JP2011068892A - カーボンブラック、その製造方法並びにその使用 - Google Patents
カーボンブラック、その製造方法並びにその使用 Download PDFInfo
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- JP2011068892A JP2011068892A JP2010216534A JP2010216534A JP2011068892A JP 2011068892 A JP2011068892 A JP 2011068892A JP 2010216534 A JP2010216534 A JP 2010216534A JP 2010216534 A JP2010216534 A JP 2010216534A JP 2011068892 A JP2011068892 A JP 2011068892A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/03—Printing inks characterised by features other than the chemical nature of the binder
- C09D11/037—Printing inks characterised by features other than the chemical nature of the binder characterised by the pigment
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
- C09C1/44—Carbon
- C09C1/48—Carbon black
- C09C1/56—Treatment of carbon black ; Purification
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
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- C09D11/324—Inkjet printing inks characterised by colouring agents containing carbon black
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- G03G—ELECTROGRAPHY; ELECTROPHOTOGRAPHY; MAGNETOGRAPHY
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- G03G9/0902—Inorganic compounds
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/12—Surface area
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/19—Oil-absorption capacity, e.g. DBP values
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/60—Optical properties, e.g. expressed in CIELAB-values
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- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
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- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
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- Wood Science & Technology (AREA)
- Inorganic Chemistry (AREA)
- Physics & Mathematics (AREA)
- General Physics & Mathematics (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Pigments, Carbon Blacks, Or Wood Stains (AREA)
- Inks, Pencil-Leads, Or Crayons (AREA)
- Developing Agents For Electrophotography (AREA)
- Compositions Of Macromolecular Compounds (AREA)
Abstract
【解決手段】本発明の課題は、22PAK法により測定した重縮合した芳香族炭化水素の含有量が5ppm未満であり、STSA表面積<90m2/gであることを特徴とするカーボンブラック、電磁線を用いて出発カーボンブラックを処理することを特徴とするカーボンブラックの製造方法、ゴム、プラスチック、印刷インキ、インク、インクジェットインク、トナー、ラッカー、着色剤、接着剤、バッテリー、ペースト、紙、燃料電池、ビチューメン、コンクリート及び他の建材におけるカーボンブラックの使用により解決された。
【選択図】なし
Description
ベンズ(a)アントラセン、ベンゾ(k)フルオランテン、ジベンズ(ah)アントラセン、ベンゾ(a)ピレン、インデノ(1,2,3−cd)ピレン、ベンゾ(b)フルオランテン及びベンゾ(j)フルオランテン、ジベンズ(ah)アクリジン、ジベンズ(aj)アクリジン、7H−ジベンゾ(cg)カルバゾール、ジベンゾ(ae)ピレン、ジベンゾ(ah)ピレン、ジベンゾ(ai)ピレン、ジベンゾ(al)ピレン及び5−メチルクリセン、その際、ベンゾ(b)フルオランテン及びベンゾ(j)フルオランテンはそれぞれ単独で数えられる(8th report on carcinogens、US Department of Health and Human Services、III−869頁)。
1.出発カーボンブラック計量供給
2.ロック(Schleuse)
3.IR透明反応器
4.熱処理のためのカーボンブラック
5.輸送ガス流
6.振動駆動系
7.生成物−排出
8.8aの1以上のIR透明なウィンドウを有するIR放射体モジュール(IR-Strahlermodule)
9.IR放射体モジュールのための電気制御
10.トレース加熱(Begleitheizung)
11.排ガス流。
12.出発カーボンブラック計量供給
13.ロック
14.MW透明反応器
15.固体床、流動層又は気泡塔としての熱処理のためのカーボンブラック
16.輸送ガス流
17.インフロー底部(Anstroemboden)
18.生成物−排出
19.19aの1以上のMW透明なウィンドウを有する共振器
20.マイクロ波供給源
21.トレース加熱
22.排ガス流。
STSA表面積: ASTM D−6556
BET表面積: ASTM D−6556
DBP吸収: ASTM D−2414。
重縮合した芳香族炭化水素(PAKs)の含有量を減少させるために、図1中に示されるようなIR−パイロット装置(IR-Pilotanlage)中でペレット化したカーボンブラックを処理する。この滞留時間及び温度は表1に記載されている。
重芳香族炭化水素(PAKs)の含有量を減少させるために、図2中に記載されるようなマイクロ波装置中でペレット化したカーボンブラックを処理する。この滞留時間及び温度は表2に記載されている。
図2に記載されるようなマイクロ波装置中では、約80gの量の出発カーボンブラックAが充填される。マイクロ波反応器を窒素(5l/h)で試験開始前に洗浄し、引き続きマイクロ波を照射し、試験終了後に窒素下で温度<120℃に冷却する。
乾燥棚中での単純な温度処理についての比較例
STSA表面積75m2/g及び油価(流動点法DIN EN ISO787−5による)460g/100gを有する出発カーボンブラック100gを、ステンレス鋼片に30×30cmの面積に分散させる。窒素下で乾燥棚中で1時間300℃で温度処理する。
Claims (14)
- 22PAK法により測定した重縮合した芳香族炭化水素の含有量が5ppm未満であり、STSA表面積<90m2/gであることを特徴とするカーボンブラック。
- 重縮合した芳香族炭化水素の含有量が0.5ppm未満であることを特徴とする請求項1記載のカーボンブラック。
- 950℃での揮発性成分の含有量が>0.6%であることを特徴とする請求項1又は2記載のカーボンブラック。
- 950℃での揮発性成分の含有量が>2%であることを特徴とする請求項3記載のカーボンブラック。
- トルエン抽出物が0.04%未満であることを特徴とする請求項1から4までのいずれか1項記載のカーボンブラック。
- 電磁線を用いて出発カーボンブラックを処理することを特徴とする、22PAK法により測定した重縮合した芳香族炭化水素の含有量5ppm未満を有するカーボンブラックの製造方法。
- 電磁線としてマイクロ波線を使用することを特徴とする請求項6記載のカーボンブラックの製造方法。
- 不活性雰囲気を使用することを特徴とする請求項6又は7記載のカーボンブラックの製造方法。
- 出発カーボンブラックとしてガスブラックを使用することを使用することを特徴とする請求項6から8までのいずれか1項記載のカーボンブラックの製造方法。
- ゴム、プラスチック、印刷インキ、インク、インクジェットインク、トナー、ラッカー、着色剤、接着剤、バッテリー、ペースト、紙、燃料電池、ビチューメン、コンクリート及び他の建材における請求項1又は2記載のカーボンブラックの使用。
- 少なくとも1種のプラスチック及び請求項1記載のカーボンブラックを含有することを特徴とするプラスチック混合物。
- 5質量%未満の結合剤、少なくとも1種の保湿剤、溶媒及び請求項1記載のカーボンブラックを含有することを特徴とするインク。
- 少なくとも1種の流動剤、プラスチック及び請求項1記載のカーボンブラックを含有することを特徴とするトナー。
- 少なくとも1種の結合剤、溶媒及び請求項1記載のカーボンブラックを含有することを特徴とする印刷インキ。
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE102009045060.2 | 2009-09-28 | ||
DE102009045060A DE102009045060A1 (de) | 2009-09-28 | 2009-09-28 | Ruß, ein Verfahren zu seiner Herstellung sowie seine Verwendung |
Publications (2)
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JP2011068892A true JP2011068892A (ja) | 2011-04-07 |
JP6086641B2 JP6086641B2 (ja) | 2017-03-01 |
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JP2010216534A Active JP6086641B2 (ja) | 2009-09-28 | 2010-09-28 | カーボンブラック、その製造方法並びにその使用 |
Country Status (14)
Country | Link |
---|---|
US (1) | US8420044B2 (ja) |
EP (1) | EP2302004B1 (ja) |
JP (1) | JP6086641B2 (ja) |
KR (1) | KR20110034554A (ja) |
CN (1) | CN102060281B (ja) |
BR (1) | BRPI1003601A2 (ja) |
DE (1) | DE102009045060A1 (ja) |
ES (1) | ES2688478T3 (ja) |
HU (1) | HUE040461T2 (ja) |
MX (1) | MX2010010419A (ja) |
PL (1) | PL2302004T3 (ja) |
RU (1) | RU2010139583A (ja) |
TW (1) | TW201125935A (ja) |
ZA (1) | ZA201006865B (ja) |
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Publication number | Priority date | Publication date | Assignee | Title |
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JP2015511981A (ja) * | 2012-03-02 | 2015-04-23 | キャボット コーポレイションCabot Corporation | 低pah量を有する変性カーボンブラック及びそれを含むエラストマー |
WO2019065128A1 (ja) * | 2017-09-29 | 2019-04-04 | 富士フイルム株式会社 | 光硬化性組成物、積層体、及び、固体撮像素子 |
JPWO2019065128A1 (ja) * | 2017-09-29 | 2020-11-19 | 富士フイルム株式会社 | 光硬化性組成物、積層体、及び、固体撮像素子 |
JP7012733B2 (ja) | 2017-09-29 | 2022-01-28 | 富士フイルム株式会社 | 光硬化性組成物、積層体、及び、固体撮像素子 |
TWI788415B (zh) * | 2017-09-29 | 2023-01-01 | 日商富士軟片股份有限公司 | 光硬化性組成物、積層體及固體攝像元件 |
WO2024069744A1 (ja) * | 2022-09-27 | 2024-04-04 | 東海カーボン株式会社 | カーボンブラック及びカーボンブラックの製造方法 |
Also Published As
Publication number | Publication date |
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US20110076608A1 (en) | 2011-03-31 |
EP2302004A1 (de) | 2011-03-30 |
MX2010010419A (es) | 2011-03-28 |
ZA201006865B (en) | 2011-06-29 |
EP2302004B1 (de) | 2018-08-08 |
TW201125935A (en) | 2011-08-01 |
DE102009045060A1 (de) | 2011-03-31 |
CN102060281B (zh) | 2014-12-03 |
RU2010139583A (ru) | 2012-04-20 |
PL2302004T3 (pl) | 2019-01-31 |
JP6086641B2 (ja) | 2017-03-01 |
KR20110034554A (ko) | 2011-04-05 |
CN102060281A (zh) | 2011-05-18 |
BRPI1003601A2 (pt) | 2013-01-22 |
US8420044B2 (en) | 2013-04-16 |
ES2688478T3 (es) | 2018-11-02 |
HUE040461T2 (hu) | 2019-03-28 |
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