2026-04-13 | キャズム アドバンスト マテリアルズ，インク． | コンクリート用途のためのカーボンナノチューブハイブリッド材料 |
| KR20240056211A (ko) * | 2022-10-21 | 2024-04-30 | 금호석유화학 주식회사 | 저직경 탄소나노튜브의 제조방법 및 그에 따라 제조된 탄소나노튜브 |
| WO2025072478A1 (en) * | 2023-09-29 | 2025-04-03 | Chasm Advanced Materials, Inc. | Carbon nanotube catalyst preconditioning |
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| US3867282A (en) | 1974-03-27 | 1975-02-18 | Mobil Oil Corp | Process for oil demetalation and desulfurization with cobalt-molybdenum impregnated magnesium aluminate spinel |
| KR970702758A (ko) * | 1994-04-29 | 1997-06-10 | 마이클 제이. 켈리 | 개선된 다이 립을 갖는 조합 롤 및 다이 피복 방법 및 장치(combination roll and die coating method and apparatus with improved die lip) |
| CN1077807C (zh) * | 1995-10-31 | 2002-01-16 | 中国科学院大连化学物理研究所 | 一种糠醛加氢制糠醇的方法及催化剂 |
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| EP1797950A1 (en) * | 2005-12-14 | 2007-06-20 | Nanocyl S.A. | Catalyst for a multi-walled carbon nanotube production process |
| DE102005051953B3 (de) * | 2005-10-29 | 2007-06-06 | Tu Bergakademie Freiberg | Verfahren zur Herstellung von feuerfesten Formkörpern oder Massen |
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| EP1995213A4 (en) * | 2006-03-13 | 2010-03-24 | Nikon Corp | METHOD OF PRODUCTION OF CARBON NANOPHONE AGGREGATES, CARBON NANOPHONIC UNITS, CATALYST LINE DISPERSION MEMBRANE, ELECTRONIC MIXTURES AND FIELD EMISSION INDICATORS |
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| JP2009062230A (ja) * | 2007-09-06 | 2009-03-26 | Bridgestone Corp | 気相成長炭素繊維の製造方法および気相成長炭素繊維 |
| DE102007046160A1 (de) * | 2007-09-27 | 2009-04-02 | Bayer Materialscience Ag | Verfahren zur Herstellung eines Katalysators für die Herstellung von Kohlenstoffnanoröhrchen |
| KR101007183B1 (ko) * | 2008-10-23 | 2011-01-12 | 제일모직주식회사 | 탄소나노튜브 합성용 담지촉매, 그 제조방법 및 이를 이용한 탄소나노튜브 |
| US20100266478A1 (en) * | 2008-12-10 | 2010-10-21 | Cheil Industries Inc. | Metal Nano Catalyst, Method for Preparing the Same and Method for Controlling the Growth Types of Carbon Nanotubes Using the Same |
| KR100976174B1 (ko) * | 2009-02-13 | 2010-08-16 | 금호석유화학 주식회사 | 얇은 다중벽 탄소나노튜브 제조용 촉매조성물 및 이의 제조방법 |
| CN106829925A (zh) * | 2009-07-17 | 2017-06-13 | 西南纳米科技公司 | 用于制备多壁碳纳米管的催化剂和方法 |
-
2010
- 2010-07-16 CN CN201610528088.3A patent/CN106829925A/zh active Pending
- 2010-07-16 EP EP10800624.8A patent/EP2454015B1/en active Active
- 2010-07-16 JP JP2012520819A patent/JP5670451B2/ja active Active
- 2010-07-16 WO PCT/US2010/042321 patent/WO2011009071A1/en not_active Ceased
- 2010-07-16 CA CA2768474A patent/CA2768474A1/en not_active Abandoned
- 2010-07-16 US US13/383,963 patent/US9084990B2/en active Active
-
2014
- 2014-12-17 JP JP2014255341A patent/JP5932010B2/ja active Active
-
2015
- 2015-06-16 US US14/740,870 patent/US9855551B2/en active Active
-
2016
- 2016-04-27 JP JP2016088743A patent/JP6310956B2/ja active Active
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