JP5791511B2 - N−イソプロピル(メタ)アクリルアミドの製造方法 - Google Patents

N−イソプロピル(メタ)アクリルアミドの製造方法 Download PDF

Info

Publication number
JP5791511B2
JP5791511B2 JP2011541268A JP2011541268A JP5791511B2 JP 5791511 B2 JP5791511 B2 JP 5791511B2 JP 2011541268 A JP2011541268 A JP 2011541268A JP 2011541268 A JP2011541268 A JP 2011541268A JP 5791511 B2 JP5791511 B2 JP 5791511B2
Authority
JP
Japan
Prior art keywords
meth
producing
phenylenediamine
butyl
isopropylmethacrylamide
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
JP2011541268A
Other languages
English (en)
Japanese (ja)
Other versions
JP2012512217A (ja
JP2012512217A5 (https=
Inventor
クネーベル ヨアヒム
クネーベル ヨアヒム
カーンブロック ヴィルヘルム
カーンブロック ヴィルヘルム
ケルシャー フォルカー
ケルシャー フォルカー
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Roehm GmbH Darmstadt
Original Assignee
Evonik Roehm GmbH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Evonik Roehm GmbH filed Critical Evonik Roehm GmbH
Publication of JP2012512217A publication Critical patent/JP2012512217A/ja
Publication of JP2012512217A5 publication Critical patent/JP2012512217A5/ja
Application granted granted Critical
Publication of JP5791511B2 publication Critical patent/JP5791511B2/ja
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C231/00Preparation of carboxylic acid amides
    • C07C231/02Preparation of carboxylic acid amides from carboxylic acids or from esters, anhydrides, or halides thereof by reaction with ammonia or amines
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C249/00Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton
    • C07C249/04Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes
    • C07C249/08Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes by reaction of hydroxylamines with carbonyl compounds
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C251/00Compounds containing nitrogen atoms doubly-bound to a carbon skeleton
    • C07C251/32Oximes
    • C07C251/34Oximes with oxygen atoms of oxyimino groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals
    • C07C251/48Oximes with oxygen atoms of oxyimino groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals with the carbon atom of at least one of the oxyimino groups bound to a carbon atom of a six-membered aromatic ring
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C273/00Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups
    • C07C273/18Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of substituted ureas
    • C07C273/1854Preparation of urea or its derivatives, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups of substituted ureas by reactions not involving the formation of the N-C(O)-N- moiety
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F220/00Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical or a salt, anhydride ester, amide, imide or nitrile thereof
    • C08F220/02Monocarboxylic acids having less than ten carbon atoms; Derivatives thereof
    • C08F220/52Amides or imides
    • C08F220/54Amides, e.g. N,N-dimethylacrylamide or N-isopropylacrylamide
    • C08F220/56Acrylamide; Methacrylamide
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C233/00Carboxylic acid amides
    • C07C233/01Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms
    • C07C233/02Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms having nitrogen atoms of carboxamide groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals
    • C07C233/09Carboxylic acid amides having carbon atoms of carboxamide groups bound to hydrogen atoms or to acyclic carbon atoms having nitrogen atoms of carboxamide groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals with carbon atoms of carboxamide groups bound to carbon atoms of an acyclic unsaturated carbon skeleton

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
JP2011541268A 2008-12-15 2009-11-19 N−イソプロピル(メタ)アクリルアミドの製造方法 Active JP5791511B2 (ja)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE102008054612A DE102008054612A1 (de) 2008-12-15 2008-12-15 Verfahren zur Herstellung von N-Isopropyl(meth)acrylamid
DE102008054612.7 2008-12-15
PCT/EP2009/065435 WO2010072480A1 (de) 2008-12-15 2009-11-19 Verfahren zur herstellung von n-isopropyl(meth)acrylamid

Related Child Applications (1)

Application Number Title Priority Date Filing Date
JP2015038420A Division JP2015134794A (ja) 2008-12-15 2015-02-27 N−イソプロピル(メタ)アクリルアミドの製造方法

Publications (3)

Publication Number Publication Date
JP2012512217A JP2012512217A (ja) 2012-05-31
JP2012512217A5 JP2012512217A5 (https=) 2015-04-23
JP5791511B2 true JP5791511B2 (ja) 2015-10-07

Family

ID=42125499

Family Applications (2)

Application Number Title Priority Date Filing Date
JP2011541268A Active JP5791511B2 (ja) 2008-12-15 2009-11-19 N−イソプロピル(メタ)アクリルアミドの製造方法
JP2015038420A Withdrawn JP2015134794A (ja) 2008-12-15 2015-02-27 N−イソプロピル(メタ)アクリルアミドの製造方法

Family Applications After (1)

Application Number Title Priority Date Filing Date
JP2015038420A Withdrawn JP2015134794A (ja) 2008-12-15 2015-02-27 N−イソプロピル(メタ)アクリルアミドの製造方法

Country Status (10)

Country Link
US (1) US9512062B2 (https=)
EP (2) EP3680231A1 (https=)
JP (2) JP5791511B2 (https=)
KR (2) KR101853597B1 (https=)
CN (2) CN106631862A (https=)
DE (1) DE102008054612A1 (https=)
ES (1) ES2790593T3 (https=)
RU (2) RU2011129251A (https=)
TW (1) TWI498314B (https=)
WO (1) WO2010072480A1 (https=)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102011089363A1 (de) * 2011-12-21 2013-06-27 Evonik Röhm Gmbh Verfahren zur Herstellung von N-Alkyl(meth)acrylamiden
US11136287B2 (en) 2017-03-01 2021-10-05 Api Corporation Method for producing n-benzyl-2-bromo-3-methoxypropionamide and intermediates thereof
CN107200695A (zh) * 2017-06-13 2017-09-26 山东瑞博龙化工科技股份有限公司 一种制备n‑羟乙基甲基丙烯酰胺的方法
CN107245039A (zh) * 2017-06-13 2017-10-13 山东瑞博龙化工科技股份有限公司 一种制备n‑羟乙基丙烯酰胺的方法
US11505520B2 (en) 2018-05-23 2022-11-22 Evonik Operations Gmbh Method for preparing keto-functionalized aromatic (meth)acrylates
EP3652151B1 (en) 2018-07-17 2020-08-12 Evonik Operations GmbH Method for preparing c-h acidic (meth)acrylates
EP3599232A1 (de) * 2018-07-26 2020-01-29 Evonik Operations GmbH Verfahren zur herstellung von n-methyl(meth)acrylamid

Family Cites Families (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1250421A (https=) * 1968-02-05 1971-10-20
CH580572A5 (https=) 1973-10-03 1976-10-15 Lonza Ag
US4288592A (en) * 1979-04-30 1981-09-08 American Cyanamid Company Process for preparing amides by reaction in presence of molecular sieve
DE3130508A1 (de) * 1981-08-01 1983-02-17 Röhm GmbH, 6100 Darmstadt "verfahren zur herstellung von methacryl- und acrylamiden"
DE3131096A1 (de) 1981-08-06 1983-02-24 Röhm GmbH, 6100 Darmstadt Verfahren zur herstellung von n-substituierten methacryl- und acrylamiden
DE3412650A1 (de) * 1984-04-04 1985-10-17 Röhm GmbH, 6100 Darmstadt Verfahren zur herstellung von hydroxyalkyl-acrylamiden und -methacrylamiden
FR2590567B1 (fr) * 1985-11-27 1988-07-15 Charbonnages Ste Chimique Nouveau procede de synthese de (meth)acrylamide de n-dialkylaminoalkyle
JPH03264549A (ja) 1990-03-15 1991-11-25 Sanyo Chem Ind Ltd 不飽和単量体の製造方法
RU2137740C1 (ru) 1995-06-08 1999-09-20 Эксон продакшн рисерч компани Способ ингибирования образования клатрат-гидратов в жидкости
DE10010811A1 (de) * 2000-03-08 2001-09-13 Basf Ag Verfahren zur Herstellung von Polymeren
US6753431B2 (en) * 2000-06-02 2004-06-22 Sumitomo Chemical Company Limited Production of mixed acid anhydride and amide compound
US20040024152A1 (en) * 2000-07-28 2004-02-05 Masayuki Toyama Gas hydrate formation inhibitor and method for inhibiting gas hydrate formation with the same
WO2005121133A1 (en) * 2004-06-11 2005-12-22 Takeda Pharmaceutical Company Limited Highly selective novel amidation method
DE102006047617B4 (de) 2006-10-09 2008-11-27 Clariant International Limited Verfahren zur Herstellung basischer (Meth)acrylamide
US8445723B2 (en) 2008-08-19 2013-05-21 Nalco Company Processes for producing N-alkyl (alkyl)acrylamides

Also Published As

Publication number Publication date
EP2358664B1 (de) 2020-03-25
US20110218312A1 (en) 2011-09-08
TWI498314B (zh) 2015-09-01
CN106631862A (zh) 2017-05-10
EP3680231A1 (de) 2020-07-15
WO2010072480A1 (de) 2010-07-01
JP2012512217A (ja) 2012-05-31
RU2015101155A3 (https=) 2018-08-31
JP2015134794A (ja) 2015-07-27
TW201035015A (en) 2010-10-01
US9512062B2 (en) 2016-12-06
DE102008054612A1 (de) 2010-06-17
ES2790593T3 (es) 2020-10-28
CN102197018A (zh) 2011-09-21
EP2358664A1 (de) 2011-08-24
RU2015101155A (ru) 2015-06-27
KR101853597B1 (ko) 2018-04-30
RU2011129251A (ru) 2013-01-20
KR20110099683A (ko) 2011-09-08
KR20170033910A (ko) 2017-03-27

Similar Documents

Publication Publication Date Title
JP2015134794A (ja) N−イソプロピル(メタ)アクリルアミドの製造方法
SK283507B6 (sk) Spôsob prípravy kyseliny (±)-3-(aminometyl)-5-metylhexánovej
CA3106334C (en) Method for preparing c-h acidic (meth)acrylates
WO2010126086A1 (ja) αβ不飽和カルボン酸-N,N二置換アミド及び3-アルコキシカルボン酸-N,N二置換アミドの製造方法
TW201815745A (zh) N,n-(二)烷基胺基烷基(甲基)丙烯醯胺或n,n-(二)烷基胺基烷基(甲基)丙烯酸酯之製備及其充當絮凝助劑和膠凝劑之四級銨鹽
JP7346544B2 (ja) N-メチル(メタ)アクリルアミドの製造方法
CA2581312C (en) Method for the continuous production of alkyl amino acryl amides
CA2758115C (en) Method for continuously producing alkylamino(meth)acrylamides
RS53772B1 (sr) Sinteza aliskirena
CN1071312C (zh) 2-氰基-3,3-二芳基丙烯酸酯的制备
CN107245039A (zh) 一种制备n‑羟乙基丙烯酰胺的方法
SK352009A3 (sk) Spôsob výroby beta-hydroxyalkylamidov
JP6844106B2 (ja) 不飽和カルボン酸シリルエステルの蒸留方法
CN112898338A (zh) 草铵膦中间体及草铵膦的制备方法
JPS63166852A (ja) エステル基を含有するn−置換アクリルアミド
TW200301250A (en) Purification method of (meth)acrylic acid ester
JP2003231664A (ja) (メタ)アクリル酸エステルの精製方法
HK1090632A1 (zh) 连续制备烷基氨基(甲基)丙烯酰胺的方法
HK1090632B (en) Method for continuously producing alkylamino (meth)acrylamides
JPS5929650A (ja) ピルビン酸またはそのエステルのシアンヒドリンの製造法
CA3050038A1 (en) Methods for producing (meth)acrylic acid norbornyl esters
WO2009127560A1 (en) Intermediates for the preparation of pregabalin and process for their preparation

Legal Events

Date Code Title Description
A621 Written request for application examination

Free format text: JAPANESE INTERMEDIATE CODE: A621

Effective date: 20121116

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20131111

A601 Written request for extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A601

Effective date: 20140210

A602 Written permission of extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A602

Effective date: 20140218

A601 Written request for extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A601

Effective date: 20140311

A602 Written permission of extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A602

Effective date: 20140318

A601 Written request for extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A601

Effective date: 20140411

A602 Written permission of extension of time

Free format text: JAPANESE INTERMEDIATE CODE: A602

Effective date: 20140418

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20140512

A02 Decision of refusal

Free format text: JAPANESE INTERMEDIATE CODE: A02

Effective date: 20141027

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20150227

A524 Written submission of copy of amendment under article 19 pct

Free format text: JAPANESE INTERMEDIATE CODE: A524

Effective date: 20150227

A911 Transfer to examiner for re-examination before appeal (zenchi)

Free format text: JAPANESE INTERMEDIATE CODE: A911

Effective date: 20150310

A131 Notification of reasons for refusal

Free format text: JAPANESE INTERMEDIATE CODE: A131

Effective date: 20150406

A521 Request for written amendment filed

Free format text: JAPANESE INTERMEDIATE CODE: A523

Effective date: 20150626

TRDD Decision of grant or rejection written
A01 Written decision to grant a patent or to grant a registration (utility model)

Free format text: JAPANESE INTERMEDIATE CODE: A01

Effective date: 20150721

A61 First payment of annual fees (during grant procedure)

Free format text: JAPANESE INTERMEDIATE CODE: A61

Effective date: 20150804

R150 Certificate of patent or registration of utility model

Ref document number: 5791511

Country of ref document: JP

Free format text: JAPANESE INTERMEDIATE CODE: R150

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

S111 Request for change of ownership or part of ownership

Free format text: JAPANESE INTERMEDIATE CODE: R313113

S531 Written request for registration of change of domicile

Free format text: JAPANESE INTERMEDIATE CODE: R313531

S533 Written request for registration of change of name

Free format text: JAPANESE INTERMEDIATE CODE: R313533

R350 Written notification of registration of transfer

Free format text: JAPANESE INTERMEDIATE CODE: R350

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250

R250 Receipt of annual fees

Free format text: JAPANESE INTERMEDIATE CODE: R250