JP2008540422A5 - - Google Patents
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- Publication number
- JP2008540422A5 JP2008540422A5 JP2008510104A JP2008510104A JP2008540422A5 JP 2008540422 A5 JP2008540422 A5 JP 2008540422A5 JP 2008510104 A JP2008510104 A JP 2008510104A JP 2008510104 A JP2008510104 A JP 2008510104A JP 2008540422 A5 JP2008540422 A5 JP 2008540422A5
- Authority
- JP
- Japan
- Prior art keywords
- phenol
- bromopropane product
- product mixture
- weight
- composition
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000000203 mixture Substances 0.000 claims 41
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 claims 40
- CYNYIHKIEHGYOZ-UHFFFAOYSA-N 1-bromopropane Chemical compound CCCBr CYNYIHKIEHGYOZ-UHFFFAOYSA-N 0.000 claims 36
- 125000004432 carbon atom Chemical group C* 0.000 claims 14
- 238000000034 method Methods 0.000 claims 13
- 125000000217 alkyl group Chemical group 0.000 claims 12
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 claims 8
- CPELXLSAUQHCOX-UHFFFAOYSA-N Hydrogen bromide Chemical compound Br CPELXLSAUQHCOX-UHFFFAOYSA-N 0.000 claims 6
- 125000004435 hydrogen atom Chemical group [H]* 0.000 claims 6
- 125000002887 hydroxy group Chemical group [H]O* 0.000 claims 6
- NWVVVBRKAWDGAB-UHFFFAOYSA-N p-methoxyphenol Chemical compound COC1=CC=C(O)C=C1 NWVVVBRKAWDGAB-UHFFFAOYSA-N 0.000 claims 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 6
- 239000007864 aqueous solution Substances 0.000 claims 5
- 150000007529 inorganic bases Chemical class 0.000 claims 5
- DKCPKDPYUFEZCP-UHFFFAOYSA-N 2,6-di-tert-butylphenol Chemical compound CC(C)(C)C1=CC=CC(C(C)(C)C)=C1O DKCPKDPYUFEZCP-UHFFFAOYSA-N 0.000 claims 3
- XESZUVZBAMCAEJ-UHFFFAOYSA-N 4-tert-butylcatechol Chemical compound CC(C)(C)C1=CC=C(O)C(O)=C1 XESZUVZBAMCAEJ-UHFFFAOYSA-N 0.000 claims 3
- NLZUEZXRPGMBCV-UHFFFAOYSA-N Butylhydroxytoluene Chemical compound CC1=CC(C(C)(C)C)=C(O)C(C(C)(C)C)=C1 NLZUEZXRPGMBCV-UHFFFAOYSA-N 0.000 claims 3
- 125000003118 aryl group Chemical group 0.000 claims 3
- 229910000042 hydrogen bromide Inorganic materials 0.000 claims 3
- DOIRQSBPFJWKBE-UHFFFAOYSA-N phthalic acid di-n-butyl ester Natural products CCCCOC(=O)C1=CC=CC=C1C(=O)OCCCC DOIRQSBPFJWKBE-UHFFFAOYSA-N 0.000 claims 3
- BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 claims 3
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims 2
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims 2
- WYURNTSHIVDZCO-UHFFFAOYSA-N Tetrahydrofuran Chemical group C1CCOC1 WYURNTSHIVDZCO-UHFFFAOYSA-N 0.000 claims 2
- 125000003545 alkoxy group Chemical group 0.000 claims 2
- 229910052799 carbon Inorganic materials 0.000 claims 2
- UOCJDOLVGGIYIQ-PBFPGSCMSA-N cefatrizine Chemical group S([C@@H]1[C@@H](C(N1C=1C(O)=O)=O)NC(=O)[C@H](N)C=2C=CC(O)=CC=2)CC=1CSC=1C=NNN=1 UOCJDOLVGGIYIQ-PBFPGSCMSA-N 0.000 claims 2
- 229910052739 hydrogen Inorganic materials 0.000 claims 2
- 239000001257 hydrogen Substances 0.000 claims 2
- 125000004430 oxygen atom Chemical group O* 0.000 claims 2
- 150000002989 phenols Chemical class 0.000 claims 2
- 125000000999 tert-butyl group Chemical group [H]C([H])([H])C(*)(C([H])([H])[H])C([H])([H])[H] 0.000 claims 2
- 150000001875 compounds Chemical class 0.000 claims 1
- 238000000746 purification Methods 0.000 claims 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US67727705P | 2005-05-03 | 2005-05-03 | |
| US60/677,277 | 2005-05-03 | ||
| PCT/US2006/016668 WO2006119212A2 (en) | 2005-05-03 | 2006-05-01 | 1-bromopropane having low acidity |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2008540422A JP2008540422A (ja) | 2008-11-20 |
| JP2008540422A5 true JP2008540422A5 (enExample) | 2009-06-18 |
| JP5055267B2 JP5055267B2 (ja) | 2012-10-24 |
Family
ID=37056960
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2008510104A Expired - Fee Related JP5055267B2 (ja) | 2005-05-03 | 2006-05-01 | 酸性度が低い１−ブロモプロパン |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US20080177116A1 (enExample) |
| EP (1) | EP1883615A2 (enExample) |
| JP (1) | JP5055267B2 (enExample) |
| CN (1) | CN101171218B (enExample) |
| AR (1) | AR057284A1 (enExample) |
| TW (1) | TW200712040A (enExample) |
| WO (1) | WO2006119212A2 (enExample) |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101171220B (zh) * | 2005-05-03 | 2012-06-06 | 雅宝公司 | 低酸度的1-溴丙烷 |
| EP2205543B1 (en) | 2007-09-25 | 2013-03-06 | Albemarle Corporation | Methods of removing impurities from alkyl bromides during distillation and distillate produced thereby |
| CN102911005A (zh) * | 2012-11-12 | 2013-02-06 | 天津市风船化学试剂科技有限公司 | 一种超纯度正溴丙烷的提纯方法 |
| CN103604899B (zh) * | 2013-11-13 | 2014-10-22 | 广州广电计量检测股份有限公司 | 皮革、纺织品中溴代正丙烷的检测方法 |
| US9617645B1 (en) * | 2015-04-24 | 2017-04-11 | MicroCor Technologies, Inc. | Anti-corrosion and water-repellent substance and method |
| CN107973692B (zh) * | 2017-11-24 | 2021-03-12 | 天津大学 | 一种溴代烷烃的制备方法 |
Family Cites Families (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS56164125A (en) * | 1980-05-23 | 1981-12-17 | Nippei Toyama Corp | Deoxidizing treating method of chlorinated hydrocarbon solvent |
| JPS62175432A (ja) * | 1986-01-29 | 1987-08-01 | Daicel Chem Ind Ltd | ハロゲン含有化合物用安定化剤又は腐蝕防止剤 |
| JPH0867643A (ja) * | 1994-08-30 | 1996-03-12 | Toagosei Co Ltd | 安定化されたブロモプロパン組成物 |
| US5858953A (en) * | 1995-04-12 | 1999-01-12 | Tosoh Corporation | Stabilized 1-bromopropane composition |
| JP2956578B2 (ja) * | 1995-04-12 | 1999-10-04 | 東ソー株式会社 | 安定化された１−ブロモプロパン組成物 |
| JP3582404B2 (ja) * | 1995-04-12 | 2004-10-27 | 東ソー株式会社 | 安定化された１−ブロモプロパン組成物 |
| JPH11343499A (ja) * | 1995-04-12 | 1999-12-14 | Tosoh Corp | 安定化された１―ブロモプロパン組成物 |
| WO1998050517A1 (en) * | 1997-05-02 | 1998-11-12 | Advanced Chemical Design | Environmentally-safe solvent compositions utilizing 1-bromopropane that are stabilized, non-flammable, and have desired solvency characteristics |
| AU2001292649A1 (en) * | 2000-09-13 | 2002-03-26 | Richard G. Henry | Reduced toxycity 1-bromopropane cleaning agent production process |
| IL146456A0 (en) * | 2001-11-12 | 2002-07-25 | Bromine Compounds Ltd | Method for the preparation of n-propyl bromide |
-
2006
- 2006-05-01 EP EP06758865A patent/EP1883615A2/en not_active Withdrawn
- 2006-05-01 WO PCT/US2006/016668 patent/WO2006119212A2/en not_active Ceased
- 2006-05-01 JP JP2008510104A patent/JP5055267B2/ja not_active Expired - Fee Related
- 2006-05-01 CN CN2006800150657A patent/CN101171218B/zh not_active Expired - Fee Related
- 2006-05-01 US US11/912,465 patent/US20080177116A1/en not_active Abandoned
- 2006-05-02 TW TW095115526A patent/TW200712040A/zh unknown
- 2006-05-02 AR ARP060101762A patent/AR057284A1/es not_active Application Discontinuation
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