JP2002522567A5 - - Google Patents
Download PDFInfo
- Publication number
- JP2002522567A5 JP2002522567A5 JP2000563392A JP2000563392A JP2002522567A5 JP 2002522567 A5 JP2002522567 A5 JP 2002522567A5 JP 2000563392 A JP2000563392 A JP 2000563392A JP 2000563392 A JP2000563392 A JP 2000563392A JP 2002522567 A5 JP2002522567 A5 JP 2002522567A5
- Authority
- JP
- Japan
- Prior art keywords
- catalyst
- dmc
- polyether polyol
- metal cyanide
- glycidyl ether
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000003054 catalyst Substances 0.000 description 29
- 229910052751 metal Inorganic materials 0.000 description 13
- 239000002184 metal Substances 0.000 description 13
- 229920000570 polyether Polymers 0.000 description 13
- GYZLOYUZLJXAJU-UHFFFAOYSA-N diglycidyl ether Chemical compound C1OC1COCC1CO1 GYZLOYUZLJXAJU-UHFFFAOYSA-N 0.000 description 12
- 239000004721 Polyphenylene oxide Substances 0.000 description 11
- 229920005862 polyol Polymers 0.000 description 11
- 150000003077 polyols Chemical class 0.000 description 11
- 239000003446 ligand Substances 0.000 description 9
- 150000003839 salts Chemical class 0.000 description 7
- 239000007864 aqueous solution Substances 0.000 description 5
- 238000004519 manufacturing process Methods 0.000 description 5
- 150000002825 nitriles Chemical class 0.000 description 5
- KBPLFHHGFOOTCA-UHFFFAOYSA-N 1-Octanol Chemical compound CCCCCCCCO KBPLFHHGFOOTCA-UHFFFAOYSA-N 0.000 description 4
- XTHFKEDIFFGKHM-UHFFFAOYSA-N Dimethoxyethane Chemical compound COCCOC XTHFKEDIFFGKHM-UHFFFAOYSA-N 0.000 description 4
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 description 4
- 125000002947 alkylene group Chemical group 0.000 description 4
- WERYXYBDKMZEQL-UHFFFAOYSA-N butane-1,4-diol Chemical compound OCCCCO WERYXYBDKMZEQL-UHFFFAOYSA-N 0.000 description 4
- MWKFXSUHUHTGQN-UHFFFAOYSA-N decan-1-ol Chemical compound CCCCCCCCCCO MWKFXSUHUHTGQN-UHFFFAOYSA-N 0.000 description 4
- LQZZUXJYWNFBMV-UHFFFAOYSA-N dodecan-1-ol Chemical compound CCCCCCCCCCCCO LQZZUXJYWNFBMV-UHFFFAOYSA-N 0.000 description 4
- ZSIAUFGUXNUGDI-UHFFFAOYSA-N hexan-1-ol Chemical compound CCCCCCO ZSIAUFGUXNUGDI-UHFFFAOYSA-N 0.000 description 4
- 125000004435 hydrogen atom Chemical group [H]* 0.000 description 4
- 229920002635 polyurethane Polymers 0.000 description 4
- 239000004814 polyurethane Substances 0.000 description 4
- 239000007858 starting material Substances 0.000 description 4
- HLZKNKRTKFSKGZ-UHFFFAOYSA-N tetradecan-1-ol Chemical compound CCCCCCCCCCCCCCO HLZKNKRTKFSKGZ-UHFFFAOYSA-N 0.000 description 4
- XFXPMWWXUTWYJX-UHFFFAOYSA-N Cyanide Chemical compound N#[C-] XFXPMWWXUTWYJX-UHFFFAOYSA-N 0.000 description 3
- -1 alcohols Glycidyl ethers Chemical class 0.000 description 3
- 238000000034 method Methods 0.000 description 3
- 238000002360 preparation method Methods 0.000 description 3
- 238000005406 washing Methods 0.000 description 3
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 2
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 description 2
- 239000002202 Polyethylene glycol Substances 0.000 description 2
- DKGAVHZHDRPRBM-UHFFFAOYSA-N Tert-Butanol Chemical compound CC(C)(C)O DKGAVHZHDRPRBM-UHFFFAOYSA-N 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- 229920001223 polyethylene glycol Polymers 0.000 description 2
- 229920001451 polypropylene glycol Polymers 0.000 description 2
- 239000011701 zinc Substances 0.000 description 2
- JIAARYAFYJHUJI-UHFFFAOYSA-L zinc dichloride Chemical compound [Cl-].[Cl-].[Zn+2] JIAARYAFYJHUJI-UHFFFAOYSA-L 0.000 description 2
- DNIAPMSPPWPWGF-VKHMYHEASA-N (+)-propylene glycol Chemical compound C[C@H](O)CO DNIAPMSPPWPWGF-VKHMYHEASA-N 0.000 description 1
- DNIAPMSPPWPWGF-GSVOUGTGSA-N (R)-(-)-Propylene glycol Chemical compound C[C@@H](O)CO DNIAPMSPPWPWGF-GSVOUGTGSA-N 0.000 description 1
- YPFDHNVEDLHUCE-UHFFFAOYSA-N 1,3-propanediol Substances OCCCO YPFDHNVEDLHUCE-UHFFFAOYSA-N 0.000 description 1
- FBPFZTCFMRRESA-FSIIMWSLSA-N D-Glucitol Natural products OC[C@H](O)[C@H](O)[C@@H](O)[C@H](O)CO FBPFZTCFMRRESA-FSIIMWSLSA-N 0.000 description 1
- FBPFZTCFMRRESA-JGWLITMVSA-N D-glucitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-JGWLITMVSA-N 0.000 description 1
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 description 1
- ZJCCRDAZUWHFQH-UHFFFAOYSA-N Trimethylolpropane Chemical compound CCC(CO)(CO)CO ZJCCRDAZUWHFQH-UHFFFAOYSA-N 0.000 description 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 125000001931 aliphatic group Chemical group 0.000 description 1
- 229910052783 alkali metal Inorganic materials 0.000 description 1
- 150000008044 alkali metal hydroxides Chemical class 0.000 description 1
- 150000001340 alkali metals Chemical class 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- BMRWNKZVCUKKSR-UHFFFAOYSA-N butane-1,2-diol Chemical compound CCC(O)CO BMRWNKZVCUKKSR-UHFFFAOYSA-N 0.000 description 1
- SZAVHWMCBDFDCM-KTTJZPQESA-N cobalt-60(3+);hexacyanide Chemical compound [60Co+3].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-] SZAVHWMCBDFDCM-KTTJZPQESA-N 0.000 description 1
- RKBAPHPQTADBIK-UHFFFAOYSA-N cobalt;hexacyanide Chemical compound [Co].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-].N#[C-] RKBAPHPQTADBIK-UHFFFAOYSA-N 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 229920001971 elastomer Polymers 0.000 description 1
- 239000000806 elastomer Substances 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 239000006260 foam Substances 0.000 description 1
- 235000011187 glycerol Nutrition 0.000 description 1
- XXMIOPMDWAUFGU-UHFFFAOYSA-N hexane-1,6-diol Chemical compound OCCCCCCO XXMIOPMDWAUFGU-UHFFFAOYSA-N 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 239000000178 monomer Substances 0.000 description 1
- SLCVBVWXLSEKPL-UHFFFAOYSA-N neopentyl glycol Chemical compound OCC(C)(C)CO SLCVBVWXLSEKPL-UHFFFAOYSA-N 0.000 description 1
- 239000003973 paint Substances 0.000 description 1
- WXZMFSXDPGVJKK-UHFFFAOYSA-N pentaerythritol Chemical compound OCC(CO)(CO)CO WXZMFSXDPGVJKK-UHFFFAOYSA-N 0.000 description 1
- 238000006116 polymerization reaction Methods 0.000 description 1
- 229920000166 polytrimethylene carbonate Polymers 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 239000000600 sorbitol Substances 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- QXJQHYBHAIHNGG-UHFFFAOYSA-N trimethylolethane Chemical compound OCC(C)(CO)CO QXJQHYBHAIHNGG-UHFFFAOYSA-N 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
- 229910052725 zinc Inorganic materials 0.000 description 1
- 235000005074 zinc chloride Nutrition 0.000 description 1
- 239000011592 zinc chloride Substances 0.000 description 1
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19834573.9 | 1998-07-31 | ||
| DE19834573A DE19834573A1 (de) | 1998-07-31 | 1998-07-31 | Doppelmetallcyanid-Katalysatoren für die Herstellung von Polyetherpolyolen |
| PCT/EP1999/005150 WO2000007721A1 (de) | 1998-07-31 | 1999-07-20 | Doppelmetallcyanid-katalysatoren für die herstellung von polyetherpolyolen |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JP2002522567A JP2002522567A (ja) | 2002-07-23 |
| JP2002522567A5 true JP2002522567A5 (enExample) | 2006-09-21 |
Family
ID=7875995
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP2000563392A Pending JP2002522567A (ja) | 1998-07-31 | 1999-07-20 | ポリエーテルポリオールを製造するための複金属シアン化物触媒 |
Country Status (16)
| Country | Link |
|---|---|
| US (1) | US6878661B1 (enExample) |
| EP (1) | EP1115488B1 (enExample) |
| JP (1) | JP2002522567A (enExample) |
| KR (1) | KR100589580B1 (enExample) |
| CN (1) | CN1129477C (enExample) |
| AT (1) | ATE266469T1 (enExample) |
| AU (1) | AU5411899A (enExample) |
| BR (1) | BR9912604A (enExample) |
| CA (1) | CA2338657A1 (enExample) |
| DE (2) | DE19834573A1 (enExample) |
| ES (1) | ES2219048T3 (enExample) |
| HK (1) | HK1039912B (enExample) |
| HU (1) | HUP0102708A3 (enExample) |
| ID (1) | ID28851A (enExample) |
| PT (1) | PT1115488E (enExample) |
| WO (1) | WO2000007721A1 (enExample) |
Families Citing this family (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2001083107A2 (en) | 2000-04-28 | 2001-11-08 | Synuthane International, Inc. | Double metal cyanide catalysts containing polyglycol ether complexing agents |
| EP1366814A4 (en) * | 2001-03-09 | 2005-03-30 | Wako Pure Chem Ind Ltd | OSMIUM OXIDE REMOVED FROM HYDROPHILIC POLYMER SUPPORT |
| CN1304459C (zh) * | 2002-04-29 | 2007-03-14 | 中国石化集团金陵石油化工有限责任公司 | 一种含硅碳链聚合物的双金属氰化物络合催化剂 |
| CN1867609A (zh) * | 2003-03-07 | 2006-11-22 | 陶氏环球技术公司 | 制备聚醚多元醇的连续方法和设备 |
| CN1294178C (zh) * | 2003-07-09 | 2007-01-10 | 中国石油化工股份有限公司 | 低不饱和度聚醚多元醇的制备方法 |
| WO2007016284A2 (en) * | 2005-07-28 | 2007-02-08 | Shire Llc | Pharmaceutical formulations/composition of guanfacine suitable for single dose form adminstration daily |
| SG11201402998PA (en) | 2011-12-20 | 2014-10-30 | Bayer Ip Gmbh | Hydroxy-aminopolymers and method for producing same |
| EP3106221A1 (en) * | 2015-06-15 | 2016-12-21 | Universität Hamburg | Process for preparing double metal cyanide catalysts and their use in polymerization reactions |
| JP7146810B2 (ja) * | 2017-05-10 | 2022-10-04 | ダウ グローバル テクノロジーズ エルエルシー | 触媒錯体 |
| EP3608018A1 (de) * | 2018-08-08 | 2020-02-12 | Covestro Deutschland AG | Verfahren zur herstellung von doppelmetallcyanid-katalysatoren |
Family Cites Families (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1063525A (en) | 1963-02-14 | 1967-03-30 | Gen Tire & Rubber Co | Organic cyclic oxide polymers, their preparation and tires prepared therefrom |
| US3829505A (en) | 1970-02-24 | 1974-08-13 | Gen Tire & Rubber Co | Polyethers and method for making the same |
| US3941849A (en) | 1972-07-07 | 1976-03-02 | The General Tire & Rubber Company | Polyethers and method for making the same |
| JP2653236B2 (ja) | 1990-10-05 | 1997-09-17 | 旭硝子株式会社 | ポリエーテル化合物の製造方法 |
| US5158922A (en) | 1992-02-04 | 1992-10-27 | Arco Chemical Technology, L.P. | Process for preparing metal cyanide complex catalyst |
| US5470813A (en) | 1993-11-23 | 1995-11-28 | Arco Chemical Technology, L.P. | Double metal cyanide complex catalysts |
| US5712216A (en) | 1995-05-15 | 1998-01-27 | Arco Chemical Technology, L.P. | Highly active double metal cyanide complex catalysts |
| US5482908A (en) | 1994-09-08 | 1996-01-09 | Arco Chemical Technology, L.P. | Highly active double metal cyanide catalysts |
| US5545601A (en) | 1995-08-22 | 1996-08-13 | Arco Chemical Technology, L.P. | Polyether-containing double metal cyanide catalysts |
| US5627120A (en) * | 1996-04-19 | 1997-05-06 | Arco Chemical Technology, L.P. | Highly active double metal cyanide catalysts |
| US5856369A (en) * | 1996-07-30 | 1999-01-05 | Osi Specialties, Inc. | Polyethers and polysiloxane copolymers manufactured with double metal cyanide catalysts |
| US5714428A (en) | 1996-10-16 | 1998-02-03 | Arco Chemical Technology, L.P. | Double metal cyanide catalysts containing functionalized polymers |
| EP1034035B1 (de) * | 1997-10-13 | 2003-06-04 | Bayer Ag | Kristalline doppelmetallcyanid-katalysatoren für die herstellung von polyetherpolyolen |
| US6696383B1 (en) * | 2002-09-20 | 2004-02-24 | Bayer Polymers Llc | Double-metal cyanide catalysts which can be used to prepare polyols and the processes related thereto |
-
1998
- 1998-07-31 DE DE19834573A patent/DE19834573A1/de not_active Withdrawn
-
1999
- 1999-07-20 CN CN99809235A patent/CN1129477C/zh not_active Expired - Fee Related
- 1999-07-20 US US09/744,357 patent/US6878661B1/en not_active Expired - Fee Related
- 1999-07-20 ID IDW20010236A patent/ID28851A/id unknown
- 1999-07-20 CA CA002338657A patent/CA2338657A1/en not_active Abandoned
- 1999-07-20 BR BR9912604-4A patent/BR9912604A/pt not_active Application Discontinuation
- 1999-07-20 WO PCT/EP1999/005150 patent/WO2000007721A1/de not_active Ceased
- 1999-07-20 AT AT99940024T patent/ATE266469T1/de not_active IP Right Cessation
- 1999-07-20 EP EP99940024A patent/EP1115488B1/de not_active Expired - Lifetime
- 1999-07-20 AU AU54118/99A patent/AU5411899A/en not_active Abandoned
- 1999-07-20 HK HK02101527.8A patent/HK1039912B/zh not_active IP Right Cessation
- 1999-07-20 ES ES99940024T patent/ES2219048T3/es not_active Expired - Lifetime
- 1999-07-20 HU HU0102708A patent/HUP0102708A3/hu unknown
- 1999-07-20 PT PT99940024T patent/PT1115488E/pt unknown
- 1999-07-20 DE DE59909487T patent/DE59909487D1/de not_active Expired - Fee Related
- 1999-07-20 JP JP2000563392A patent/JP2002522567A/ja active Pending
- 1999-07-20 KR KR1020017001262A patent/KR100589580B1/ko not_active Expired - Fee Related
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| ES2257302T3 (es) | Polimerizacion de oxido de etileno utilizando catalizadores de cianuro metalico. | |
| ES2201537T3 (es) | Catalizadores cristalinos de cianuros metalicos dobles para la fabricacion de polioles polieter. | |
| ES2243955T3 (es) | Procedimiento de preparacion de polioxialquileno polieter polioles conbajos niveles de metales de transicion, preparados usando un catalizador de cianuro de metal doble. | |
| EP2709757B1 (en) | Process for preparing highly active double metal cyanide catalysts and their use in the synthesis of polyether polyols | |
| JP2002522566A5 (enExample) | ||
| KR100602046B1 (ko) | 폴리에테르 폴리올 제조용의 이중 금속 시아니드 촉매 | |
| ES2275895T3 (es) | Catalizador complejo de metal doble. | |
| ES2199712T3 (es) | Nuevos catalizadores de cianuro bimetalico para la fabricacion de polioleteres. | |
| CZ224598A3 (cs) | Zinko-kovový hexakyanokobaltový katalyzátor pro výrobu polyetherpolyolů, způsob jeho výroby a jeho použití | |
| JP2002506088A (ja) | ポリエーテルポリオールを製造するための改良された複金属シアン化物触媒 | |
| JP2002522567A5 (enExample) | ||
| JP2002522566A (ja) | ポリエーテルポリオールを製造するための複金属シアン化物触媒 | |
| ES2315236T3 (es) | Metodo de humedad incipiente para obtener catalizadores de cianuro que contienen metal. | |
| JP6861145B2 (ja) | 高活性複金属シアン化物触媒、及びその製造方法、並びにその応用 | |
| KR100589580B1 (ko) | 폴리에테르 폴리올의 제조에 사용되는 이중 금속시아나이드 촉매 | |
| US20040249221A1 (en) | Method for producing polyether alcohols | |
| TW568798B (en) | Double metal cyanide catalysts for the preparation of polyether polyols | |
| KR100558232B1 (ko) | 폴리에테르 폴리올 제조용의 이중 금속 시아나이드 촉매 | |
| JP2001519467A5 (enExample) | ||
| JP2003326174A (ja) | ポリエーテルポリオール製造用複金属シアン化物触媒 | |
| KR20040029087A (ko) | 폴리에테르 폴리올의 제조를 위한 이중 금속 시안화물 촉매 | |
| JPH107787A (ja) | 複合金属シアン化物錯体触媒およびその製造方法 | |
| JP2005520891A (ja) | ゼロ原子価金属を用いる金属シアニド触媒の製造方法 | |
| MXPA01001115A (en) | Bimetallic-cyanide catalysts used for preparing polyether polyols | |
| MXPA00003563A (en) | Crystalline double metal cyanide catalysts for producing polyether polyols |