JP2012512217A5 - - Google Patents
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- Publication number
- JP2012512217A5 JP2012512217A5 JP2011541268A JP2011541268A JP2012512217A5 JP 2012512217 A5 JP2012512217 A5 JP 2012512217A5 JP 2011541268 A JP2011541268 A JP 2011541268A JP 2011541268 A JP2011541268 A JP 2011541268A JP 2012512217 A5 JP2012512217 A5 JP 2012512217A5
- Authority
- JP
- Japan
- Prior art keywords
- isopropylmethacrylamide
- mol
- methacrylic acid
- acid chloride
- stirred
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 6
- YQIGLEFUZMIVHU-UHFFFAOYSA-N 2-methyl-n-propan-2-ylprop-2-enamide Chemical compound CC(C)NC(=O)C(C)=C YQIGLEFUZMIVHU-UHFFFAOYSA-N 0.000 description 3
- VHRYZQNGTZXDNX-UHFFFAOYSA-N methacryloyl chloride Chemical compound CC(=C)C(Cl)=O VHRYZQNGTZXDNX-UHFFFAOYSA-N 0.000 description 3
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 1
- 125000000484 butyl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 238000004817 gas chromatography Methods 0.000 description 1
- 239000003112 inhibitor Substances 0.000 description 1
- JJWLVOIRVHMVIS-UHFFFAOYSA-N isopropylamine Chemical compound CC(C)N JJWLVOIRVHMVIS-UHFFFAOYSA-N 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE102008054612A DE102008054612A1 (de) | 2008-12-15 | 2008-12-15 | Verfahren zur Herstellung von N-Isopropyl(meth)acrylamid |
| DE102008054612.7 | 2008-12-15 | ||
| PCT/EP2009/065435 WO2010072480A1 (de) | 2008-12-15 | 2009-11-19 | Verfahren zur herstellung von n-isopropyl(meth)acrylamid |
Related Child Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2015038420A Division JP2015134794A (ja) | 2008-12-15 | 2015-02-27 | Ｎ−イソプロピル（メタ）アクリルアミドの製造方法 |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2012512217A JP2012512217A (ja) | 2012-05-31 |
| JP2012512217A5 true JP2012512217A5 (https=) | 2015-04-23 |
| JP5791511B2 JP5791511B2 (ja) | 2015-10-07 |
Family
ID=42125499
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2011541268A Active JP5791511B2 (ja) | 2008-12-15 | 2009-11-19 | Ｎ−イソプロピル（メタ）アクリルアミドの製造方法 |
| JP2015038420A Withdrawn JP2015134794A (ja) | 2008-12-15 | 2015-02-27 | Ｎ−イソプロピル（メタ）アクリルアミドの製造方法 |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2015038420A Withdrawn JP2015134794A (ja) | 2008-12-15 | 2015-02-27 | Ｎ−イソプロピル（メタ）アクリルアミドの製造方法 |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US9512062B2 (https=) |
| EP (2) | EP3680231A1 (https=) |
| JP (2) | JP5791511B2 (https=) |
| KR (2) | KR101853597B1 (https=) |
| CN (2) | CN106631862A (https=) |
| DE (1) | DE102008054612A1 (https=) |
| ES (1) | ES2790593T3 (https=) |
| RU (2) | RU2011129251A (https=) |
| TW (1) | TWI498314B (https=) |
| WO (1) | WO2010072480A1 (https=) |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE102011089363A1 (de) * | 2011-12-21 | 2013-06-27 | Evonik Röhm Gmbh | Verfahren zur Herstellung von N-Alkyl(meth)acrylamiden |
| US11136287B2 (en) | 2017-03-01 | 2021-10-05 | Api Corporation | Method for producing n-benzyl-2-bromo-3-methoxypropionamide and intermediates thereof |
| CN107200695A (zh) * | 2017-06-13 | 2017-09-26 | 山东瑞博龙化工科技股份有限公司 | 一种制备n‑羟乙基甲基丙烯酰胺的方法 |
| CN107245039A (zh) * | 2017-06-13 | 2017-10-13 | 山东瑞博龙化工科技股份有限公司 | 一种制备n‑羟乙基丙烯酰胺的方法 |
| US11505520B2 (en) | 2018-05-23 | 2022-11-22 | Evonik Operations Gmbh | Method for preparing keto-functionalized aromatic (meth)acrylates |
| EP3652151B1 (en) | 2018-07-17 | 2020-08-12 | Evonik Operations GmbH | Method for preparing c-h acidic (meth)acrylates |
| EP3599232A1 (de) * | 2018-07-26 | 2020-01-29 | Evonik Operations GmbH | Verfahren zur herstellung von n-methyl(meth)acrylamid |
Family Cites Families (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1250421A (https=) * | 1968-02-05 | 1971-10-20 | ||
| CH580572A5 (https=) | 1973-10-03 | 1976-10-15 | Lonza Ag | |
| US4288592A (en) * | 1979-04-30 | 1981-09-08 | American Cyanamid Company | Process for preparing amides by reaction in presence of molecular sieve |
| DE3130508A1 (de) * | 1981-08-01 | 1983-02-17 | Röhm GmbH, 6100 Darmstadt | "verfahren zur herstellung von methacryl- und acrylamiden" |
| DE3131096A1 (de) | 1981-08-06 | 1983-02-24 | Röhm GmbH, 6100 Darmstadt | Verfahren zur herstellung von n-substituierten methacryl- und acrylamiden |
| DE3412650A1 (de) * | 1984-04-04 | 1985-10-17 | Röhm GmbH, 6100 Darmstadt | Verfahren zur herstellung von hydroxyalkyl-acrylamiden und -methacrylamiden |
| FR2590567B1 (fr) * | 1985-11-27 | 1988-07-15 | Charbonnages Ste Chimique | Nouveau procede de synthese de (meth)acrylamide de n-dialkylaminoalkyle |
| JPH03264549A (ja) | 1990-03-15 | 1991-11-25 | Sanyo Chem Ind Ltd | 不飽和単量体の製造方法 |
| RU2137740C1 (ru) | 1995-06-08 | 1999-09-20 | Эксон продакшн рисерч компани | Способ ингибирования образования клатрат-гидратов в жидкости |
| DE10010811A1 (de) * | 2000-03-08 | 2001-09-13 | Basf Ag | Verfahren zur Herstellung von Polymeren |
| US6753431B2 (en) * | 2000-06-02 | 2004-06-22 | Sumitomo Chemical Company Limited | Production of mixed acid anhydride and amide compound |
| US20040024152A1 (en) * | 2000-07-28 | 2004-02-05 | Masayuki Toyama | Gas hydrate formation inhibitor and method for inhibiting gas hydrate formation with the same |
| WO2005121133A1 (en) * | 2004-06-11 | 2005-12-22 | Takeda Pharmaceutical Company Limited | Highly selective novel amidation method |
| DE102006047617B4 (de) | 2006-10-09 | 2008-11-27 | Clariant International Limited | Verfahren zur Herstellung basischer (Meth)acrylamide |
| US8445723B2 (en) | 2008-08-19 | 2013-05-21 | Nalco Company | Processes for producing N-alkyl (alkyl)acrylamides |
-
2008
- 2008-12-15 DE DE102008054612A patent/DE102008054612A1/de not_active Withdrawn
-
2009
- 2009-11-19 RU RU2011129251/04A patent/RU2011129251A/ru unknown
- 2009-11-19 RU RU2015101155/04A patent/RU2015101155A/ru not_active Application Discontinuation
- 2009-11-19 EP EP20156880.5A patent/EP3680231A1/de not_active Withdrawn
- 2009-11-19 WO PCT/EP2009/065435 patent/WO2010072480A1/de not_active Ceased
- 2009-11-19 JP JP2011541268A patent/JP5791511B2/ja active Active
- 2009-11-19 CN CN201710008630.7A patent/CN106631862A/zh active Pending
- 2009-11-19 KR KR1020177007294A patent/KR101853597B1/ko active Active
- 2009-11-19 KR KR1020117010969A patent/KR20110099683A/ko not_active Ceased
- 2009-11-19 CN CN2009801421344A patent/CN102197018A/zh active Pending
- 2009-11-19 US US13/119,244 patent/US9512062B2/en active Active
- 2009-11-19 ES ES09756729T patent/ES2790593T3/es active Active
- 2009-11-19 EP EP09756729.1A patent/EP2358664B1/de active Active
- 2009-12-10 TW TW098142285A patent/TWI498314B/zh active
-
2015
- 2015-02-27 JP JP2015038420A patent/JP2015134794A/ja not_active Withdrawn
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