FR2193042A1 - Monomer removal from pvc - using condensed water vapour - Google Patents

Monomer removal from pvc - using condensed water vapour

Info

Publication number
FR2193042A1
FR2193042A1 FR7324646A FR7324646A FR2193042A1 FR 2193042 A1 FR2193042 A1 FR 2193042A1 FR 7324646 A FR7324646 A FR 7324646A FR 7324646 A FR7324646 A FR 7324646A FR 2193042 A1 FR2193042 A1 FR 2193042A1
Authority
FR
France
Prior art keywords
polymer
condensed water
water vapour
pvc
monomer
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
FR7324646A
Other languages
English (en)
Other versions
FR2193042B1 (fr
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Solvay SA
Original Assignee
Solvay SA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Solvay SA filed Critical Solvay SA
Publication of FR2193042A1 publication Critical patent/FR2193042A1/fr
Application granted granted Critical
Publication of FR2193042B1 publication Critical patent/FR2193042B1/fr
Granted legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18—Stationary reactors having moving elements inside
    • B01J19/20—Stationary reactors having moving elements inside in the form of helices, e.g. screw reactors
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/18—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
    • B01J8/24—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles according to "fluidised-bed" technique
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F6/00—Post-polymerisation treatments
    • C08F6/001—Removal of residual monomers by physical means
    • C08F6/005—Removal of residual monomers by physical means from solid polymers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00026—Controlling or regulating the heat exchange system
    • B01J2208/00035—Controlling or regulating the heat exchange system involving measured parameters
    • B01J2208/00044—Temperature measurement
    • B01J2208/00061—Temperature measurement of the reactants
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00026—Controlling or regulating the heat exchange system
    • B01J2208/00035—Controlling or regulating the heat exchange system involving measured parameters
    • B01J2208/0007—Pressure measurement
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00106—Controlling the temperature by indirect heat exchange
    • B01J2208/00168—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles
    • B01J2208/00256—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles in a heat exchanger for the heat exchange medium separate from the reactor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00539—Pressure
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00548—Flow
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00121—Controlling the temperature by direct heating or cooling
    • B01J2219/00128—Controlling the temperature by direct heating or cooling by evaporation of reactants
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/18—Details relating to the spatial orientation of the reactor
    • B01J2219/182—Details relating to the spatial orientation of the reactor horizontal
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/18—Details relating to the spatial orientation of the reactor
    • B01J2219/185—Details relating to the spatial orientation of the reactor vertical
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/19—Details relating to the geometry of the reactor
    • B01J2219/194—Details relating to the geometry of the reactor round
    • B01J2219/1941—Details relating to the geometry of the reactor round circular or disk-shaped
    • B01J2219/1946—Details relating to the geometry of the reactor round circular or disk-shaped conical

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Combustion & Propulsion (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
FR7324646A 1972-07-19 1973-07-03 Monomer removal from pvc - using condensed water vapour Granted FR2193042A1 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
BE120023 1972-07-19
BE125979 1972-12-29

Publications (2)

Publication Number Publication Date
FR2193042A1 true FR2193042A1 (en) 1974-02-15
FR2193042B1 FR2193042B1 (fr) 1976-05-28

Family

ID=25647603

Family Applications (1)

Application Number Title Priority Date Filing Date
FR7324646A Granted FR2193042A1 (en) 1972-07-19 1973-07-03 Monomer removal from pvc - using condensed water vapour

Country Status (5)

Country Link
DE (1) DE2331895C2 (fr)
FI (1) FI57423C (fr)
FR (1) FR2193042A1 (fr)
IT (1) IT989178B (fr)
NL (1) NL172860C (fr)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2291236A1 (fr) * 1974-11-14 1976-06-11 Hoechst Ag Procede de preparation de melanges pulverulents prets au faconnage, a base de polymeres de chlorure de vinyle
DE2641563A1 (de) * 1975-09-15 1977-03-17 Tenneco Chem Verfahren zum herabsetzen des gehaltes an monomerem vinylchlorid in trockenen polyvinylchloridteilchen
FR2372178A1 (fr) * 1976-11-24 1978-06-23 Hoechst Ag Procede pour ameliorer les proprietes des polymeres de chlorure de vinyle
CN111841453A (zh) * 2020-06-18 2020-10-30 西北大学 一种应用于热重分析的微型流化床反应装置

Families Citing this family (29)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2463047C2 (fr) * 1974-06-21 1988-02-04 Hoechst Ag, 6230 Frankfurt, De
DE2429776C3 (de) * 1974-06-21 1981-12-24 Hoechst Ag, 6000 Frankfurt Verfahren zur Entfernung von restlichem Vinylchlorid aus wäßrigen Polyvinylchloriddispersionen
DE2429777B2 (de) * 1974-06-21 1981-04-02 Hoechst Ag, 6000 Frankfurt Verfahren zur Entfernung von nicht ungesetztem, restlichem Vinylchlorid aus wäßrigen Dispersionen von Vinylchloridpolymerisaten
DE2439203B2 (de) * 1974-08-16 1981-07-23 Hoechst Ag, 6000 Frankfurt Verfahren zur Entfernung von nicht umgesetztem, restlichen Vinchlorid aus wäßrigen Dispersionen von Vinylchloridpolymerisaten
US3956249A (en) * 1974-06-24 1976-05-11 Tenneco Chemicals, Inc. Manufacture of polyvinyl chloride of low vinyl chloride monomer content by treatment of wet polyvinyl chloride
IL47420A (en) * 1974-06-24 1978-07-31 Tenneco Chem Process for the removal of vinyl chloride from pvc slurries and latexes and pvc thus obtained
ES438975A1 (es) * 1974-08-14 1977-02-16 Solvay Un procedimiento para la eliminacion del cloruro de vinilo residual procedente de la polimerizacion en los polimeros decloruro de vinilo.
US4104459A (en) * 1974-08-19 1978-08-01 Ethyl Corporation Treating polyvinyl chloride resins
JPS5126988A (ja) * 1974-08-30 1976-03-05 Sumitomo Chemical Co Enkabinirukeijugotaichunizanzonsuru enkabinirutanryotai no jokyohoho
DE2450464A1 (de) * 1974-10-24 1976-04-29 Basf Ag Verfahren zur emissionsarmen entfernung von vinylchlorid aus polymerisaten des vinylchlorids
JPS5169587A (en) * 1974-12-13 1976-06-16 Tetsukosha Kk Jugotaichuno zanzonenkabinirutanryotaijokyohoho
DE2500765C3 (de) * 1975-01-10 1983-03-03 Chemische Werke Hüls AG, 4370 Marl Verfahren zur Verringerung des Gehaltes an monomerem Vinylchlorid in durch Massepolymerisation hergestelltem Polyvinylchlorid
JPS6020402B2 (ja) * 1975-02-25 1985-05-22 チッソ株式会社 塩化ビニル樹脂から微量の塩化ビニル単量体を分離する方法
US4031056A (en) * 1975-02-27 1977-06-21 Tenneco Chemicals, Inc. Process for the removal of vinyl chloride from latexes containing polyvinyl chloride
US4217444A (en) * 1975-03-28 1980-08-12 Rhone-Poulenc Industries Method of degassing polymers prepared by mass polymerizing a monomeric composition based on vinyl chloride
FR2305446A1 (fr) * 1975-03-28 1976-10-22 Rhone Poulenc Ind Procede ameliore de degazage des polymeres et copolymeres prepares par polymerisation en masse d'une composition monomere a base de chlorure de vinyle
JPS51127187A (en) * 1975-04-26 1976-11-05 Kureha Chem Ind Co Ltd A process and an apparatus for recovering monomers
JPS51149389A (en) * 1975-05-14 1976-12-22 Sumitomo Chem Co Ltd A method to decrease the vinyl chloride monomer remaining in the polyv inyl chloride resin slurry
US4171427A (en) * 1975-05-16 1979-10-16 Hoechst Aktiengesellschaft Process for continuously removing monomers from an aqueous dispersion of a polymer
JPS51135990A (en) * 1975-05-20 1976-11-25 Shin Etsu Chem Co Ltd Method of removing residual monomers f rom polyvinylchloride slurries
FR2312514A1 (fr) * 1975-05-26 1976-12-24 Solvay Procede pour la polymerisation du chlorure de vinyle en suspension aqueuse
IL50060A (en) * 1975-08-13 1979-09-30 Tenneco Chem Process for the removal of vinyl chloride from polyvinyl chloride latexes and slurries
US4168373A (en) * 1975-11-24 1979-09-18 Borden, Inc. Removal of residual vinyl chloride monomer from polyvinyl chloride latex
JPS5813563B2 (ja) * 1976-04-03 1983-03-14 信越化学工業株式会社 塩化ビニルの水性分散液から未反応モノマ−を除去する方法およびその装置
US4226976A (en) * 1976-09-20 1980-10-07 Tenneco Chemicals, Inc. Process for the removal of vinyl chloride from polyvinyl chloride latexes and slurries with hydrocarbon compounds
US4226974A (en) * 1977-01-21 1980-10-07 Tenneco Chemicals, Inc. Process for the removal of vinyl chloride from polyvinyl chloride latexes and slurries
US4219640A (en) * 1977-09-22 1980-08-26 Tenneco Chemicals, Inc. Polymers of vinyl chloride having low vinyl chloride monomer content, and method of making same
US4229569A (en) * 1979-02-05 1980-10-21 Tenneco Chemicals, Inc. Process for the removal of vinyl chloride from aqueous slurries of vinyl chloride polymers
DE3122614A1 (de) * 1981-06-06 1983-01-05 Hoechst Ag, 6000 Frankfurt "verfahren zur polymerisation von vinylchlorid in der masse"

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1126743A (en) * 1964-02-12 1968-09-11 Dunlop Co Ltd Preparation of solid polymeric compositions

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE954920C (de) * 1955-02-19 1956-12-27 Hoechst Ag Verfahren zum Aufarbeiten von Emulsionen von Polyvinylverbindungen, insbesondere Polyvinylchlorid
NL126831C (fr) * 1963-10-24
BE686088A (fr) * 1966-08-29 1967-02-28
US3622553A (en) * 1967-12-18 1971-11-23 Phillips Petroleum Co Agitated reactor and gas fluidized bed reactor in series for polymerization of vinyl chloride
DE2442931B2 (de) * 1974-09-07 1976-11-04 Chemische Werke Hüls AG, 4370 Mari Verfahren zur entfernung von nicht umgesetztem vinylchlorid aus waessrigen polyvinylchlorid-dispersionen

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB1126743A (en) * 1964-02-12 1968-09-11 Dunlop Co Ltd Preparation of solid polymeric compositions

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2291236A1 (fr) * 1974-11-14 1976-06-11 Hoechst Ag Procede de preparation de melanges pulverulents prets au faconnage, a base de polymeres de chlorure de vinyle
DE2641563A1 (de) * 1975-09-15 1977-03-17 Tenneco Chem Verfahren zum herabsetzen des gehaltes an monomerem vinylchlorid in trockenen polyvinylchloridteilchen
FR2323704A1 (fr) * 1975-09-15 1977-04-08 Tenneco Chem Polymeres du chlorure de vinyle ayant une faible teneur en chlorure de vinyle monomere, et leur obtention
FR2372178A1 (fr) * 1976-11-24 1978-06-23 Hoechst Ag Procede pour ameliorer les proprietes des polymeres de chlorure de vinyle
CN111841453A (zh) * 2020-06-18 2020-10-30 西北大学 一种应用于热重分析的微型流化床反应装置
CN111841453B (zh) * 2020-06-18 2022-08-23 西北大学 一种应用于热重分析的微型流化床反应装置

Also Published As

Publication number Publication date
FR2193042B1 (fr) 1976-05-28
FI57423C (fi) 1980-08-11
DE2331895C2 (de) 1989-04-06
NL172860C (nl) 1986-02-17
FI57423B (fi) 1980-04-30
NL7309808A (fr) 1974-01-22
IT989178B (it) 1975-05-20
NL172860B (nl) 1983-06-01
DE2331895A1 (de) 1974-01-31

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