HUP0002297A2 - Eljárás perfluorszulfonamidok, perfluorszulfonimidek és ezek sóinak előállítására, valamint az eljárásban alkalmazott szulfonilező reagensek - Google Patents
Eljárás perfluorszulfonamidok, perfluorszulfonimidek és ezek sóinak előállítására, valamint az eljárásban alkalmazott szulfonilező reagensekInfo
- Publication number
- HUP0002297A2 HUP0002297A2 HU0002297A HUP0002297A HUP0002297A2 HU P0002297 A2 HUP0002297 A2 HU P0002297A2 HU 0002297 A HU0002297 A HU 0002297A HU P0002297 A HUP0002297 A HU P0002297A HU P0002297 A2 HUP0002297 A2 HU P0002297A2
- Authority
- HU
- Hungary
- Prior art keywords
- atom
- perfluorosulphonamides
- sulfonyl
- halide
- perfluorinated
- Prior art date
Links
- 239000003153 chemical reaction reagent Substances 0.000 title abstract 3
- 238000000034 method Methods 0.000 title abstract 3
- USPTVMVRNZEXCP-UHFFFAOYSA-N sulfamoyl fluoride Chemical class NS(F)(=O)=O USPTVMVRNZEXCP-UHFFFAOYSA-N 0.000 title 2
- 230000015572 biosynthetic process Effects 0.000 title 1
- 150000003839 salts Chemical class 0.000 title 1
- 238000003786 synthesis reaction Methods 0.000 title 1
- 125000004429 atom Chemical group 0.000 abstract 2
- 229910052799 carbon Inorganic materials 0.000 abstract 2
- 125000004432 carbon atom Chemical group C* 0.000 abstract 2
- 150000004820 halides Chemical class 0.000 abstract 2
- 229910052757 nitrogen Inorganic materials 0.000 abstract 2
- 125000004433 nitrogen atom Chemical group N* 0.000 abstract 2
- 230000000269 nucleophilic effect Effects 0.000 abstract 2
- 125000000472 sulfonyl group Chemical group *S(*)(=O)=O 0.000 abstract 2
- 229910052717 sulfur Inorganic materials 0.000 abstract 2
- 125000004434 sulfur atom Chemical group 0.000 abstract 2
- 239000012038 nucleophile Substances 0.000 abstract 1
- 239000000758 substrate Substances 0.000 abstract 1
- 150000003461 sulfonyl halides Chemical class 0.000 abstract 1
- YBBRCQOCSYXUOC-UHFFFAOYSA-N sulfuryl dichloride Chemical compound ClS(Cl)(=O)=O YBBRCQOCSYXUOC-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
- C07C303/36—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of amides of sulfonic acids
- C07C303/38—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of amides of sulfonic acids by reaction of ammonia or amines with sulfonic acids, or with esters, anhydrides, or halides thereof
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
Abstract
A találmány perfluorszulfonilezési eljárásra vonatkozik, amelyneksorán egy nukleofilt, amelyben a nukleofil atom egy nitrogénatom,alábbi komponenseket tartalmazó reagenssel hoznak érintkezésbe, amelykomponenseket egymást követően vagy egyidejűleg adagolják: - egyszulfonil halogenid, ahol a halogenid (nagy atomtömegű), előnyösenszulfonil-klorid és - egy szerves bázis, amely ezzel egyidejűleg nemalkilezhető és zsíroldékony, azzal a megkötéssel, hogy amikor anitrogénatom, azaz a szubsztrátum nukleofil atomja már nem hordozkénatommal szomszédos szénatomján perfluorozott szulfonil funkcióscsoportot, akkor a szulfonil-(nagy atomtömegű halogenid)-származékszerves része kénatomhoz kapcsolódó szénatomján perfluorozva van. Atalálmány kiterjed a fenti eljárásban alkalmazott reagensekre. Ó
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR9706064A FR2763331B1 (fr) | 1997-05-16 | 1997-05-16 | Procede de synthese de sulfonimides et de leurs sels |
Publications (2)
Publication Number | Publication Date |
---|---|
HUP0002297A2 true HUP0002297A2 (hu) | 2000-11-28 |
HUP0002297A3 HUP0002297A3 (en) | 2002-09-30 |
Family
ID=9506986
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
HU0002297A HUP0002297A3 (en) | 1997-05-16 | 1998-05-15 | Method for the synthesis of perfluorosulphonamides, perfluorosulphonamides and their salts, and a sulphonation reagent |
Country Status (16)
Country | Link |
---|---|
US (2) | US6297398B1 (hu) |
EP (1) | EP0983216B1 (hu) |
JP (1) | JP4865115B2 (hu) |
CN (1) | CN1264785C (hu) |
AT (1) | ATE334955T1 (hu) |
AU (1) | AU7773398A (hu) |
BR (1) | BR9809837B1 (hu) |
CA (1) | CA2289005C (hu) |
DE (1) | DE69835427T2 (hu) |
EA (1) | EA004498B1 (hu) |
ES (1) | ES2270519T3 (hu) |
FR (1) | FR2763331B1 (hu) |
HU (1) | HUP0002297A3 (hu) |
NO (1) | NO322194B1 (hu) |
WO (1) | WO1998052886A1 (hu) |
ZA (1) | ZA984155B (hu) |
Families Citing this family (23)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US6252111B1 (en) | 1999-02-16 | 2001-06-26 | Central Glass Company, Limited | Method for producing sulfonimide or its salt |
EP1122240A3 (en) * | 2000-01-31 | 2003-11-26 | Morita Chemical Industries Co., Ltd. | Process for producing sulfonylimide compound |
FR2818994B1 (fr) * | 2000-12-29 | 2004-01-09 | Rhodia Chimie Sa | Procede de preparation par voie electrochimique de sels metalliques |
US20030054172A1 (en) | 2001-05-10 | 2003-03-20 | 3M Innovative Properties Company | Polyoxyalkylene ammonium salts and their use as antistatic agents |
US6555510B2 (en) * | 2001-05-10 | 2003-04-29 | 3M Innovative Properties Company | Bis(perfluoroalkanesulfonyl)imides and their salts as surfactants/additives for applications having extreme environments and methods therefor |
US6885025B2 (en) * | 2003-07-10 | 2005-04-26 | Universal Display Corporation | Organic light emitting device structures for obtaining chromaticity stability |
JP2008222659A (ja) * | 2007-03-14 | 2008-09-25 | Asahi Kasei Corp | スルホンアミド化合物の製造方法 |
US20090043016A1 (en) * | 2007-08-06 | 2009-02-12 | Jing-Chung Chang | Flame retardant polytrimethylene terephthalate composition |
US20090043017A1 (en) * | 2007-08-06 | 2009-02-12 | Jing-Chung Chang | Flame retardant polytrimethylene terephthalate composition |
US20090043021A1 (en) * | 2007-08-06 | 2009-02-12 | Jing-Chung Chang | Flame retardant polytrimethylene terephthalate composition |
JP5191267B2 (ja) * | 2008-04-23 | 2013-05-08 | 旭化成株式会社 | スルホンイミド塩の精製方法 |
JP2010083764A (ja) * | 2008-09-29 | 2010-04-15 | Asahi Kasei Corp | 新規スルホンイミド塩の精製方法 |
US8258341B2 (en) * | 2009-07-10 | 2012-09-04 | E.I. Du Pont De Nemours And Company | Polyfluorosulfonamido amine and intermediate |
JP5730513B2 (ja) * | 2009-08-13 | 2015-06-10 | 三菱マテリアル株式会社 | 含フッ素スルホニルイミド化合物の製造方法 |
JP2011037784A (ja) * | 2009-08-13 | 2011-02-24 | Mitsubishi Materials Corp | ペルフルオロアルキルスルホンアミドの製造方法 |
CN102405189B (zh) | 2009-11-27 | 2014-07-09 | 株式会社日本触媒 | 氟磺酰亚胺盐以及氟磺酰亚胺盐的制备方法 |
WO2011149095A1 (ja) * | 2010-05-28 | 2011-12-01 | 株式会社日本触媒 | フルオロスルホニルイミドのアルカリ金属塩およびその製造方法 |
CN102180816B (zh) * | 2011-03-15 | 2013-06-12 | 浙江大学 | 非对称型双氟代磺酰亚胺钾的制备方法 |
CN102617414B (zh) * | 2012-03-02 | 2014-12-17 | 苏州氟特电池材料有限公司 | 含氯磺酰/磷酰亚胺碱金属盐和含氟磺酰/磷酰亚胺碱金属盐的制备方法 |
FR2993556B1 (fr) | 2012-07-23 | 2014-08-15 | Rhodia Operations | Procede de preparation d'un compose sulfonimide et de ses sels |
CN104710639B (zh) * | 2015-03-03 | 2017-12-01 | 上海交通大学 | 一种基于全氟磺酰胺阴离子交换膜的制备方法 |
JP2018039760A (ja) * | 2016-09-08 | 2018-03-15 | 三菱マテリアル電子化成株式会社 | ペルフルオロアルカンスルホンアミドアンモニウムの製造方法 |
CN114470826B (zh) * | 2022-02-17 | 2023-03-14 | 中船(邯郸)派瑞特种气体股份有限公司 | 一种双(三氟甲磺酰)亚胺的纯化装置和方法 |
Family Cites Families (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0149423B1 (de) * | 1983-12-16 | 1987-10-28 | Ciba-Geigy Ag | Verfahren zum Schützen von Keratinmaterial vor dem Befall durch keratinfressende Insekten und neue Phenoxytrifluormethansulfonanilide |
FR2637284B1 (fr) * | 1988-10-05 | 1991-07-05 | Elf Aquitaine | Methode de synthese de sulfonylimidures |
FR2645533B1 (fr) * | 1989-04-06 | 1991-07-12 | Centre Nat Rech Scient | Procede de synthese de sulfonylimidures |
DE4217366A1 (de) * | 1992-05-26 | 1993-12-02 | Bayer Ag | Imide und deren Salze sowie deren Verwendung |
JP3117369B2 (ja) * | 1994-09-12 | 2000-12-11 | セントラル硝子株式会社 | スルホンイミドの製造方法 |
US5874616A (en) * | 1995-03-06 | 1999-02-23 | Minnesota Mining And Manufacturing Company | Preparation of bis (fluoroalkylenesulfonyl) imides and (fluoroalkysulfony) (fluorosulfonyl) imides |
GB9702194D0 (en) * | 1997-02-04 | 1997-03-26 | Lilly Co Eli | Sulphonide derivatives |
-
1997
- 1997-05-16 FR FR9706064A patent/FR2763331B1/fr not_active Expired - Lifetime
-
1998
- 1998-05-15 US US09/423,486 patent/US6297398B1/en not_active Expired - Lifetime
- 1998-05-15 CN CNB988051737A patent/CN1264785C/zh not_active Expired - Lifetime
- 1998-05-15 ES ES98925721T patent/ES2270519T3/es not_active Expired - Lifetime
- 1998-05-15 CA CA002289005A patent/CA2289005C/fr not_active Expired - Lifetime
- 1998-05-15 DE DE69835427T patent/DE69835427T2/de not_active Expired - Lifetime
- 1998-05-15 HU HU0002297A patent/HUP0002297A3/hu unknown
- 1998-05-15 AT AT98925721T patent/ATE334955T1/de not_active IP Right Cessation
- 1998-05-15 JP JP55003598A patent/JP4865115B2/ja not_active Expired - Lifetime
- 1998-05-15 WO PCT/FR1998/000973 patent/WO1998052886A1/fr active IP Right Grant
- 1998-05-15 EP EP98925721A patent/EP0983216B1/fr not_active Expired - Lifetime
- 1998-05-15 EA EA199901039A patent/EA004498B1/ru not_active IP Right Cessation
- 1998-05-15 BR BRPI9809837-3A patent/BR9809837B1/pt not_active IP Right Cessation
- 1998-05-15 AU AU77733/98A patent/AU7773398A/en not_active Abandoned
- 1998-05-18 ZA ZA984155A patent/ZA984155B/xx unknown
-
1999
- 1999-11-15 NO NO19995595A patent/NO322194B1/no not_active IP Right Cessation
-
2001
- 2001-08-07 US US09/923,493 patent/US6399821B2/en not_active Expired - Lifetime
Also Published As
Publication number | Publication date |
---|---|
BR9809837B1 (pt) | 2010-02-09 |
HUP0002297A3 (en) | 2002-09-30 |
JP2001525844A (ja) | 2001-12-11 |
WO1998052886A1 (fr) | 1998-11-26 |
DE69835427D1 (de) | 2006-09-14 |
FR2763331A1 (fr) | 1998-11-20 |
US20020004613A1 (en) | 2002-01-10 |
CA2289005C (fr) | 2007-04-17 |
BR9809837A (pt) | 2000-06-20 |
EA004498B1 (ru) | 2004-04-29 |
NO995595D0 (no) | 1999-11-15 |
EA199901039A1 (ru) | 2000-04-24 |
EP0983216B1 (fr) | 2006-08-02 |
NO995595L (no) | 2000-01-14 |
US6399821B2 (en) | 2002-06-04 |
ATE334955T1 (de) | 2006-08-15 |
CA2289005A1 (fr) | 1998-11-26 |
NO322194B1 (no) | 2006-08-28 |
JP4865115B2 (ja) | 2012-02-01 |
ES2270519T3 (es) | 2007-04-01 |
CN1273573A (zh) | 2000-11-15 |
AU7773398A (en) | 1998-12-11 |
CN1264785C (zh) | 2006-07-19 |
FR2763331B1 (fr) | 1999-06-25 |
DE69835427T2 (de) | 2007-02-01 |
US6297398B1 (en) | 2001-10-02 |
ZA984155B (en) | 1998-12-28 |
EP0983216A1 (fr) | 2000-03-08 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
FD9A | Lapse of provisional protection due to non-payment of fees |