JP2004026660A5 - - Google Patents
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- Publication number
- JP2004026660A5 JP2004026660A5 JP2002180859A JP2002180859A JP2004026660A5 JP 2004026660 A5 JP2004026660 A5 JP 2004026660A5 JP 2002180859 A JP2002180859 A JP 2002180859A JP 2002180859 A JP2002180859 A JP 2002180859A JP 2004026660 A5 JP2004026660 A5 JP 2004026660A5
- Authority
- JP
- Japan
- Prior art keywords
- mol
- hour
- reaction solution
- triethylamine
- addition
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 6
- ZMANZCXQSJIPKH-UHFFFAOYSA-N Triethylamine Chemical compound CCN(CC)CC ZMANZCXQSJIPKH-UHFFFAOYSA-N 0.000 description 6
- KQIADDMXRMTWHZ-UHFFFAOYSA-N chloro-tri(propan-2-yl)silane Chemical compound CC(C)[Si](Cl)(C(C)C)C(C)C KQIADDMXRMTWHZ-UHFFFAOYSA-N 0.000 description 4
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonia chloride Chemical compound [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 description 2
- NLZUEZXRPGMBCV-UHFFFAOYSA-N Butylhydroxytoluene Chemical compound CC1=CC(C(C)(C)C)=C(O)C(C(C)(C)C)=C1 NLZUEZXRPGMBCV-UHFFFAOYSA-N 0.000 description 2
- 238000009835 boiling Methods 0.000 description 2
- 238000010992 reflux Methods 0.000 description 2
- PQSIXYSSKXAOFE-UHFFFAOYSA-N tri(propan-2-yl)silyl prop-2-enoate Chemical compound CC(C)[Si](C(C)C)(C(C)C)OC(=O)C=C PQSIXYSSKXAOFE-UHFFFAOYSA-N 0.000 description 2
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 description 1
- NIXOWILDQLNWCW-UHFFFAOYSA-N 2-Propenoic acid Natural products OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 1
- CERQOIWHTDAKMF-UHFFFAOYSA-N Methacrylic acid Chemical compound CC(=C)C(O)=O CERQOIWHTDAKMF-UHFFFAOYSA-N 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- 235000019270 ammonium chloride Nutrition 0.000 description 1
- 235000010354 butylated hydroxytoluene Nutrition 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- DOIRQSBPFJWKBE-UHFFFAOYSA-N phthalic acid di-n-butyl ester Natural products CCCCOC(=O)C1=CC=CC=C1C(=O)OCCCC DOIRQSBPFJWKBE-UHFFFAOYSA-N 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- KNNOZYMZRGTZQM-UHFFFAOYSA-N tri(propan-2-yl)silyl 2-methylprop-2-enoate Chemical compound CC(C)[Si](C(C)C)(C(C)C)OC(=O)C(C)=C KNNOZYMZRGTZQM-UHFFFAOYSA-N 0.000 description 1
- ILWRPSCZWQJDMK-UHFFFAOYSA-N triethylazanium;chloride Chemical compound Cl.CCN(CC)CC ILWRPSCZWQJDMK-UHFFFAOYSA-N 0.000 description 1
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2002180859A JP4178369B2 (ja) | 2002-06-21 | 2002-06-21 | シリル（メタ）アクリレート化合物の製造方法 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2002180859A JP4178369B2 (ja) | 2002-06-21 | 2002-06-21 | シリル（メタ）アクリレート化合物の製造方法 |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| JP2004026660A JP2004026660A (ja) | 2004-01-29 |
| JP2004026660A5 true JP2004026660A5 (enExample) | 2005-05-26 |
| JP4178369B2 JP4178369B2 (ja) | 2008-11-12 |
Family
ID=31177847
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2002180859A Expired - Fee Related JP4178369B2 (ja) | 2002-06-21 | 2002-06-21 | シリル（メタ）アクリレート化合物の製造方法 |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JP4178369B2 (enExample) |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2009139476A1 (ja) * | 2008-05-16 | 2009-11-19 | 旭硝子株式会社 | 重合性化合物、光硬化性組成物、光学素子および光ヘッド装置 |
| DE102008054740A1 (de) * | 2008-12-16 | 2010-06-17 | Basf Se | Verfahren zur Silylierung von Monocarbonsäuren |
| DE102010002358A1 (de) * | 2010-02-25 | 2011-08-25 | Evonik Degussa GmbH, 45128 | Carboxyfunktionalisierte Silicium enthaltende Vorläuferverbindung verschiedener organischer Carbonsäuren |
| EP2935288B1 (en) * | 2012-12-19 | 2016-10-19 | Jotun A/S | Silyl ester copolymer |
| CN103709190A (zh) * | 2014-01-08 | 2014-04-09 | 浙江胡涂硅有限公司 | 一种三异丙基硅基丙烯酸酯的制备方法 |
-
2002
- 2002-06-21 JP JP2002180859A patent/JP4178369B2/ja not_active Expired - Fee Related
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