JP2012508305A5 - - Google Patents
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- Publication number
- JP2012508305A5 JP2012508305A5 JP2011535782A JP2011535782A JP2012508305A5 JP 2012508305 A5 JP2012508305 A5 JP 2012508305A5 JP 2011535782 A JP2011535782 A JP 2011535782A JP 2011535782 A JP2011535782 A JP 2011535782A JP 2012508305 A5 JP2012508305 A5 JP 2012508305A5
- Authority
- JP
- Japan
- Prior art keywords
- alkyl
- aralkyl
- aryl
- solvent
- independently
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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- 239000002904 solvent Substances 0.000 claims description 34
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 claims description 27
- 229920000642 polymer Polymers 0.000 claims description 26
- 125000003118 aryl group Chemical group 0.000 claims description 25
- SCPYDCQAZCOKTP-UHFFFAOYSA-N silanol Chemical compound [SiH3]O SCPYDCQAZCOKTP-UHFFFAOYSA-N 0.000 claims description 25
- 238000000034 method Methods 0.000 claims description 24
- 125000000217 alkyl group Chemical group 0.000 claims description 21
- 150000001993 dienes Chemical class 0.000 claims description 10
- 238000006116 polymerization reaction Methods 0.000 claims description 10
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 10
- 239000000178 monomer Substances 0.000 claims description 6
- 150000001875 compounds Chemical class 0.000 claims description 5
- 230000008569 process Effects 0.000 claims description 5
- 239000000463 material Substances 0.000 claims description 4
- 239000003607 modifier Substances 0.000 claims description 4
- 239000000126 substance Substances 0.000 claims description 4
- 239000004711 α-olefin Substances 0.000 claims description 4
- 230000008878 coupling Effects 0.000 claims description 3
- 239000007822 coupling agent Substances 0.000 claims description 3
- 238000010168 coupling process Methods 0.000 claims description 3
- 238000005859 coupling reaction Methods 0.000 claims description 3
- 230000000379 polymerizing effect Effects 0.000 claims description 3
- 238000004064 recycling Methods 0.000 claims description 3
- 125000003710 aryl alkyl group Chemical group 0.000 claims 21
- 125000001183 hydrocarbyl group Chemical group 0.000 claims 13
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims 10
- 125000004178 (C1-C4) alkyl group Chemical group 0.000 claims 6
- 125000000229 (C1-C4)alkoxy group Chemical group 0.000 claims 6
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims 6
- 239000001257 hydrogen Substances 0.000 claims 6
- 229910052739 hydrogen Inorganic materials 0.000 claims 6
- 229910052760 oxygen Inorganic materials 0.000 claims 6
- 239000001301 oxygen Substances 0.000 claims 6
- 229920006395 saturated elastomer Polymers 0.000 claims 6
- 229910052710 silicon Inorganic materials 0.000 claims 6
- 239000010703 silicon Substances 0.000 claims 6
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims 5
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims 5
- 150000001412 amines Chemical class 0.000 claims 5
- 150000001983 dialkylethers Chemical class 0.000 claims 5
- 229910052757 nitrogen Inorganic materials 0.000 claims 5
- 229910052717 sulfur Inorganic materials 0.000 claims 5
- 239000011593 sulfur Substances 0.000 claims 5
- 125000004001 thioalkyl group Chemical group 0.000 claims 5
- 125000003808 silyl group Chemical group [H][Si]([H])([H])[*] 0.000 claims 3
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims 2
- 125000001181 organosilyl group Chemical group [SiH3]* 0.000 claims 2
- XDTMQSROBMDMFD-UHFFFAOYSA-N Cyclohexane Chemical compound C1CCCCC1 XDTMQSROBMDMFD-UHFFFAOYSA-N 0.000 claims 1
- 239000005062 Polybutadiene Substances 0.000 claims 1
- 150000001335 aliphatic alkanes Chemical class 0.000 claims 1
- 229910000323 aluminium silicate Inorganic materials 0.000 claims 1
- 229920001577 copolymer Polymers 0.000 claims 1
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 claims 1
- 150000002431 hydrogen Chemical class 0.000 claims 1
- 125000004435 hydrogen atom Chemical group [H]* 0.000 claims 1
- 229920002857 polybutadiene Polymers 0.000 claims 1
- 239000000377 silicon dioxide Substances 0.000 claims 1
- 230000007246 mechanism Effects 0.000 description 11
- 230000004913 activation Effects 0.000 description 4
- 229910018512 Al—OH Inorganic materials 0.000 description 3
- 238000006664 bond formation reaction Methods 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 150000004819 silanols Chemical class 0.000 description 3
- 238000001179 sorption measurement Methods 0.000 description 3
- KPUWHANPEXNPJT-UHFFFAOYSA-N disiloxane Chemical class [SiH3]O[SiH3] KPUWHANPEXNPJT-UHFFFAOYSA-N 0.000 description 2
- 239000012454 non-polar solvent Substances 0.000 description 2
- -1 siloxanes Chemical class 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 229910008051 Si-OH Inorganic materials 0.000 description 1
- 229910002808 Si–O–Si Inorganic materials 0.000 description 1
- 229910006358 Si—OH Inorganic materials 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000004817 gas chromatography Methods 0.000 description 1
- UQEAIHBTYFGYIE-UHFFFAOYSA-N hexamethyldisiloxane Chemical compound C[Si](C)(C)O[Si](C)(C)C UQEAIHBTYFGYIE-UHFFFAOYSA-N 0.000 description 1
- 230000003993 interaction Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 230000007935 neutral effect Effects 0.000 description 1
- 239000003960 organic solvent Substances 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 125000005372 silanol group Chemical group 0.000 description 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US11330108P | 2008-11-11 | 2008-11-11 | |
| US61/113,301 | 2008-11-11 | ||
| PCT/US2009/063961 WO2010056694A1 (en) | 2008-11-11 | 2009-11-11 | Process to remove silanol from the preparation of a modified polymer |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2012508305A JP2012508305A (ja) | 2012-04-05 |
| JP2012508305A5 true JP2012508305A5 (enExample) | 2012-07-05 |
| JP5591816B2 JP5591816B2 (ja) | 2014-09-17 |
Family
ID=41559229
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2011535782A Expired - Fee Related JP5591816B2 (ja) | 2008-11-11 | 2009-11-11 | 変性ポリマーの製造からシラノールを除去する方法 |
Country Status (11)
| Country | Link |
|---|---|
| US (1) | US8952100B2 (enExample) |
| EP (1) | EP2358762B1 (enExample) |
| JP (1) | JP5591816B2 (enExample) |
| KR (1) | KR101707693B1 (enExample) |
| CN (1) | CN102216335B (enExample) |
| BR (1) | BRPI0915242A2 (enExample) |
| ES (1) | ES2444429T3 (enExample) |
| MX (1) | MX2011004961A (enExample) |
| PL (1) | PL2358762T3 (enExample) |
| RU (1) | RU2531821C2 (enExample) |
| WO (1) | WO2010056694A1 (enExample) |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR101604503B1 (ko) | 2008-06-06 | 2016-03-25 | 트린세오 유럽 게엠베하 | 개질된 탄성중합체성 중합체 |
| CN102933613B (zh) | 2009-12-21 | 2015-03-11 | 斯泰隆欧洲有限责任公司 | 改性聚合物组合物 |
| ES2439669T3 (es) | 2009-12-21 | 2014-01-24 | Styron Europe Gmbh | Composiciones poliméricas modificadas |
| SG11201401599VA (en) | 2011-12-07 | 2014-07-30 | Jsr Corp | Method for manufacturing modified polymer and hydrogen adduct thereof |
| KR102008415B1 (ko) | 2016-11-14 | 2019-10-21 | 주식회사 엘지화학 | 변성 공액디엔계 중합체 및 이의 제조방법 |
| KR102106806B1 (ko) | 2018-02-09 | 2020-05-06 | 주식회사 엘지화학 | 공액디엔계 중합체 제조방법 및 공액디엔계 중합체 제조장치 |
| EP3801446A4 (en) * | 2018-06-08 | 2022-03-09 | Adaptive Surface Technologies, Inc. | PENDANT FUNCTIONALIZED ORGANOSILOXANES, COATING COMPOSITIONS CONTAINING PENDANT FUNCTIONALIZED ORGANOSILOXANES, COATED ARTICLES AND PROCESSES FOR THEIR MANUFACTURE AND THEIR USE |
Family Cites Families (52)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2519344A (en) * | 1947-04-08 | 1950-08-22 | Union Oil Co | Adsorption process |
| IT582279A (enExample) * | 1957-04-02 | 1900-01-01 | Progil Electrochimie | |
| US3484427A (en) * | 1964-12-30 | 1969-12-16 | Phillips Petroleum Co | Diluent purification process and apparatus |
| GB1271265A (en) | 1968-06-08 | 1972-04-19 | Bridgestone Tire Co Ltd | Method of preparing conjugated diene polymers using catalysts based on organolithium compounds |
| US3951936A (en) | 1974-09-03 | 1976-04-20 | The Goodyear Tire & Rubber Company | Polymerization process |
| CA1212932A (en) | 1982-04-01 | 1986-10-21 | Derek K. Jenkins | Polymerisation of conjugated dienes |
| FR2567135B1 (fr) | 1984-07-03 | 1989-01-13 | Asahi Chemical Ind | Polymere ou copolymere de butadiene et procede de preparation |
| JPS62179506A (ja) * | 1986-01-27 | 1987-08-06 | ロクタイト．コ−ポレ−シヨン | ポリ光重合開始剤とその調製方法および該開始剤の性質を利用した硬化性組成物 |
| JPS63108082A (ja) | 1986-10-24 | 1988-05-12 | Hitachi Chem Co Ltd | 酸化ケイ素被膜形成用塗布液 |
| US5134199A (en) | 1987-11-27 | 1992-07-28 | Asahi Kasei Kogyo Kabushiki Kaisha | Diene block polymer and polymer composition |
| JP3048539B2 (ja) * | 1989-02-28 | 2000-06-05 | 鐘淵化学工業株式会社 | 有機重合体、その製造方法およびそれを用いた硬化性組成物 |
| JP2730163B2 (ja) | 1989-04-07 | 1998-03-25 | 日本合成ゴム株式会社 | 高トランス低ビニル共役ジエン系重合体の製造方法 |
| US5089574A (en) | 1990-10-22 | 1992-02-18 | The Goodyear Tire & Rubber Company | Trans-1,4-polybutadiene synthesis |
| EP1199313B1 (en) * | 1993-12-29 | 2005-08-24 | Bridgestone Corporation | Diene polymers and copolymers having an alkoxysilane group |
| US5448002A (en) | 1994-08-12 | 1995-09-05 | The Goodyear Tire & Rubber Company | Synthesis of trans-1,4-polybutadiene having controlled molecular weight |
| JPH08319352A (ja) * | 1995-05-25 | 1996-12-03 | Toray Dow Corning Silicone Co Ltd | オルガノポリシロキサンの精製方法 |
| WO1997006192A1 (en) | 1995-08-03 | 1997-02-20 | Fmc Corporation | Functionalized polystyrene/polydiene copolymers and processes for making same |
| IT1277581B1 (it) | 1995-09-14 | 1997-11-11 | Enichem Elastomers | Composizione elastomerica utile come battistrada per pneumatici |
| JP3580619B2 (ja) * | 1995-11-15 | 2004-10-27 | 旭化成ケミカルズ株式会社 | エチレン系重合体の製造方法 |
| US5753579A (en) | 1995-12-26 | 1998-05-19 | The Goodyear Tire & Rubber Company | Trans microstructure directing initiator system |
| US5753761A (en) | 1996-12-27 | 1998-05-19 | The Goodyear Tire & Rubber Company | Method of preparing trans polybutadiene blend for use in tires |
| EP0877034A1 (en) | 1997-05-05 | 1998-11-11 | The Goodyear Tire & Rubber Company | Random trans SBR with low vinyl microstructure |
| US5834573A (en) | 1997-05-21 | 1998-11-10 | The Goodyear Tire & Rubber Company | Synthesis of trans-1,4-polybutadiene |
| US6018007A (en) | 1997-09-22 | 2000-01-25 | Bridgestone Corporation | Synthesis of 1,4-trans-polybutadiene using a lanthanide organic acid salt catalyst |
| JP3709061B2 (ja) | 1997-10-28 | 2005-10-19 | 新日本製鐵株式会社 | 無機・有機ハイブリッドと無機粒子の複合体の製造方法 |
| US6197713B1 (en) | 1997-12-19 | 2001-03-06 | Bridgestone Corporation | Use of Lewis acids for the breakdown of gelatinous rare earth compounds in hydrocarbon solutions |
| JP3889509B2 (ja) | 1998-04-25 | 2007-03-07 | 株式会社フジキン | 流体分配用配管構造 |
| US6177603B1 (en) | 1998-06-12 | 2001-01-23 | Bridgestone Corporation | Organo zinc and rare earth catalyst system in the polymerization of conjugated dienes |
| US7015271B2 (en) | 1999-08-19 | 2006-03-21 | Ppg Industries Ohio, Inc. | Hydrophobic particulate inorganic oxides and polymeric compositions containing same |
| US6489415B2 (en) | 1999-12-31 | 2002-12-03 | The Goodyear Tire & Rubber Company | Process for synthesizing trans-1,4-polybutadiene |
| CA2425330A1 (fr) * | 2000-10-13 | 2002-04-18 | Jean-Claude Tardivat | Composition de caoutchouc comportant a titre d'agent de couplage un organosilane polyfonctionnel |
| US6310152B1 (en) | 2000-10-24 | 2001-10-30 | The Goodyear Tire & Rubber Company | Synthesis of elastomeric high trans-1,4-polybutadiene |
| US6627715B2 (en) | 2001-08-16 | 2003-09-30 | The Goodyear Tire & Rubber Company | Group IIa metal containing catalyst system |
| US6617406B2 (en) | 2001-08-30 | 2003-09-09 | The Goodyear Tire & Rubber Company | Synthesis of elastomeric high trans-1,4-polybutadiene |
| CA2461259C (en) | 2001-09-27 | 2011-01-04 | Jsr Corporation | Conjugated diolefin (co)polymer rubber, process for producing (co)polymer rubber, rubber composition, composite and tire |
| JP4129619B2 (ja) | 2001-09-27 | 2008-08-06 | Ｊｓｒ株式会社 | 共役ジオレフィン（共）重合ゴム、該（共）重合ゴムの製造方法、ゴム組成物およびタイヤ |
| CN100516103C (zh) | 2001-10-31 | 2009-07-22 | 米其林技术公司 | 轮胎胎面组合物用嵌段共聚物的制备方法,和这样的共聚物 |
| US6765065B2 (en) * | 2002-01-09 | 2004-07-20 | Sumitomo Chemical Company, Limited | Process for producing modified polymer rubber |
| DE10218977A1 (de) | 2002-04-27 | 2003-11-06 | Merck Patent Gmbh | Oberflächenmodifizierung von Phasenwechselmaterial |
| EP1367069A1 (en) | 2002-05-28 | 2003-12-03 | Dow Global Technologies Inc. | Process for homo-or copolymerization of conjugated diens |
| US6693160B1 (en) | 2002-08-16 | 2004-02-17 | The Goodyear Tire & Rubber Company | Functionalized monomers for synthesis of rubbery polymers |
| US6790920B2 (en) | 2002-09-12 | 2004-09-14 | Kraton Polymers U.S. Llc | Process for removal of silicon compounds from solvents by selective absorption |
| WO2004041398A2 (en) | 2002-10-30 | 2004-05-21 | Waters Investments Limited | Porous inorganic/organic hybrid materials and preparation thereof |
| US7125488B2 (en) | 2004-02-12 | 2006-10-24 | Varian, Inc. | Polar-modified bonded phase materials for chromatographic separations |
| TWI385182B (zh) * | 2004-03-15 | 2013-02-11 | Jsr Corp | Conjugated diene (co) poly rubber and method for producing the same |
| JP2005347575A (ja) * | 2004-06-03 | 2005-12-15 | Sharp Corp | 流体供給装置、洗浄装置および洗浄方法 |
| KR100588475B1 (ko) * | 2004-06-07 | 2006-06-09 | 한국화학연구원 | 폴리실록산계 화합물을 포함하는 고체 고분자 전해질 조성물 |
| EP1867604B1 (en) * | 2005-04-07 | 2013-05-15 | Toagosei Co., Ltd. | Method for purification of disilicon hexachloride and high purity disilicon hexachloride |
| JP5270356B2 (ja) | 2005-10-19 | 2013-08-21 | スティロン ヨーロッパ ゲゼルシャフト ミット ベシュレンクテル ハフツング | シラン−スルフィドにより鎖末端修飾されたエラストマーポリマー |
| JP4792575B2 (ja) | 2005-11-04 | 2011-10-12 | 国立大学法人 香川大学 | 撥水性ガラス板とその製造方法及びそれを用いた乗り物またはガラス窓 |
| WO2008076875A1 (en) | 2006-12-19 | 2008-06-26 | Dow Global Technologies Inc. | Sulfide modified elastomeric polymers |
| KR101604503B1 (ko) | 2008-06-06 | 2016-03-25 | 트린세오 유럽 게엠베하 | 개질된 탄성중합체성 중합체 |
-
2009
- 2009-11-11 JP JP2011535782A patent/JP5591816B2/ja not_active Expired - Fee Related
- 2009-11-11 US US13/128,512 patent/US8952100B2/en not_active Expired - Fee Related
- 2009-11-11 KR KR1020117013383A patent/KR101707693B1/ko not_active Expired - Fee Related
- 2009-11-11 RU RU2011123900/05A patent/RU2531821C2/ru not_active IP Right Cessation
- 2009-11-11 BR BRPI0915242A patent/BRPI0915242A2/pt not_active IP Right Cessation
- 2009-11-11 MX MX2011004961A patent/MX2011004961A/es active IP Right Grant
- 2009-11-11 PL PL09756607T patent/PL2358762T3/pl unknown
- 2009-11-11 CN CN200980145028.1A patent/CN102216335B/zh not_active Expired - Fee Related
- 2009-11-11 WO PCT/US2009/063961 patent/WO2010056694A1/en not_active Ceased
- 2009-11-11 ES ES09756607.9T patent/ES2444429T3/es active Active
- 2009-11-11 EP EP09756607.9A patent/EP2358762B1/en not_active Not-in-force
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