GB1422272A - Compositions containing compounds producing a cooling sensation - Google Patents
Compositions containing compounds producing a cooling sensationInfo
- Publication number
- GB1422272A GB1422272A GB923173A GB923173A GB1422272A GB 1422272 A GB1422272 A GB 1422272A GB 923173 A GB923173 A GB 923173A GB 923173 A GB923173 A GB 923173A GB 1422272 A GB1422272 A GB 1422272A
- Authority
- GB
- United Kingdom
- Prior art keywords
- oil
- menthol
- tobacco
- anethole
- flavouring
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/34—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances containing a carbocyclic ring other than a six-membered aromatic ring
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
- A23L21/00—Marmalades, jams, jellies or the like; Products from apiculture; Preparation or treatment thereof
- A23L21/10—Marmalades; Jams; Jellies; Other similar fruit or vegetable compositions; Simulated fruit products
- A23L21/12—Marmalades; Jams; Jellies; Other similar fruit or vegetable compositions; Simulated fruit products derived from fruit or vegetable solids
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES, NOT OTHERWISE PROVIDED FOR; PREPARATION OR TREATMENT THEREOF
- A23L27/00—Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
- A23L27/20—Synthetic spices, flavouring agents or condiments
- A23L27/203—Alicyclic compounds
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q11/00—Preparations for care of the teeth, of the oral cavity or of dentures; Dentifrices, e.g. toothpastes; Mouth rinses
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/24—Thermal properties
- A61K2800/244—Endothermic; Cooling; Cooling sensation
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- Veterinary Medicine (AREA)
- Public Health (AREA)
- Nutrition Science (AREA)
- Epidemiology (AREA)
- Birds (AREA)
- General Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Toxicology (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Oral & Maxillofacial Surgery (AREA)
- Emergency Medicine (AREA)
- Cosmetics (AREA)
- Dairy Products (AREA)
- Non-Alcoholic Beverages (AREA)
- Jellies, Jams, And Syrups (AREA)
- Manufacture Of Tobacco Products (AREA)
- Seasonings (AREA)
- Medicinal Preparation (AREA)
- Edible Oils And Fats (AREA)
- Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| LU64851 | 1972-02-28 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1422272A true GB1422272A (en) | 1976-01-21 |
Family
ID=19726960
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB923173A Expired GB1422272A (en) | 1972-02-28 | 1973-02-26 | Compositions containing compounds producing a cooling sensation |
Country Status (14)
| Country | Link |
|---|---|
| US (1) | US4029759A (enExample) |
| JP (1) | JPS4898012A (enExample) |
| AT (1) | AT331415B (enExample) |
| AU (1) | AU466320B2 (enExample) |
| BE (1) | BE795751A (enExample) |
| BR (1) | BR7301470D0 (enExample) |
| CA (1) | CA1007108A (enExample) |
| CH (1) | CH578841A5 (enExample) |
| DE (1) | DE2309256A1 (enExample) |
| FR (1) | FR2174104A1 (enExample) |
| GB (1) | GB1422272A (enExample) |
| LU (1) | LU64851A1 (enExample) |
| NL (1) | NL7302675A (enExample) |
| NO (1) | NO137476C (enExample) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB2147492A (en) * | 1983-10-03 | 1985-05-15 | Tobacco Res & Dev | Cigarettes with improved initial impact |
| CN109699758A (zh) * | 2019-02-20 | 2019-05-03 | 山东天博食品配料有限公司 | 一种芹菜精油及其制备方法 |
Families Citing this family (79)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4292028A (en) * | 1979-07-13 | 1981-09-29 | Arthur Barr | Cosmetic breath freshener and palate coolant composition and method of use |
| US4528182A (en) * | 1983-07-13 | 1985-07-09 | Colgate-Palmolive Company | Stable antiplaque dentifrice with improved foaming |
| JP2546226B2 (ja) * | 1984-02-23 | 1996-10-23 | ライオン株式会社 | 安息香酸類配合練歯磨組成物の肌荒れ防止方法 |
| US5009893A (en) * | 1989-07-17 | 1991-04-23 | Warner-Lambert Company | Breath-freshening edible compositions of methol and a carboxamide |
| WO2004091296A1 (ja) * | 1993-10-22 | 2004-10-28 | Takeshi Ikemoto | 有害生物忌避剤 |
| JP2770081B2 (ja) * | 1992-10-29 | 1998-06-25 | 久光製薬株式会社 | シクロヘキサノール誘導体,これを含有する冷感剤および冷感性組成物,並びに該誘導体の製造方法およびその中間体 |
| CN1038670C (zh) * | 1993-11-18 | 1998-06-10 | 久光制药株式会社 | 环己醇衍生物、含有它的冷感剂和冷感性组合物,以及该衍生物的制造方法及其中间体 |
| WO1995034277A1 (en) * | 1994-06-10 | 1995-12-21 | The Procter & Gamble Company | Mouthrinse compositions |
| US5752529A (en) * | 1996-08-21 | 1998-05-19 | V. Mane Fils S.A. | Tobacco products containing coolant compositions |
| US6455080B1 (en) | 1997-12-29 | 2002-09-24 | Wm. Wrigley Jr., Company | Chewing gum containing controlled release acyclic carboxamide and method of making |
| WO1999013734A1 (en) | 1997-09-18 | 1999-03-25 | Wm. Wrigley Jr. Company | Chewing gum containing physiological cooling agents |
| US6627233B1 (en) * | 1997-09-18 | 2003-09-30 | Wm. Wrigley Jr. Company | Chewing gum containing physiological cooling agents |
| US6290940B1 (en) * | 1999-04-16 | 2001-09-18 | Fd Management, Inc. | Breath refreshening lipstick |
| US6383475B1 (en) * | 1999-04-16 | 2002-05-07 | Fd Management, Inc. | Breath freshening lipstick |
| US6780443B1 (en) * | 2000-02-04 | 2004-08-24 | Takasago International Corporation | Sensate composition imparting initial sensation upon contact |
| EP1398306A3 (en) * | 2000-02-04 | 2004-12-15 | Takasago International Corporation | A (1'R, 2'S, 5'R)-3-l-Menthoxyalkan-1-ol cooling sensate |
| JP2001294546A (ja) | 2000-02-28 | 2001-10-23 | Takasago Internatl Corp | (1’R,2’S,5’R)3−l−メントキシアルカン−1−オール冷感剤 |
| US6303817B1 (en) | 2000-08-10 | 2001-10-16 | International Flavors & Fragrances Inc. | Method for making amides |
| US6365215B1 (en) * | 2000-11-09 | 2002-04-02 | International Flavors & Fragrances Inc. | Oral sensory perception-affecting compositions containing dimethyl sulfoxide, complexes thereof and salts thereof |
| PL369924A1 (en) * | 2001-11-23 | 2005-05-02 | Unilever N.V. | Water continuous food product with cooling flavour |
| US20030161802A1 (en) * | 2002-02-05 | 2003-08-28 | Flammer Linda J. | Anti-dandruff and anti-itch compositions containing sensate and sensate enhancer-containing compounds |
| US7361376B2 (en) * | 2003-04-11 | 2008-04-22 | International Flavors & Fragrances Inc. | Alkyldienamides exhibiting taste and sensory effect in flavor compositions |
| US7632531B2 (en) * | 2003-04-11 | 2009-12-15 | International Flavors & Fragnances Inc. | Alkyldienamides exhibiting taste and sensory effect in flavor compositions |
| US6884906B2 (en) * | 2003-07-01 | 2005-04-26 | International Flavors & Fragrances Inc. | Menthyl half acid ester derivatives, processes for preparing same, and uses thereof for their cooling/refreshing effect in consumable materials |
| US7141686B2 (en) * | 2003-07-10 | 2006-11-28 | International Flavors & Fragrances Inc. | E2, E4, Z8-undecatrienoic acid and ester and carboxamide derivatives thereof, organoleptic uses thereof and processes for preparing same |
| US7025997B2 (en) * | 2003-09-24 | 2006-04-11 | International Flavors & Fragrances Inc. | Coolant plant extract compositions containing monomenthyl succinate |
| US8007839B2 (en) * | 2003-10-03 | 2011-08-30 | International Flavors & Fragrances | Conjugated dienamides, methods of production thereof, compositions containing same and uses thereof |
| US7329767B2 (en) * | 2003-10-03 | 2008-02-12 | International Flavors & Fragrances Inc. | Conjugated dienamides, methods of production thereof, compositions containing same and uses thereof |
| CA2556745C (en) * | 2004-02-26 | 2010-04-20 | Wm. Wrigley Jr. Company | Confections containing a blend of physiological cooling agents |
| US7541055B2 (en) * | 2004-09-10 | 2009-06-02 | International Flavors & Fragrances Inc. | Saturated and unsaturated N-alkamides exhibiting taste and flavor enhancement effect in flavor compositions |
| US7427421B2 (en) * | 2004-09-10 | 2008-09-23 | International Flavors & Fragrances Inc. | Saturated and unsaturated N-alkamides exhibiting taste and flavor enhancement effect in flavor compositions |
| AU2005322104A1 (en) * | 2004-12-29 | 2006-07-06 | Wm. Wrigley Jr. Company | Combinations of cooling agents for use in confections |
| ATE484960T1 (de) * | 2005-05-27 | 2010-11-15 | Cadbury Adams Usa Llc | Zusammensetzungen mit vanillegeschmack und abgabesystem dafür |
| US20060280852A1 (en) * | 2005-05-27 | 2006-12-14 | Cadbury Adams Usa Llc. | Vanilla-flavored compositions and delivery systems therefor |
| CN103168899A (zh) | 2005-10-05 | 2013-06-26 | 卡夫食品环球品牌有限责任公司 | 包含薄荷酯的清凉组合物 |
| CN101346073B (zh) | 2005-12-23 | 2013-02-13 | 卡夫食品环球品牌有限责任公司 | 提供基本上类似于由薄荷醇提供的感觉的组合物 |
| WO2007126430A1 (en) | 2005-12-23 | 2007-11-08 | Cadbury Adams Usa Llc | Compositions providing a heating sensation for oral or dermal delivery |
| AU2008225848B2 (en) * | 2007-03-14 | 2011-08-25 | Unilever Plc | Aeratable and aerated products |
| US20090098173A1 (en) * | 2007-10-11 | 2009-04-16 | Robinson Ronni L | Topical pain relief product |
| JP5384641B2 (ja) * | 2008-08-15 | 2014-01-08 | ザ プロクター アンド ギャンブル カンパニー | 消費者製品における感覚剤として有用なシクロヘキサン誘導体の合成 |
| BRPI0917997A2 (pt) * | 2008-08-15 | 2015-11-17 | Procter & Gamble | solução de mentanocarboxamidas para uso em produtos destinados ao consumidor |
| MX2011005374A (es) * | 2008-11-20 | 2011-06-06 | Procter & Gamble | Composiciones para el cuidado personal que proporcionan una sensacion refrescante mejorada. |
| EP2432445A2 (en) * | 2009-05-20 | 2012-03-28 | Givaudan SA | Menthol replacement |
| US9185925B2 (en) | 2009-10-09 | 2015-11-17 | Philip Morris Usa Inc. | Immobilized flavorants for flavor delivery |
| US9937115B2 (en) | 2010-10-01 | 2018-04-10 | The Procter & Gamble Company | Oral care compositions with improved flavor |
| US20130042482A1 (en) | 2011-08-16 | 2013-02-21 | Valerie Jean Bradford | Skin Engaging Member Comprising An Anti-Irritation Agent |
| AU2012302149B2 (en) | 2011-09-01 | 2015-08-13 | The Procter & Gamble Company | Oral care compositions with improved rheology |
| US20130315843A1 (en) | 2012-05-25 | 2013-11-28 | The Procter & Gamble Company | Composition for reduction of trpa1 and trpv1 sensations |
| CN104884129B (zh) | 2012-09-28 | 2017-09-29 | 吉列有限公司 | 包含至少一种热弹性感觉剂的皮肤接合构件 |
| EP2900332B1 (en) | 2012-09-28 | 2017-08-02 | The Gillette Company LLC | A skin engaging shaving aid member comprising at least one thermally resilient sensate |
| US9884130B2 (en) | 2013-11-13 | 2018-02-06 | The Procter & Gamble Company | Compositions for delivery of oral comfort sensations |
| AU2015222884A1 (en) | 2014-02-27 | 2016-08-04 | The Procter & Gamble Company | Oral care compositions with a reduced bitter taste perception |
| US20150272847A1 (en) | 2014-03-26 | 2015-10-01 | The Gillette Company | Skin Engaging Shaving Aid Comprising A Thermally Resilient Sensate And A TRPA1 Receptor Inhibitor |
| US20150273711A1 (en) | 2014-03-26 | 2015-10-01 | The Gillette Company | Razor Comprising A Molded Shaving Aid Composition Comprising A Thermally Resilient Sensate |
| MX2016013618A (es) | 2014-04-23 | 2017-02-28 | Procter & Gamble | Ciclohexanocarboxamida con propiedades de enfriamiento. |
| AU2015301965B2 (en) | 2014-08-15 | 2018-10-04 | The Procter & Gamble Company | Oral care compositions and regimens |
| CA2956964C (en) | 2014-08-15 | 2019-07-16 | The Procter & Gamble Company | Oral care compositions with an enhanced sensory experience |
| RU2017103157A (ru) | 2014-08-15 | 2018-09-18 | Дзе Проктер Энд Гэмбл Компани | Средство ухода за зубами, обеспечивающее поэтапное химическое воздействие |
| AU2015353904B2 (en) | 2014-11-26 | 2018-12-20 | The Gillette Company Llc | A skin engaging member comprising ethylene vinyl acetate |
| US9951295B2 (en) | 2015-02-19 | 2018-04-24 | The Procter & Gamble Company | Compositions for deposition on biological surfaces |
| AR104220A1 (es) | 2015-04-09 | 2017-07-05 | Procter & Gamble | Reducción de la aversión al sabor del cpc mediante la reducción de la activación del cpc de los receptores de trpa1, receptores de trpv1, o ambos |
| CA3000021C (en) | 2015-10-22 | 2020-10-13 | The Procter & Gamble Company | Method of separating stereoisomers using supercritical fluid chromatography |
| CA3000022A1 (en) | 2015-10-22 | 2017-04-27 | The Procter & Gamble Company | Synthesis of cyclohexane carboxamide derivatives useful as sensates in consumer products |
| CN108368035A (zh) | 2015-12-18 | 2018-08-03 | 宝洁公司 | 在消费品中可用作感觉剂的环己烷酯衍生物的合成 |
| WO2017173196A1 (en) | 2016-04-01 | 2017-10-05 | The Procter & Gamble Company | Oral care compositions containing gel networks and potassium nitrate |
| MX2018011990A (es) | 2016-04-01 | 2019-02-13 | Procter & Gamble | Composiciones para el cuidado bucal que contienen nitrato de potasio y peroxido. |
| MX2018011989A (es) | 2016-04-01 | 2019-02-13 | Procter & Gamble | Composiciones para el cuidado bucal que contienen una fase de red de gel. |
| CN108883039A (zh) | 2016-04-01 | 2018-11-23 | 宝洁公司 | 具有有效风味显示的口腔护理组合物 |
| BR112018069874A2 (pt) | 2016-04-01 | 2019-02-05 | Procter & Gamble | composições para tratamento bucal contendo uma fase de rede de gel e nitrato de potássio |
| US20170334082A1 (en) | 2016-05-18 | 2017-11-23 | The Gillette Company Llc | Skin Engaging Member Comprising Ethylene Vinyl Acetate |
| US11198972B2 (en) | 2016-10-25 | 2021-12-14 | The Procter & Gamble Company | Fibrous structures |
| CA3177722A1 (en) | 2016-10-25 | 2018-05-03 | The Procter & Gamble Company | Differential pillow height fibrous structures |
| WO2018085479A1 (en) | 2016-11-03 | 2018-05-11 | The Gillette Company Llc | Skin engaging member comprising ethylene vinyl acetate |
| BR112019009754B1 (pt) | 2016-11-17 | 2022-11-22 | The Gillette Company Llc | Membro de contato com a pele compreendendo etileno-acetato de vinila e uma fragrância |
| ES2944116T3 (es) * | 2017-12-20 | 2023-06-19 | Firmenich & Cie | Composiciones para el cuidado bucal |
| US12049584B2 (en) * | 2019-03-18 | 2024-07-30 | Sabine Zureikat | Composition and method for producing the sensory stimulant |
| EP4216915A1 (en) | 2020-09-28 | 2023-08-02 | The Procter & Gamble Company | Oral care composition comprising hops and flavor |
| AU2022273061B2 (en) | 2021-05-11 | 2025-05-22 | The Procter & Gamble Company | Oral care compositions comprising block copolymer |
| WO2024203570A1 (ja) * | 2023-03-31 | 2024-10-03 | 三菱瓦斯化学株式会社 | 香料組成物及び脂環式アルコール組成物 |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE123909C (enExample) * | ||||
| DD123909A4 (enExample) | 1970-06-29 | 1977-01-26 |
-
0
- BE BE795751D patent/BE795751A/xx unknown
-
1972
- 1972-02-28 LU LU64851A patent/LU64851A1/xx unknown
-
1973
- 1973-02-15 US US05/332,955 patent/US4029759A/en not_active Expired - Lifetime
- 1973-02-22 AU AU52514/73A patent/AU466320B2/en not_active Expired
- 1973-02-24 DE DE19732309256 patent/DE2309256A1/de active Pending
- 1973-02-26 AT AT169273A patent/AT331415B/de not_active IP Right Cessation
- 1973-02-26 GB GB923173A patent/GB1422272A/en not_active Expired
- 1973-02-26 CH CH276273A patent/CH578841A5/xx not_active IP Right Cessation
- 1973-02-27 JP JP48023648A patent/JPS4898012A/ja active Pending
- 1973-02-27 FR FR7306954A patent/FR2174104A1/fr not_active Withdrawn
- 1973-02-27 CA CA165,050A patent/CA1007108A/en not_active Expired
- 1973-02-27 NO NO785/73A patent/NO137476C/no unknown
- 1973-02-27 BR BR731470A patent/BR7301470D0/pt unknown
- 1973-02-27 NL NL7302675A patent/NL7302675A/xx not_active Application Discontinuation
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB2147492A (en) * | 1983-10-03 | 1985-05-15 | Tobacco Res & Dev | Cigarettes with improved initial impact |
| CN109699758A (zh) * | 2019-02-20 | 2019-05-03 | 山东天博食品配料有限公司 | 一种芹菜精油及其制备方法 |
Also Published As
| Publication number | Publication date |
|---|---|
| AT331415B (de) | 1976-08-25 |
| CH578841A5 (enExample) | 1976-08-31 |
| ATA169273A (de) | 1975-11-15 |
| LU64851A1 (enExample) | 1973-09-04 |
| BR7301470D0 (pt) | 1974-08-29 |
| BE795751A (fr) | 1973-08-21 |
| NL7302675A (enExample) | 1973-08-30 |
| CA1007108A (en) | 1977-03-22 |
| NO137476C (no) | 1978-03-08 |
| AU5251473A (en) | 1974-08-22 |
| US4029759A (en) | 1977-06-14 |
| FR2174104A1 (enExample) | 1973-10-12 |
| NO137476B (no) | 1977-11-28 |
| AU466320B2 (en) | 1975-10-23 |
| JPS4898012A (enExample) | 1973-12-13 |
| DE2309256A1 (de) | 1973-09-13 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PS | Patent sealed [section 19, patents act 1949] | ||
| PCNP | Patent ceased through non-payment of renewal fee |