JP2011006413A - 高吸収性ポリマーおよび有機uv遮断剤を含む化粧品組成物 - Google Patents
高吸収性ポリマーおよび有機uv遮断剤を含む化粧品組成物 Download PDFInfo
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- JP2011006413A JP2011006413A JP2010142616A JP2010142616A JP2011006413A JP 2011006413 A JP2011006413 A JP 2011006413A JP 2010142616 A JP2010142616 A JP 2010142616A JP 2010142616 A JP2010142616 A JP 2010142616A JP 2011006413 A JP2011006413 A JP 2011006413A
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- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
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Abstract
【解決手段】本発明の対象は、少なくとも1つの水相および少なくとも1つの脂肪相、高吸収性ポリマーおよび少なくとも1種の有機UV遮断剤を含むエマルジョンの形態の化粧品組成物である。
【選択図】なし
Description
「高吸収性ポリマー」という用語は、乾燥状態で、ポリマー自体の重量の少なくとも20倍の水性流体、具体的には水、特に蒸留水を自然に吸収することができるポリマーを意味することが理解される。かかる高吸収性ポリマーは、1990年にElsevierに発表されたL. Brannon-PappasおよびR. Harlandによる研究「Absorbent Polymer Technology、Studies in Polymer Science 8」に記載されている。
-アクリルポリマー(ホモポリマーまたはコポリマー)によってグラフトされたデンプン、具体的には、三洋化成工業株式会社によってSanfresh ST-100C、ST100MCおよびIM-300MCという名で販売されているもの(INCI名:ポリアクリル酸ナトリウムデンプン)などのポリアクリル酸ナトリウムによってグラフトされたデンプン、
-アクリルポリマー(ホモポリマーまたはコポリマー)によってグラフトされた加水分解デンプン、具体的には、Grain Processing社によってWater Lock A-240、A-180、B-204、D-223、A-100、C-200およびD-223という名で販売されているもの(INCI名:デンプン/アクリルアミド/アクリル酸ナトリウムコポリマー)などのアクリロアクリルアミド/アクリル酸ナトリウムコポリマーによってグラフトされた加水分解デンプン、
-Lysac社によってLysorb 220という名で販売されている、デンプン、グアーガムおよびカルボキシメチルセルロースナトリウムを含むものなど、デンプン、ガムおよびセルロース誘導体に基づくポリマー、
-およびそれらの混合物から選択される吸収性ポリマーを特に挙げることができる。
有機遮断剤は、一般に、本発明による組成物中で、組成物の全重量に対して0.05〜30重量%の割合で、好ましくは組成物の全重量に対して0.1〜20重量%、さらには0.5〜15重量%の割合で存在する。
ジベンゾイルメタン誘導体:
-以下の式に対応する、Merck社によって「Eusolex 8020」という名で販売されている4-イソプロピルジベンゾイルメタン:
アミノベンゾフェノン:
「Uvinul A+」という商品名で販売されている2-(4-ジエチルアミノ-2-ヒドロキシベンゾイル)安息香酸n-ヘキシル、
アントラニル酸誘導体:
Haarmann and Reimer社によって「Neo Heliopan MA」という商品名で販売されているアントラニル酸メンチル、
4,4-ジアリールブタジエン誘導体:
1,1-ジカルボキシ-(2,2'-ジメチルプロピル)-4,4-ジフェニルブタジエンを挙げることができる。
パラアミノベンゾアート:
エチルPABA
エチルジヒドロキシプロピルPABA
エチルヘキシルジメチルPABA(ISP社からのEscalol 507)
サリチル酸誘導体:
Rona/EM Industries社によって「Eusolex HMS」という名で販売されているホモサラート、
Haarmann and Reimer社によって「Neo Heliopan OS」という名で販売されているサリチル酸エチルヘキシル、
Scher社によって「Dipsal」という名で販売されているサリチル酸ジプロピレングリコール、
Haarmann and Reimer社によって「Neo Heliopan TS」という名で販売されているサリチル酸TEA、
シンナマート:
具体的にはHoffmann-La Roche社によって「Parsol MCX」という商品名で販売されているメトキシケイ皮酸エチルヘキシル、
メトキシケイ皮酸イソプロピル、
Haarmann and Reimer社によって「Neo Heliopan E 1000」という商品名で販売されているメトキシケイ皮酸イソアミル、
メトキシケイ皮酸ジイソプロピル、
シノキサート、
ジメトキシケイ皮酸エチルへキサン酸グリセリル、
β,β-ジフェニルアクリラート誘導体:
具体的にはBASF社によって「Uvinul N539」という商品名で販売されているオクトクリレン、
具体的にはBASF社によって「Uvinul N35」という商品名で販売されているエトクリレン、
ベンジリデンカンファー誘導体:
Chimex社によって「Mexoryl SD」という名で製造されている3-ベンジリデンカンファー、
Merck社によって「Eusolex 6300」という名で販売されているメチルベンジリデンカンファー、
Chimex社によって「Mexoryl SW」という名で製造されているポリアクリルアミドメチルベンジリデンカンファー、
トリアジン誘導体:
具体的には、BASF社によって「Uvinul T150」という商品名で販売されているエチルヘキシルトリアゾン、
Sigma 3V社によって「Uvasorb HEB」という商品名で販売されているジエチルヘキシルブタミドトリアゾン、
2,4,6-トリス(4'-アミノベンザルマロン酸ジネオペンチル)-s-トリアジン、
2,4,6-トリス(4'-アミノベンザルマロン酸ジイソブチル)-s-トリアジン、
2,4-ビス(4'-アミノベンザルマロン酸ジネオペンチル)-6-(4'-アミノ安息香酸n-ブチル)-s-トリアジン、
2,4-ビス(4'-アミノ安息香酸n-ブチル)-6-(アミノプロピル-トリシロキサン)-s-トリアジン、
イミダゾリン誘導体:
ジメトキシベンジリデンジオキソイミダゾリンプロピオン酸エチルヘキシル、
ベンザルマロナート誘導体:
Hoffmann-La Roche社によって「Parsol SLX」という商品名で販売されているポリシリコーン-15などのベンザルマロナート官能基を含むポリオルガノシロキサン、
4'-メトキシベンザルマロン酸ジネオペンチル、
メロシアニン誘導体:
5-N,N-ジエチルアミノ-2-フェニルスルホニル-2,4-ペンタジエン酸オクチルを挙げることができる。
ベンゾフェノン誘導体:
BASF社によって「Uvinul 400」という商品名で販売されているベンゾフェノン-1、
BASF社によって「Uvinul D50」という商品名で販売されているベンゾフェノン-2、
BASF社によって「Uvinul M40」という商品名で販売されているベンゾフェノン-3またはオキシベンゾン、
Norquay社によって「Helisorb 11」という商品名で販売されているベンゾフェノン-6、
American Cyanamid社によって「Spectra-Sorb UV-24」という商品名で販売されているベンゾフェノン-8、
ベンゾフェノン-10、
ベンゾフェノン-11、
ベンゾフェノン-12、
ベンゾトリアゾール誘導体:
Rhodia Chimie社によって「Silatrizole」という名で販売されているドロメトリゾールトリシロキサン、
Ciba-Geigy社によって「Tinoguard AS」という名で販売されているブメトリゾール、
ビスレソルシニルトリアジン誘導体:
Ciba Geigy社によって「Tinosorb S」という商品名で販売されているビスエチルヘキシルオキシフェノールメトキシフェニルトリアジン、
ベンゾオキサゾール誘導体:
Sigma 3V社によってUvasorb K2Aという名で販売されている2,4-ビス[5-1(ジメチルプロピル)ベンゾオキサゾル-2-イル-(4-フェニル)イミノ]-6-(2-エチルヘキシル)イミノ-1,3,5-トリアジンを挙げることができる。
R4およびR5は、同一であるかまたは異なっており、-COOR6、-(C=O)NHR6、-(C=O)R6または-CNを表す(式中、R6は1〜12個の炭素原子を含みシラン、シロキサンまたはポリシロキサン基を含むことができる、直鎖または分枝状のアルキル基を表す)。
- 2-(3,3-ジフェニルプロプ-2-エニリデン)マロン酸ジメチル
- 2-(3,3-ジフェニルプロプ-2-エニリデン)マロン酸ジイソブチル
- 2-(3,3-ジフェニルプロプ-2-エニリデン)マロン酸ビス(1,3-ジメチルブチル)
- 2-(3,3-ジフェニルプロプ-2-エニリデン)マロン酸ジネオペンチル
- (2Z)-2-シアノ-5,5-ジフェニルペンタ-2,4-ジエン酸メチル
- (2Z)-2-(3,3-ジフェニルプロプ-2-エニリデン)マロン酸エチル(トリメチルシリル)メチル
- (2E)-2-シアノ-5,5-ジフェニル-N-(3-{1,3,3,3-テトラメチル-1-[(トリメチルシリル)オキシ]ジシロキサニル}プロピル)ペンタ-2,4-ジエンアミド
- 2-メチル-3-{1,3,3,3-テトラメチル-1-[(トリメチルシリル)オキシ]ジシロキサニル}プロピル(2E)-2-(3,3-ジフェニルプロプ-2-エニリデン)マロン酸エチル
- (2Z)-5,5-ジフェニル-2-{[(3-{1,3,3,3-テトラメチル-1-[(トリメチルシリル)オキシ]ジシロキサニル}プロピル)アミノ]カルボニル}ペンタ-2,4-ジエン酸エチル。
を挙げることができる。
pおよびqを意味する
- 2'-ヒドロキシカルコン
- 4'-ヒドロキシカルコン
- 4'-メトキシカルコン
- 2'-ヒドロキシ-4-メトキシカルコン
- 2'-ヒドロキシ-4-ヘキシルオキシカルコン
- 2'-ヒドロキシ-4-メチルカルコン
- 2'-ヒドロキシ-3-ヘキシルオキシカルコン
- 2'-ヒドロキシ-4'-ヘキシルオキシ-4-メチルカルコン
- 2'-ヒドロキシ-4'-ヘキサノイルオキシ-4-メトキシカルコン
- 2',4',4-トリヒドロキシ-3,3'-ジアリルカルコン(Kazonolという名で知られている)
-2',4',4-トリヒドロキシ-5'-(3-メチルブト-2-エニル)カルコン(Broussochalcone Bという名で知られている)
-2',3',4',6',4-ペンタヒドロキシカルコン(Carthaminという名で知られている)を挙げることができる。
または以下の式(Vb):
-サリチル酸誘導体、具体的にはホモサラートまたはサリチル酸エチルヘキシル、
-メトキシケイ皮酸エチルヘキシルなどのケイ皮酸誘導体、
-オクトクリレンなどのβ,β-ジフェニルアクリラート誘導体、
-ブチルメトキシジベンゾイルメタンなどのジベンゾイルメタン誘導体、
-エチルヘキシルトリアゾンまたはジエチルヘキシルブタミドトリアゾンなどのトリアジン誘導体、
-ドロメトリゾールトリシロキサンなどのベンゾトリアゾール誘導体、
-およびそれらの混合物
から選択することができる。
Chimex社によって「Mexoryl SX」という名で製造されているテレフタリリデンジカンファースルホン酸、欧州特許第669 323号および米国特許第2,463,264号に記載されているなどのビスベンゾオキサゾリル誘導体、より具体的には、Haarmann and Reimer社によって「Neo Heliopan AP」という商品名で販売されている化合物フェニルジベンズイミダゾールテトラスルホン酸二ナトリウムなどの320〜400nmのUV線を吸収することができる水溶性UV-A遮断剤:
PABA、グリセリルPABAおよびBASF社によって「Uvinul P25」という名で販売されているPEG-25 PABAなどのp-アミノ安息香酸(PABA)誘導体、
具体的には、Merck社によって「Eusolex 232」という商品名で販売されているフェニルベンズイミダゾールスルホン酸、
フェルラ酸、
サリチル酸、
メトキシケイ皮酸DEA、
Chimex社によって「Mexoryl SL」という名で製造されているベンジリデンカンファースルホン酸、
Chimex社によって「Mexoryl SO」という名で製造されているカンファーベンザルコニウムメトスルファートなどの280〜320nmのUV線を吸収することができる水溶性UV-B遮断剤、および
BASF社によって「Uvinul MS40」という商品名で販売されているベンゾフェノン-4、
ベンゾフェノン-5、および
ベンゾフェノン-9などの水溶性UV-AおよびUV-B遮断剤を挙げることができる。
本発明による組成物の水相は、少なくとも水を含む。組成物の配合形態に応じて、水相の量は、組成物の全重量に対して0.1〜99重量%、好ましくは0.5〜98重量%、さらには30〜95重量%、さらにより良いのは40〜95重量%の範囲となり得る。この量は、所望の組成物の配合形態に依存する。水の量は、すべてのまたは一部の水相を表すことができ、それは一般に組成物の全重量に対して少なくとも30重量%である。
エマルジョンの脂肪相の割合は、例えば、組成物の全重量に対して1〜80重量%、好ましくは2〜50重量%、さらには5〜30重量%の範囲となり得る。
-ペルヒドロスクアレンなど、動物由来の炭化水素油;
-ヘプタン酸またはオクタン酸のトリグリセリド、または、例えば、ヒマワリ油、トウモロコシ油、大豆油、キュウリ油、グレープシード油、ゴマ油、ヘーゼルナッツ油、杏油、マカダミア油、アララ油、ヒマシ油またはアボカド油、Stearineries Dubois社によって販売されているものまたはDynamit Nobel社によってMiglyol 810、812および818という名で販売されているものなどのカプリル酸/カプリン酸のトリグリセリド、ホホバ油またはシアバター油など、4〜10個の炭素原子を含む脂肪酸液体トリグリセリドなどの、植物由来の炭化水素油;
-例えば、ピュアセリン油、イソノナン酸イソノニル、ミリスチン酸イソプロピル、パルミチン酸2-エチルヘキシル、ステアリン酸2-オクチルドデシル、エルカ酸2-オクチルドデシルまたはイソステアリン酸イソステアリル;乳酸イソステアリル、ヒドロキシステアリン酸オクチル、ヒドロキシステアリン酸オクチルドデシル、リンゴ酸ジイソステアリル、クエン酸トリイソセチルまたは脂肪アルコールのヘプタナート、オクタナートもしくはデカノアートなどのヒドロキシル化エステル;ジオクタン酸プロピレングリコール、ジヘプタン酸ネオペンチルグリコールおよびジイソノナン酸ジエチレングリコールなどのポリオールエステル;およびテトライソステアリン酸ペンタエリスリチルなどのペンタエリスリトールエステルなど、油または式RaCOORbおよびRaORb(式中、Raは、8〜29個の炭素原子を含む脂肪酸の残基を表し、Rbは、3〜30個の炭素原子を含む分枝または非分枝炭化水素鎖を表す)などの特に脂肪酸の合成エステルおよびエーテル;
-揮発性であってもなくてもよい流動パラフィンおよびそれらの誘導体、ワセリン、ポリデセン、イソヘキサデカン、イソドデカンまたはParleam(登録商標)油などの水素化ポリイソブテンなどの、鉱物由来または合成由来の実質的に直鎖または分枝状の炭化水素;
-セチルアルコール、ステアリルアルコールおよびそれらの混合物(セテアリルアルコール)、オクチルドデカノール、2-ブチルオクタノール、2-ヘキシルデカノール、2-ウンデシルペンタデカノール、オレイルアルコールまたはリノレイルアルコールなど、8〜26個の炭素原子を有する脂肪アルコール;
-アルコキシ化脂肪アルコール、具体的には、oleth-12、セテアレス-12およびセテアレス-20などのエトキシ化脂肪アルコール;
-特開平2-295912号の文献に記載されているものなど、炭化水素および/またはシリコーンを部分的に含むフッ素化油。フッ素化油として、BNFL Fluorochemicals社によって「Flutec PC1(登録商標)」および「Flutec PC3(登録商標)」という名で販売されているペルフルオロメチルシクロペンタンおよびペルフルオロ-1,3-ジメチルシクロヘキサン;ペルフルオロ-1,2-ジメチルシクロブタン;3M社によって「PF 5050(登録商標)」および「PF 5060(登録商標)」という名で販売されているドデカフルオロペンタンおよびテトラデカフルオロヘキサン、またはAtochem社によって「Foralkyl(登録商標)」という名で販売されているブロモペルフルオロオクチルなどのペルフルオロアルカン;3M社によって「MSX 4518(登録商標)」という名で販売されているノナフルオロメトキシブタン、およびノナフルオロエトキシイソブタン;または3M社によって「PF 5052(登録商標)」という名で販売されている4-(トリフルオロメチル)ペルフルオロモルホリンなどのペルフルオロモルホリン誘導体;
-周囲温度で液体またくはペーストである実質的に直鎖または環式のシリコーン鎖を含む揮発性または不揮発性ポリメチルシロキサン(PDMS)などのシリコーン油、具体的には、シクロヘキサジメチルシロキサンおよびシクロオエンタジメチルシロキサンなどのシクロポリジメチルシロキサン(シクロメチコン);ペンダントアルキル、アルコキシもしくはフェニル基またはシリコーン鎖の末端のアルキル、アルコキシもしくはフェニル基を含むポリジメチルシロキサンであり、これらの基は2〜24個の炭素原子を有するポリジメチルシロキサン;または、フェニルトリメチコン、フェニルジメチコン、フェニル(トリメチルシロキシ)ジフェニルシロキサン、ジフェニルジメチコン、ジフェニル(メチルジフェニル)-トリシロキサン、(2-フェニルエチル)トリメチルシロキシシリカートおよびポリメチルフェニルシロキサンなどのフェニル化シリコーン;
-それらの混合物を挙げることができる。
上記で示したように、本発明の組成物は、酸化感受性親水性有効成分の存在下で安定であり、前記有効成分を安定化することができる。本発明によれば、「親水性有効成分」という用語は、周囲温度(25℃)で少なくとも0.25%の水に溶解性を有する化合物を意味するものと理解される。さらに、本発明によれば、「酸化感受性親水性有効成分」という用語は、酸化機序によって分解されることのできる天然起源または合成起源の任意の有効成分を意味するものと理解される。このような酸化現象は、いくつかの原因、特に酸素、光または金属イオンの存在、高温またはある種のpH状態を有し得る。
(実施例1〜3)保湿用O/W型エマルジョン SPF15
親油性遮断剤および高吸収性ポリマーを含む本発明による組成物(実施例1)および親油性日焼け止めおよび高吸収性ではないアクリルポリマーを含む2つの比較組成物(実施例2および3)を調製する。
相Aを85℃まで加熱し、次いで75℃に戻す。
親油性遮断剤および高吸収性ポリマーを含む本発明による組成物(実施例4)および親油性日焼け止めおよび高吸収性でないアクリルポリマーを含む比較組成物(実施例5)を調製する。
相Aを85℃まで加熱し、次いで75℃に戻す。
Claims (15)
- 少なくとも1つの水相および少なくとも1つの脂肪相、高吸収性ポリマーおよび少なくとも1種の有機UV遮断剤を含むエマルジョンの形態の化粧品組成物。
- 高吸収性ポリマーが、10μm〜1000μmの数平均直径を有する粒子の形態で提供されることを特徴とする、請求項1に記載の組成物。
- 高吸収性ポリマーが、100μm以下、好ましくは50μm以下の数平均直径を有する粒子の形態で提供されることを特徴とする、請求項1または請求項2に記載の組成物。
- 高吸収性ポリマーが、10〜100g/g、好ましくは20〜80g/g、さらには50〜70g/gの吸水能を示すことを特徴とする、請求項1から3の一項に記載の組成物。
- 高吸収性ポリマーが、架橋ポリアクリル酸ナトリウム、アクリルポリマーによってグラフトされたデンプン、アクリルポリマー、特にアクリロアクリルアミド/アクリル酸ナトリウムコポリマーによってグラフトされた加水分解デンプン、デンプン、ガムおよびセルロース誘導体に基づくポリマー、およびそれらの混合物から選択されることを特徴とする、請求項1から4の一項に記載の組成物。
- 高吸収性ポリマーが、好ましくは中和されている架橋アクリルホモポリマーまたはコポリマーから選択されることを特徴とする、請求項1から5の一項に記載の組成物。
- 高吸収性ポリマーが架橋ポリアクリル酸ナトリウムから選択されることを特徴とする、請求項1から6の一項に記載の組成物。
- 高吸収性ポリマーが球状粒子の形態で提供されることを特徴とする、請求項1から7の一項に記載の組成物。
- 高吸収性ポリマーが、活性物質として、組成物の全重量に対して0.03〜15重量%、好ましくは0.05〜10重量%、好ましくは0.1〜5重量%、優先的に0.1〜3重量%、さらには0.1〜2重量%の含有量で存在することを特徴とする、請求項1から8の一項に記載の組成物。
- 少なくとも1種の親油性有機UV遮断剤を含むことを特徴とする、請求項1から9の一項に記載の組成物。
- 親油性有機日焼け止めが、パラアミノ安息香酸誘導体、サリチル酸誘導体、ケイ皮酸誘導体、ベンゾフェノンまたはアミノベンゾフェノン、アントラニル酸誘導体、ジベンゾイルメタン誘導体、β,β-ジフェニルアクリラート誘導体、ベンジリデンカンファー誘導体、フェニルベンゾイミダゾール誘導体、ベンゾトリアゾール誘導体、トリアジン誘導体、ビスレソルシニルトリアジン、イミダゾリン誘導体、ベンザルマロナート誘導体、4,4-ジアリールブタジエン誘導体、ベンゾオキサゾール誘導体、メロシアニン、ジフェニルブタジエンマロナート誘導体またはジフェニルブタジエンマロニトリル誘導体、カルコンおよびそれらの混合物
から選択されることを特徴とする、請求項10に記載の組成物。 - 親油性有機日焼け止めが、
サリチル酸誘導体、具体的にはホモサラートまたはサリチル酸エチルヘキシル、
メトキシケイ皮酸エチルヘキシルなどのケイ皮酸誘導体、
オクトクリレンなどのβ,β-ジフェニルアクリラート誘導体、
ブチルメトキシジベンゾイルメタンなどのジベンゾイルメタン誘導体、
エチルヘキシルトリアゾンまたはジエチルヘキシルブタミドトリアゾンなどのトリアジン誘導体、
ドロメトリゾールトリシロキサンなどのベンゾトリアゾール誘導体、
およびそれらの混合物
から選択されることを特徴とする、請求項10および11のいずれかに記載の組成物。 - 少なくとも1種の親水性有機UV遮断剤を含むことを特徴とする、請求項1から12の一項に記載の組成物。
- 有機遮断剤が、組成物の全重量に対して0.05〜30重量%の割合で、組成物の全重量に対して、好ましくは0.1〜20重量%、さらには0.5〜15重量%の割合で存在することを特徴とする、請求項1から13の一項に記載の組成物。
- 請求項1から14のいずれか一項により定義される化粧品組成物が、角質性物質に適用されることを特徴とする、角質性物質の美容的処置方法。
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FR0954311 | 2009-06-24 | ||
FR0954311A FR2947174B1 (fr) | 2009-06-24 | 2009-06-24 | Composition cosmetique comprenant un polymere superabsorbant et un filtre uv organique |
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EP (1) | EP2266531B1 (ja) |
JP (2) | JP6250258B2 (ja) |
CN (2) | CN107028798A (ja) |
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KR20140055343A (ko) * | 2012-10-31 | 2014-05-09 | (주)아모레퍼시픽 | 수용성 점증제를 함유하는 수분산 화장료 조성물 |
JP2015510897A (ja) * | 2012-03-19 | 2015-04-13 | ザ プロクター アンド ギャンブルカンパニー | スキンケア組成物において使用するための超吸収性ポリマー及びシリコーンエラストマー |
JP2016147813A (ja) * | 2015-02-10 | 2016-08-18 | 住友精化株式会社 | 紫外線吸収剤を含有する組成物 |
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JP2015510897A (ja) * | 2012-03-19 | 2015-04-13 | ザ プロクター アンド ギャンブルカンパニー | スキンケア組成物において使用するための超吸収性ポリマー及びシリコーンエラストマー |
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Also Published As
Publication number | Publication date |
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US20100330018A1 (en) | 2010-12-30 |
US20150224046A1 (en) | 2015-08-13 |
CN101926744A (zh) | 2010-12-29 |
JP6250258B2 (ja) | 2017-12-20 |
JP2016028105A (ja) | 2016-02-25 |
ES2634898T3 (es) | 2017-09-29 |
EP2266531A1 (fr) | 2010-12-29 |
EP2266531B1 (fr) | 2017-06-14 |
FR2947174A1 (fr) | 2010-12-31 |
FR2947174B1 (fr) | 2011-07-15 |
CN107028798A (zh) | 2017-08-11 |
CN101926744B (zh) | 2017-04-12 |
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