FI77213B - Foerfarande foer framstaellning av vaeteperoxid i en loesning innehaollande alkylerad antrakinon och hydrerade derivat daerav. - Google Patents

Foerfarande foer framstaellning av vaeteperoxid i en loesning innehaollande alkylerad antrakinon och hydrerade derivat daerav. Download PDF

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Publication number
FI77213B
FI77213B FI851136A FI851136A FI77213B FI 77213 B FI77213 B FI 77213B FI 851136 A FI851136 A FI 851136A FI 851136 A FI851136 A FI 851136A FI 77213 B FI77213 B FI 77213B
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FI
Finland
Prior art keywords
hydrogenation
reactants
preparation solution
hydrogenated
tetrahydro
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Application number
FI851136A
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English (en)
Finnish (fi)
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FI851136L (fi
FI77213C (sv
FI851136A0 (fi
Inventor
Dalbir Singh Sethi
Morton Meadow
Elizabeth Alice Scarito
Original Assignee
Fmc Corp
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Application filed by Fmc Corp filed Critical Fmc Corp
Publication of FI851136A0 publication Critical patent/FI851136A0/fi
Publication of FI851136L publication Critical patent/FI851136L/fi
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Application granted granted Critical
Publication of FI77213C publication Critical patent/FI77213C/sv

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B15/00—Peroxides; Peroxyhydrates; Peroxyacids or salts thereof; Superoxides; Ozonides
    • C01B15/01—Hydrogen peroxide
    • C01B15/022—Preparation from organic compounds
    • C01B15/023—Preparation from organic compounds by the alkyl-anthraquinone process

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Medicines Containing Material From Animals Or Micro-Organisms (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Saccharide Compounds (AREA)
  • Oxygen, Ozone, And Oxides In General (AREA)
  • Compounds Of Unknown Constitution (AREA)
  • Nitrogen And Oxygen Or Sulfur-Condensed Heterocyclic Ring Systems (AREA)
  • Catalysts (AREA)
  • Epoxy Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Claims (4)

1. Förfarande för framställning av väteperoxid medelst cykliska steg, vid vilka man reducerar, oxiderar 5 och extralierar en franiställningslösning innehällande sä-som reagerande föreningar en alkylerad antrakinon och motsvarande hydrokinon, tetrahydroantrakinon och tetra-hydroandrahydrokinon, kännetecknad därav, att molandelen av de reagerande föreningarnas ringhydre- 10 rade tetrahydrokomponenter i framställningslösningen ökas genom att reglera halten av de inte ringhydrerade reagerande föreningarna sä att den maximalt motsvarar maximi-lösligheten för den i framställningslösningen bildade ant-rahydrokinonen vid hydreringstemperatur, framställnings- 15 lösningen hydreras i närvaro av en palladiumkatalysator vid ett tryck av 50 - 400 kilopascal och en temperatur högst 50°C, och minst 90 % av den hydrerade framställningslösningen cirkuleras utan oxidering och extrahering tili hydreringsanordningen , och sä ökas molandelen av de reage- 20 rande föreningarnas tetrahydrokomponenter utan att väsent-liga mängder av icke-önskade biprodukter bildas.
2. Förfarande enligt patentkravet 1, k ä n n e -t e c k n a t därav, att den alkylerade antrakinonen väljs av gruppen bestäende av 2-etylantrakinon, 2-isobut- 25 ylantrakinon och 2-amy laiitrakinon, trycket är inom om-rädet 100 - 200 kilopascal och hydreringstemperatur är inom omradet 40 - 50°C.
3. Förfarande enligt patentkravet 1 eller 2, kännetecknat därav, att minst 95 % av den 30 hydrerade framställningslösningen cirkuleras tili hyd-' rering9anordningen.
4. Förfarande enligt nägot av patentkraven 1-3, kännetecknat därav, att en reagerande för-ening som väljts av gruppen 2-etylantrakinon, 2-isobutyl- 35 antrakinon, 2-amylantrakinon, motsvarande 2-alkylantraki-non, motsvarande 5,6,7,8-tetrahydro-2-alkylantrakinon
FI851136A 1984-04-19 1985-03-21 Förfarande för framställning av väteperoxid i en lösning innehållande alkylerad antrakinon och hydrerade derivat därav. FI77213C (sv)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US06/601,823 US4539196A (en) 1984-04-19 1984-04-19 Process for hydrogenating an alkylated anthraquinone
US60182384 1984-04-19

Publications (4)

Publication Number Publication Date
FI851136A0 FI851136A0 (fi) 1985-03-21
FI851136L FI851136L (fi) 1985-10-20
FI77213B true FI77213B (fi) 1988-10-31
FI77213C FI77213C (sv) 1989-02-10

Family

ID=24408919

Family Applications (1)

Application Number Title Priority Date Filing Date
FI851136A FI77213C (sv) 1984-04-19 1985-03-21 Förfarande för framställning av väteperoxid i en lösning innehållande alkylerad antrakinon och hydrerade derivat därav.

Country Status (16)

Country Link
US (1) US4539196A (sv)
EP (1) EP0158864B1 (sv)
JP (1) JPS60235703A (sv)
AT (1) ATE40340T1 (sv)
AU (1) AU566339B2 (sv)
BR (1) BR8501566A (sv)
CA (1) CA1228219A (sv)
DE (1) DE3567842D1 (sv)
DK (1) DK127985A (sv)
ES (1) ES8607180A1 (sv)
FI (1) FI77213C (sv)
MX (1) MX160994A (sv)
NO (1) NO164229C (sv)
PT (1) PT80211B (sv)
TR (1) TR22380A (sv)
ZA (1) ZA852189B (sv)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE4013090A1 (de) * 1990-04-25 1991-10-31 Peroxid Chemie Gmbh Verfahren zur herstellung von alkyltetrahydroanthrahydrochinon und diese enthaltende arbeitsloesungen fuer die wasserstoffperoxid-herstellung nach dem anthrachinonverfahren
JP3617532B2 (ja) * 1992-12-25 2005-02-09 三菱瓦斯化学株式会社 過酸化水素の製造方法
NO941388D0 (no) * 1994-04-15 1994-04-15 Kvaerner Process Systems As Produksjon av kjemikalier som kan anvendes i celluloseindustrien
FR2730985B1 (fr) * 1995-02-28 1997-08-01 Chemoxal Sa Procede et installation de production de peroxyde d'hydrogene
FR2730986B1 (fr) * 1995-02-28 1997-05-16 Chemoxal Sa Installation de production de peroxyde d'hydrogene
DE60025143T2 (de) 1999-11-22 2006-07-06 Akzo Nobel N.V. Verfahren und Zusammensetzung zur Herstellung von Wasserstoffperoxid
JP4973041B2 (ja) * 2006-07-14 2012-07-11 三菱瓦斯化学株式会社 過酸化水素の製造方法
KR100998082B1 (ko) * 2008-07-22 2010-12-03 오씨아이 주식회사 생산성을 향상시킨 과산화수소 제조 방법 및 이를 위한조성물
CN106672911B (zh) * 2015-11-11 2018-08-14 中国石油化工股份有限公司 一种蒽醌法生产双氧水的氧化-萃取工艺
WO2023102759A1 (en) * 2021-12-08 2023-06-15 Solvay Sa A composition comprising 2-amylenyl-anthraquinones, preparation method and its use thereof

Family Cites Families (28)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2158525A (en) * 1935-10-10 1939-05-16 Ig Farbenindustrie Ag Production of hydrogen peroxide
US2495229A (en) * 1947-03-13 1950-01-24 Buffalo Electro Chem Co Production of tetrahydroanthraquinones
US2657980A (en) * 1949-11-05 1953-11-03 Du Pont Production of hydrogen peroxide
US2673140A (en) * 1951-11-29 1954-03-23 Du Pont Production of hydrogen peroxide
US2914382A (en) * 1953-06-09 1959-11-24 Laporte Chemical Production of hydrogen peroxide
BE529462A (sv) * 1953-06-09
US2739042A (en) * 1954-01-12 1956-03-20 Allied Chem & Dye Corp Process for the production of hydrogen peroxide
US2867507A (en) * 1958-05-08 1959-01-06 Du Pont Hydrogenation of alkylanthraquinones
US3030186A (en) * 1958-05-16 1962-04-17 Fmc Corp Manufacture of hydrogen peroxide
US3009782A (en) * 1958-05-22 1961-11-21 Fmc Corp Production of hydrogen peroxide by anthraquinone process in the presence of a fixed bed catalyst
US2995424A (en) * 1958-10-06 1961-08-08 Allied Chem Hydrogen peroxide via tetrahydroanthraquinone
US3041143A (en) * 1959-06-18 1962-06-26 Lynn H Dawsey Production of hydrogen peroxide
US3062622A (en) * 1960-06-27 1962-11-06 Fmc Corp Production of hydrogen peroxide by anthraquinone process
US3073680A (en) * 1961-03-20 1963-01-15 Fmc Corp Production of hydrogen peroxide
US3132001A (en) * 1961-04-28 1964-05-05 Solvay Process for the generation of recycle solutions employed for the manufacture of hydrogen peroxide via intermediary alkylanthraquinones
US3307909A (en) * 1962-10-04 1967-03-07 Du Pont Chemical process for the production of hydrogen peroxide
US3330625A (en) * 1963-10-22 1967-07-11 Pittsburgh Plate Glass Co Hydrogen peroxide manufacture
GB1132693A (en) * 1964-11-17 1968-11-06 Laporte Chemical Improvements in or relating to hydrogen peroxide
US3565581A (en) * 1968-05-16 1971-02-23 Fmc Corp Production of hydrogen peroxide in the anthraquinone process using a novel catalytic fixed bed
US3615207A (en) * 1969-06-16 1971-10-26 Fmc Corp Production of hydrogen peroxide by anthraquinone process
US3965251A (en) * 1970-08-18 1976-06-22 Mitsubishi Gas Chemical Company, Inc. Method of regenerating a degraded working solution for the production of hydrogen peroxide
US3887490A (en) * 1970-08-27 1975-06-03 Degussa Process for regenerating noble metal catalyst for the synthesis of hydrogen peroxide according to the anthraquinone process
US3755552A (en) * 1970-10-21 1973-08-28 Fmc Corp Process for producing hydrogen peroxide
US3767779A (en) * 1971-07-06 1973-10-23 Oxysynthese Process for manufacturing hydrogen peroxide
BE769675A (fr) * 1971-07-08 1972-01-10 Solvay Procede cyclique de fabrication de peroxyde d'hydrogene.
FR2503124A1 (fr) * 1981-04-07 1982-10-08 Ugine Kuhlmann Amelioration au procede de fabrication cyclique du peroxyde d'hydrogene
JPS5955843A (ja) * 1982-09-27 1984-03-31 イ−・アイ・デユ・ポン・ドウ・ヌム−ル・アンド・カンパニ− アルキルアントラキノン使用液の水添処理法
JPS6074594A (ja) * 1983-09-30 1985-04-26 日立電子株式会社 ハイブリッドｉｃ用小片基板の製造方法

Also Published As

Publication number Publication date
ATE40340T1 (de) 1989-02-15
TR22380A (tr) 1987-03-16
PT80211A (en) 1985-05-01
DK127985A (da) 1985-10-20
BR8501566A (pt) 1985-12-03
EP0158864A2 (en) 1985-10-23
JPS60235703A (ja) 1985-11-22
NO164229C (no) 1990-09-12
MX160994A (es) 1990-06-29
FI851136L (fi) 1985-10-20
ZA852189B (en) 1985-11-27
FI77213C (sv) 1989-02-10
EP0158864A3 (en) 1986-02-19
FI851136A0 (fi) 1985-03-21
DE3567842D1 (en) 1989-03-02
NO851132L (no) 1985-10-21
ES541820A0 (es) 1986-05-16
US4539196A (en) 1985-09-03
PT80211B (en) 1987-02-16
ES8607180A1 (es) 1986-05-16
AU566339B2 (en) 1987-10-15
DK127985D0 (da) 1985-03-21
NO164229B (no) 1990-06-05
AU4034985A (en) 1985-10-24
EP0158864B1 (en) 1989-01-25
CA1228219A (en) 1987-10-20

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Owner name: FMC CORPORATION