JP2004531632A5 - - Google Patents

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Publication number
JP2004531632A5
JP2004531632A5 JP2003509001A JP2003509001A JP2004531632A5 JP 2004531632 A5 JP2004531632 A5 JP 2004531632A5 JP 2003509001 A JP2003509001 A JP 2003509001A JP 2003509001 A JP2003509001 A JP 2003509001A JP 2004531632 A5 JP2004531632 A5 JP 2004531632A5
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JP
Japan
Prior art keywords
coc
preparing
emulsifier
anion
fluoropolymer
Prior art date
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JP2003509001A
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English (en)
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JP4080998B2 (ja
JP2004531632A (ja
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Priority claimed from US09/896,319 external-priority patent/US6545109B2/en
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Publication of JP2004531632A publication Critical patent/JP2004531632A/ja
Publication of JP2004531632A5 publication Critical patent/JP2004531632A5/ja
Application granted granted Critical
Publication of JP4080998B2 publication Critical patent/JP4080998B2/ja
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

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Claims (5)

  1. 水性相中でフリーラジカル条件下、少なくとも１種の乳化剤および少なくとも１種の開始剤の存在下で少なくとも１種のフルオロモノマーを乳化重合することを含む、フルオロポリマーの調製方法であって、前記乳化剤が、
    （ａ）以下の式：
    Figure 2004531632
     ［式中、各Ｑが独立してＣＯまたはＳＯ2であり、各Ｒfが独立して過フッ素化アルキル基である］の少なくとも１種のアニオン、および
    （ｂ）非妨害性カチオン、を含む方法。
  2. 前記アニオンがビス（ペルフルオロブタンスルホニル）イミドである、請求項１に記載のフルオロポリマーの調製方法。
  3. 前記アニオンが、
    Figure 2004531632
     並びにそれらの混合物、からなる群から選択される、請求項１に記載のフルオロポリマーの調製方法。
  4. 前記カチオンが、Ｈ+、ＮＨ4 +、Ｈ3Ｏ+、Ｌｉ+、Ｋ+、Ｎａ+、Ｃａ2+、またはＭｇ2+である、請求項１に記載のフルオロポリマーの調製方法。
  5. 前記乳化剤が、ＮＨ4 +-Ｎ（ＳＯ2Ｃ4Ｆ9）2、ＮＨ4 +-Ｎ（ＳＯ2Ｃ4Ｆ9）（ＣＯＣ4Ｆ9）、ＮＨ4 +-Ｎ（ＣＯＣ4Ｆ9）2、ＮＨ4 +-Ｎ（ＳＯ2Ｃ2Ｆ5）2、ＮＨ4 +-Ｎ（ＳＯ2Ｃ4Ｆ9）（ＣＯＣ3Ｆ7）、ＮＨ4 +-Ｎ（ＣＯＣ3Ｆ7）2、ＮＨ4 + -Ｎ（ＳＯ2ＣＦ3）（ＳＯ2Ｃ4Ｆ9）、ＮＨ4 +-Ｎ（ＣＯＣ5Ｈ11）（ＳＯ2Ｃ4Ｆ9）、Ｌｉ+-Ｎ（ＳＯ2Ｃ4Ｆ9）2、Ｃａ2+［-Ｎ（ＳＯ2Ｃ4Ｆ9）（ＣＯＣ4Ｆ9）］2、Ｃａ2+［-Ｎ（ＣＯＣ4Ｆ9）2］2、Ｈ3Ｏ+-Ｎ（ＳＯ2Ｃ4Ｆ9）2、またはそれらの混合物である、請求項１に記載のフルオロポリマーの調製方法。
JP2003509001A 2001-06-29 2002-04-02 フルオロオレフィンの重合のための乳化剤としてのイミド塩 Expired - Fee Related JP4080998B2 (ja)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US09/896,319 US6545109B2 (en) 2001-06-29 2001-06-29 Imide salts as emulsifiers for the polymerization of fluoroolefins
PCT/US2002/010291 WO2003002622A1 (en) 2001-06-29 2002-04-02 Imide salts as emulsifiers for the polymerization of fluoroolefins

Publications (3)

Publication Number Publication Date
JP2004531632A JP2004531632A (ja) 2004-10-14
JP2004531632A5 true JP2004531632A5 (ja) 2005-12-22
JP4080998B2 JP4080998B2 (ja) 2008-04-23

Family

ID=25406004

Family Applications (1)

Application Number Title Priority Date Filing Date
JP2003509001A Expired - Fee Related JP4080998B2 (ja) 2001-06-29 2002-04-02 フルオロオレフィンの重合のための乳化剤としてのイミド塩

Country Status (6)

Country Link
US (1) US6545109B2 (ja)
EP (1) EP1406936B1 (ja)
JP (1) JP4080998B2 (ja)
AT (1) ATE330977T1 (ja)
DE (1) DE60212635T2 (ja)
WO (1) WO2003002622A1 (ja)

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US6555510B2 (en) * 2001-05-10 2003-04-29 3M Innovative Properties Company Bis(perfluoroalkanesulfonyl)imides and their salts as surfactants/additives for applications having extreme environments and methods therefor
US7303852B2 (en) * 2001-12-27 2007-12-04 Shin-Etsu Chemical Co., Ltd. Photoacid generating compounds, chemically amplified positive resist materials, and pattern forming method
JP4493393B2 (ja) * 2004-04-23 2010-06-30 東京応化工業株式会社 リソグラフィー用リンス液
JP2008144206A (ja) * 2006-12-07 2008-06-26 Kobe Steel Ltd チタンまたはチタン合金用酸洗液、およびこれを用いた酸洗方法
US20100113691A1 (en) * 2008-11-06 2010-05-06 E. I. Du Pont De Nemours And Company Fluoro olefin polymerization
EP2284200A1 (en) * 2009-07-31 2011-02-16 3M Innovative Properties Company Aqueous fluoropolymer dispersions containing a polyol comprising at least one long chain residue and method for producing them
US9969899B2 (en) 2013-02-18 2018-05-15 Honeywell International Inc. Fluoropolymers containing a copolymerized fluoromonomer and a functional hydrocarbon comonomer and articles made from such fluoropolymers
WO2019044476A1 (ja) * 2017-09-01 2019-03-07 三菱マテリアル電子化成株式会社 含フッ素ビススルホニルイミド化合物及び界面活性剤
US11827774B2 (en) 2017-12-18 2023-11-28 Borealis Ag Polymer blend composition for wire and cable applications with advantageous electrical properties
US11506581B2 (en) 2018-03-20 2022-11-22 Agilent Technologies, Inc. Mass spectrometry compatible salt formation for ionic liquid sample preparation
WO2020084854A1 (ja) 2018-10-24 2020-04-30 三菱マテリアル電子化成株式会社 含フッ素イミド塩化合物及び界面活性剤

Family Cites Families (19)

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Publication number Priority date Publication date Assignee Title
US2701814A (en) 1955-02-08 Fluorocarbon compounds
DE3024450A1 (de) 1980-06-28 1982-01-28 Hoechst Ag, 6000 Frankfurt Verfahren zur herstellung von waessrigen, kolloidalen dispersionen von copolymerisaten des typs tetrafluorethylen-ethylen
US4558142A (en) 1981-03-11 1985-12-10 Hoffmann-La Roche Inc. 7-Fluoro-prostacyclin analogs
FR2527602A1 (fr) 1982-06-01 1983-12-02 Anvar Bis perhalogenoacyl- ou sulfonyl- imidures de metaux alcalins, leurs solutions solides avec des matieres plastiques et leur application a la constitution d'elements conducteurs pour des generateurs electrochimiques
US4529781A (en) 1984-02-13 1985-07-16 E. I. Du Pont De Nemours And Company Process for the suspension polymerization of tetrafluoroethylene
US4555556A (en) 1985-03-12 1985-11-26 E. I. Du Pont De Nemours And Company Tertiary perfluorinated compounds as rate enhancing additives in PTFE dispersion polymerization
FR2606217B1 (fr) 1986-10-30 1990-12-14 Elf Aquitaine Nouveau materiau a conduction ionique constitue par un sel en solution dans un electrolyte liquide
US5256821A (en) 1988-10-05 1993-10-26 Societe Nationale Elf Aquitaine Method of synthesis of sulphonylimides
FR2645533B1 (fr) 1989-04-06 1991-07-12 Centre Nat Rech Scient Procede de synthese de sulfonylimidures
US5285002A (en) 1993-03-23 1994-02-08 Minnesota Mining And Manufacturing Company Fluorine-containing polymers and preparation and use thereof
US5318674A (en) 1993-06-30 1994-06-07 Minnesota Mining And Manufacturing Company Process for preparing perfluoroalkanesulfonyl fluorides
JP3117369B2 (ja) 1994-09-12 2000-12-11 セントラル硝子株式会社 スルホンイミドの製造方法
US5874616A (en) 1995-03-06 1999-02-23 Minnesota Mining And Manufacturing Company Preparation of bis (fluoroalkylenesulfonyl) imides and (fluoroalkysulfony) (fluorosulfonyl) imides
US5688884A (en) 1995-08-31 1997-11-18 E. I. Du Pont De Nemours And Company Polymerization process
US6080487A (en) 1996-08-26 2000-06-27 3M Innovative Properties Company Method of improving adhesion between a fluoropolymer and a substrate
CA2187046A1 (fr) 1996-10-03 1998-04-03 Alain Vallee Sulfonylimidures et sulfonylmethylures, leur utilisation comme photoinitiateur
US6013795A (en) 1996-11-04 2000-01-11 3M Innovative Properties Company Alpha-branched fluoroalkylcarbonyl fluorides and their derivatives
DE69721748T2 (de) 1996-12-30 2004-03-11 Hydro-Québec, Montréal Oberflächenmodifizierte kohlenstoffmaterialien
JP2001526451A (ja) * 1997-12-10 2001-12-18 ミネソタ マイニング アンド マニュファクチャリング カンパニー 電気化学系中のビス（ペルフルオロアルキルスルホニル）イミド界面活性剤塩

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