RU2011129251A - Способ получения n-изопропил (мет) акриламида - Google Patents
Способ получения n-изопропил (мет) акриламида Download PDFInfo
- Publication number
- RU2011129251A RU2011129251A RU2011129251/04A RU2011129251A RU2011129251A RU 2011129251 A RU2011129251 A RU 2011129251A RU 2011129251/04 A RU2011129251/04 A RU 2011129251/04A RU 2011129251 A RU2011129251 A RU 2011129251A RU 2011129251 A RU2011129251 A RU 2011129251A
- Authority
- RU
- Russia
- Prior art keywords
- unsaturated carboxylic
- isolated
- amide
- producing
- carboxylic acid
- Prior art date
Links
- 238000004519 manufacturing process Methods 0.000 title claims abstract 7
- HRPVXLWXLXDGHG-UHFFFAOYSA-N Acrylamide Chemical compound NC(=O)C=C HRPVXLWXLXDGHG-UHFFFAOYSA-N 0.000 title 1
- 150000001408 amides Chemical class 0.000 claims abstract 34
- 150000001735 carboxylic acids Chemical class 0.000 claims abstract 13
- 238000000034 method Methods 0.000 claims abstract 12
- 150000001244 carboxylic acid anhydrides Chemical class 0.000 claims abstract 10
- 230000003993 interaction Effects 0.000 claims abstract 8
- 239000002904 solvent Substances 0.000 claims abstract 7
- 239000012442 inert solvent Substances 0.000 claims abstract 6
- 150000001412 amines Chemical class 0.000 claims abstract 4
- 150000001732 carboxylic acid derivatives Chemical class 0.000 claims abstract 4
- 239000012452 mother liquor Substances 0.000 claims abstract 4
- 150000003141 primary amines Chemical class 0.000 claims abstract 4
- 150000003335 secondary amines Chemical class 0.000 claims abstract 3
- CERQOIWHTDAKMF-UHFFFAOYSA-N Methacrylic acid Chemical compound CC(=C)C(O)=O CERQOIWHTDAKMF-UHFFFAOYSA-N 0.000 claims abstract 2
- 238000004821 distillation Methods 0.000 claims abstract 2
- 238000002955 isolation Methods 0.000 claims abstract 2
- 238000000926 separation method Methods 0.000 claims abstract 2
- YQIGLEFUZMIVHU-UHFFFAOYSA-N 2-methyl-n-propan-2-ylprop-2-enamide Chemical compound CC(C)NC(=O)C(C)=C YQIGLEFUZMIVHU-UHFFFAOYSA-N 0.000 claims 4
- 229920001577 copolymer Polymers 0.000 claims 3
- 239000000178 monomer Substances 0.000 claims 3
- 229920000642 polymer Polymers 0.000 claims 3
- JJWLVOIRVHMVIS-UHFFFAOYSA-N isopropylamine Chemical compound CC(C)N JJWLVOIRVHMVIS-UHFFFAOYSA-N 0.000 claims 2
- DCUFMVPCXCSVNP-UHFFFAOYSA-N methacrylic anhydride Chemical compound CC(=C)C(=O)OC(=O)C(C)=C DCUFMVPCXCSVNP-UHFFFAOYSA-N 0.000 claims 2
- 150000008064 anhydrides Chemical class 0.000 claims 1
- 230000015572 biosynthetic process Effects 0.000 claims 1
- 150000004677 hydrates Chemical class 0.000 claims 1
- 239000003112 inhibitor Substances 0.000 claims 1
- 238000006116 polymerization reaction Methods 0.000 claims 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C231/00—Preparation of carboxylic acid amides
- C07C231/02—Preparation of carboxylic acid amides from carboxylic acids or from esters, anhydrides, or halides thereof by reaction with ammonia or amines
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C249/00—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton
- C07C249/04—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes
- C07C249/08—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes by reaction of hydroxylamines with carbonyl compounds
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C251/00—Compounds containing nitrogen atoms doubly-bound to a carbon skeleton
- C07C251/32—Oximes
- C07C251/34—Oximes with oxygen atoms of oxyimino groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals
- C07C251/48—Oximes with oxygen atoms of oxyimino groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals with the carbon atom of at least one of the oxyimino groups bound to a carbon atom of a six-membered aromatic ring
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C273/00—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups
- C07C273/18—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of substituted ureas
- C07C273/1854—Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of substituted ureas by reactions not involving the formation of the N-C(O)-N- moiety
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F220/00—Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical or a salt, anhydride ester, amide, imide or nitrile thereof
- C08F220/02—Monocarboxylic acids having less than ten carbon atoms; Derivatives thereof
- C08F220/52—Amides or imides
- C08F220/54—Amides, e.g. N,N-dimethylacrylamide or N-isopropylacrylamide
- C08F220/56—Acrylamide; Methacrylamide
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C233/00—Carboxylic acid amides
- C07C233/01—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms
- C07C233/02—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms having nitrogen atoms of carboxamide groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals
- C07C233/09—Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms having nitrogen atoms of carboxamide groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals with carbon atoms of carboxamide groups bound to carbon atoms of an acyclic unsaturated carbon skeleton
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE102008054612A DE102008054612A1 (de) | 2008-12-15 | 2008-12-15 | Verfahren zur Herstellung von N-Isopropyl(meth)acrylamid |
| DE102008054612.7 | 2008-12-15 | ||
| PCT/EP2009/065435 WO2010072480A1 (de) | 2008-12-15 | 2009-11-19 | Verfahren zur herstellung von n-isopropyl(meth)acrylamid |
Related Child Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| RU2015101155/04A Division RU2015101155A (ru) | 2008-12-15 | 2009-11-19 | Способ получения n-изопропил(мет)акриламида |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| RU2011129251A true RU2011129251A (ru) | 2013-01-20 |
Family
ID=42125499
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| RU2011129251/04A RU2011129251A (ru) | 2008-12-15 | 2009-11-19 | Способ получения n-изопропил (мет) акриламида |
| RU2015101155/04A RU2015101155A (ru) | 2008-12-15 | 2009-11-19 | Способ получения n-изопропил(мет)акриламида |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| RU2015101155/04A RU2015101155A (ru) | 2008-12-15 | 2009-11-19 | Способ получения n-изопропил(мет)акриламида |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US9512062B2 (https=) |
| EP (2) | EP3680231A1 (https=) |
| JP (2) | JP5791511B2 (https=) |
| KR (2) | KR101853597B1 (https=) |
| CN (2) | CN106631862A (https=) |
| DE (1) | DE102008054612A1 (https=) |
| ES (1) | ES2790593T3 (https=) |
| RU (2) | RU2011129251A (https=) |
| TW (1) | TWI498314B (https=) |
| WO (1) | WO2010072480A1 (https=) |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE102011089363A1 (de) * | 2011-12-21 | 2013-06-27 | Evonik Röhm Gmbh | Verfahren zur Herstellung von N-Alkyl(meth)acrylamiden |
| US11136287B2 (en) | 2017-03-01 | 2021-10-05 | Api Corporation | Method for producing n-benzyl-2-bromo-3-methoxypropionamide and intermediates thereof |
| CN107200695A (zh) * | 2017-06-13 | 2017-09-26 | 山东瑞博龙化工科技股份有限公司 | 一种制备n‑羟乙基甲基丙烯酰胺的方法 |
| CN107245039A (zh) * | 2017-06-13 | 2017-10-13 | 山东瑞博龙化工科技股份有限公司 | 一种制备n‑羟乙基丙烯酰胺的方法 |
| US11505520B2 (en) | 2018-05-23 | 2022-11-22 | Evonik Operations Gmbh | Method for preparing keto-functionalized aromatic (meth)acrylates |
| EP3652151B1 (en) | 2018-07-17 | 2020-08-12 | Evonik Operations GmbH | Method for preparing c-h acidic (meth)acrylates |
| EP3599232A1 (de) * | 2018-07-26 | 2020-01-29 | Evonik Operations GmbH | Verfahren zur herstellung von n-methyl(meth)acrylamid |
Family Cites Families (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1250421A (https=) * | 1968-02-05 | 1971-10-20 | ||
| CH580572A5 (https=) | 1973-10-03 | 1976-10-15 | Lonza Ag | |
| US4288592A (en) * | 1979-04-30 | 1981-09-08 | American Cyanamid Company | Process for preparing amides by reaction in presence of molecular sieve |
| DE3130508A1 (de) * | 1981-08-01 | 1983-02-17 | Röhm GmbH, 6100 Darmstadt | "verfahren zur herstellung von methacryl- und acrylamiden" |
| DE3131096A1 (de) | 1981-08-06 | 1983-02-24 | Röhm GmbH, 6100 Darmstadt | Verfahren zur herstellung von n-substituierten methacryl- und acrylamiden |
| DE3412650A1 (de) * | 1984-04-04 | 1985-10-17 | Röhm GmbH, 6100 Darmstadt | Verfahren zur herstellung von hydroxyalkyl-acrylamiden und -methacrylamiden |
| FR2590567B1 (fr) * | 1985-11-27 | 1988-07-15 | Charbonnages Ste Chimique | Nouveau procede de synthese de (meth)acrylamide de n-dialkylaminoalkyle |
| JPH03264549A (ja) | 1990-03-15 | 1991-11-25 | Sanyo Chem Ind Ltd | 不飽和単量体の製造方法 |
| RU2137740C1 (ru) | 1995-06-08 | 1999-09-20 | Эксон продакшн рисерч компани | Способ ингибирования образования клатрат-гидратов в жидкости |
| DE10010811A1 (de) * | 2000-03-08 | 2001-09-13 | Basf Ag | Verfahren zur Herstellung von Polymeren |
| US6753431B2 (en) * | 2000-06-02 | 2004-06-22 | Sumitomo Chemical Company Limited | Production of mixed acid anhydride and amide compound |
| US20040024152A1 (en) * | 2000-07-28 | 2004-02-05 | Masayuki Toyama | Gas hydrate formation inhibitor and method for inhibiting gas hydrate formation with the same |
| WO2005121133A1 (en) * | 2004-06-11 | 2005-12-22 | Takeda Pharmaceutical Company Limited | Highly selective novel amidation method |
| DE102006047617B4 (de) | 2006-10-09 | 2008-11-27 | Clariant International Limited | Verfahren zur Herstellung basischer (Meth)acrylamide |
| US8445723B2 (en) | 2008-08-19 | 2013-05-21 | Nalco Company | Processes for producing N-alkyl (alkyl)acrylamides |
-
2008
- 2008-12-15 DE DE102008054612A patent/DE102008054612A1/de not_active Withdrawn
-
2009
- 2009-11-19 RU RU2011129251/04A patent/RU2011129251A/ru unknown
- 2009-11-19 RU RU2015101155/04A patent/RU2015101155A/ru not_active Application Discontinuation
- 2009-11-19 EP EP20156880.5A patent/EP3680231A1/de not_active Withdrawn
- 2009-11-19 WO PCT/EP2009/065435 patent/WO2010072480A1/de not_active Ceased
- 2009-11-19 JP JP2011541268A patent/JP5791511B2/ja active Active
- 2009-11-19 CN CN201710008630.7A patent/CN106631862A/zh active Pending
- 2009-11-19 KR KR1020177007294A patent/KR101853597B1/ko active Active
- 2009-11-19 KR KR1020117010969A patent/KR20110099683A/ko not_active Ceased
- 2009-11-19 CN CN2009801421344A patent/CN102197018A/zh active Pending
- 2009-11-19 US US13/119,244 patent/US9512062B2/en active Active
- 2009-11-19 ES ES09756729T patent/ES2790593T3/es active Active
- 2009-11-19 EP EP09756729.1A patent/EP2358664B1/de active Active
- 2009-12-10 TW TW098142285A patent/TWI498314B/zh active
-
2015
- 2015-02-27 JP JP2015038420A patent/JP2015134794A/ja not_active Withdrawn
Also Published As
| Publication number | Publication date |
|---|---|
| EP2358664B1 (de) | 2020-03-25 |
| US20110218312A1 (en) | 2011-09-08 |
| JP5791511B2 (ja) | 2015-10-07 |
| TWI498314B (zh) | 2015-09-01 |
| CN106631862A (zh) | 2017-05-10 |
| EP3680231A1 (de) | 2020-07-15 |
| WO2010072480A1 (de) | 2010-07-01 |
| JP2012512217A (ja) | 2012-05-31 |
| RU2015101155A3 (https=) | 2018-08-31 |
| JP2015134794A (ja) | 2015-07-27 |
| TW201035015A (en) | 2010-10-01 |
| US9512062B2 (en) | 2016-12-06 |
| DE102008054612A1 (de) | 2010-06-17 |
| ES2790593T3 (es) | 2020-10-28 |
| CN102197018A (zh) | 2011-09-21 |
| EP2358664A1 (de) | 2011-08-24 |
| RU2015101155A (ru) | 2015-06-27 |
| KR101853597B1 (ko) | 2018-04-30 |
| KR20110099683A (ko) | 2011-09-08 |
| KR20170033910A (ko) | 2017-03-27 |
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