FI68403C - Foerfarande foer framstaellning av 4,1',6'-triklor-4,1',6'-trideoxi-galaktosackaros - Google Patents

Foerfarande foer framstaellning av 4,1',6'-triklor-4,1',6'-trideoxi-galaktosackaros Download PDF

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Publication number
FI68403C
FI68403C FI803982A FI803982A FI68403C FI 68403 C FI68403 C FI 68403C FI 803982 A FI803982 A FI 803982A FI 803982 A FI803982 A FI 803982A FI 68403 C FI68403 C FI 68403C
Authority
FI
Finland
Prior art keywords
sucrose
penta
chlorination
pentaacetate
reaction
Prior art date
Application number
FI803982A
Other languages
English (en)
Finnish (fi)
Swedish (sv)
Other versions
FI803982L (fi
FI68403B (fi
Inventor
Graham Jackson
Michael Ralph Jenner
David Waite
John Clive Williams
Original Assignee
Tate & Lyle Plc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Tate & Lyle Plc filed Critical Tate & Lyle Plc
Publication of FI803982L publication Critical patent/FI803982L/fi
Publication of FI68403B publication Critical patent/FI68403B/fi
Application granted granted Critical
Publication of FI68403C publication Critical patent/FI68403C/fi

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H5/00—Compounds containing saccharide radicals in which the hetero bonds to oxygen have been replaced by the same number of hetero bonds to halogen, nitrogen, sulfur, selenium, or tellurium
    • C07H5/02—Compounds containing saccharide radicals in which the hetero bonds to oxygen have been replaced by the same number of hetero bonds to halogen, nitrogen, sulfur, selenium, or tellurium to halogen

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Biochemistry (AREA)
  • Biotechnology (AREA)
  • General Health & Medical Sciences (AREA)
  • Genetics & Genomics (AREA)
  • Molecular Biology (AREA)
  • Saccharide Compounds (AREA)
FI803982A 1979-12-20 1980-12-19 Foerfarande foer framstaellning av 4,1',6'-triklor-4,1',6'-trideoxi-galaktosackaros FI68403C (fi)

Applications Claiming Priority (10)

Application Number Priority Date Filing Date Title
GB7943933 1979-12-20
GB7943933 1979-12-20
GB8010629 1980-03-28
GB8010629 1980-03-28
GB8011086 1980-04-02
GB8011086 1980-04-02
GB8016668 1980-05-20
GB8016668 1980-05-20
GB8036711 1980-11-14
GB8036711 1980-11-14

Publications (3)

Publication Number Publication Date
FI803982L FI803982L (fi) 1981-06-21
FI68403B FI68403B (fi) 1985-05-31
FI68403C true FI68403C (fi) 1985-09-10

Family

ID=27516402

Family Applications (1)

Application Number Title Priority Date Filing Date
FI803982A FI68403C (fi) 1979-12-20 1980-12-19 Foerfarande foer framstaellning av 4,1',6'-triklor-4,1',6'-trideoxi-galaktosackaros

Country Status (15)

Country Link
US (1) US4362869A (ru)
EP (1) EP0031651B1 (ru)
AU (1) AU532217B2 (ru)
CA (1) CA1152983A (ru)
DE (1) DE3062467D1 (ru)
DK (1) DK155946C (ru)
FI (1) FI68403C (ru)
GR (1) GR72482B (ru)
IL (1) IL61763A (ru)
NO (1) NO149389C (ru)
NZ (1) NZ195891A (ru)
PH (1) PH16877A (ru)
PT (1) PT72208B (ru)
SU (1) SU1176844A3 (ru)
YU (1) YU41010B (ru)

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US4612373A (en) * 1982-09-13 1986-09-16 Tate & Lyle Public Limited Co. Trichloro, 6-substituted sucrose compounds, compositions and uses therefor
GB8525871D0 (en) * 1985-10-21 1985-11-27 Tate & Lyle Plc Chemical compound
GB8525953D0 (en) * 1985-10-21 1985-11-27 Mcneilab Inc Preparation of galactopyranoside
GB8525954D0 (en) * 1985-10-21 1985-11-27 Mcneilab Inc Chlorination of carbohydrates &c alcohols
GB8622345D0 (en) * 1986-09-17 1986-10-22 Tate & Lyle Plc Sucrose derivatives
GB8622342D0 (en) * 1986-09-17 1986-10-22 Tate & Lyle Plc Process
US4950746A (en) * 1988-07-18 1990-08-21 Noramco, Inc. Process for synthesizing sucrose derivatives by regioselective reaction
GB8818430D0 (en) * 1988-08-03 1988-09-07 Tate & Lyle Plc Process
GB8822673D0 (en) * 1988-09-27 1988-11-02 Tate & Lyle Plc Selective acylation of sugars
EP0364100B1 (en) * 1988-09-16 1992-11-25 TATE & LYLE PUBLIC LIMITED COMPANY Process for the chlorination of sugars
GB8822674D0 (en) * 1988-09-27 1988-11-02 Tate & Lyle Plc Preparation of acylated sucrose derivatives
US4980463A (en) * 1989-07-18 1990-12-25 Noramco, Inc. Sucrose-6-ester chlorination
US5089608A (en) * 1990-03-23 1992-02-18 Mcneil-Ppc, Inc. Selective 6-acylation of sucrose mediated by cyclic adducts of dialkyltin oxides and diols
US5023329A (en) * 1990-04-23 1991-06-11 Noramco, Inc. Sucrose-6-ester production process
US5136031A (en) * 1990-07-09 1992-08-04 Tate & Lyle Public Limited Company Chlorination of sugars
NZ240818A (en) 1990-12-14 1993-08-26 Mcneil Ppc Inc Liquid sucralose concentrate compositions containing preservative, buffer and liquid
GB9110821D0 (en) 1991-05-21 1991-07-10 Tate & Lyle Plc Continuous process for the preparation of sucrose 6-esters
AU2691802A (en) 2000-11-17 2002-05-27 Mcneil Ppc Inc Improved sucralose composition and process for its preparation
US7049435B2 (en) 2002-03-08 2006-05-23 Tate & Lyle Public Limited Company Extractive methods for purifying sucralose
US6998480B2 (en) 2002-03-08 2006-02-14 Tate & Lyle Public Limited Company Process for improving sucralose purity and yield
US6890581B2 (en) * 2002-04-05 2005-05-10 Tate & Lyle Public Limited Company Methods for buffer stabilized aqueous deacylation
US20040170735A2 (en) * 2002-04-05 2004-09-02 Mcneil-Ppc, Inc. Methods and compositions for altering the sweetness delivery profile of sucralose
US20040086605A1 (en) * 2002-10-30 2004-05-06 Sox Thomas E. Composition for delivering a high intensity sweetener
US6943248B2 (en) 2003-04-30 2005-09-13 Tate & Lyle Public Limited Company Crystalline form of sucralose, and method for producing it
WO2005087020A1 (en) * 2004-03-05 2005-09-22 Richmond Chemical Corporation High-intensity sweetener-polyol compositions
US20050214425A1 (en) * 2004-03-23 2005-09-29 Roma Vazirani Sugar substitute prepared with nutritive and high-intensity sweeteners
US20080125584A1 (en) * 2004-12-10 2008-05-29 Rakesh Ratnam Salts Assisted Selective Extraction Of 6-Acetyl- 4,1' , 6' Trichlorogalactosucrose And 4,1', 6' Trichlorogalactosucrosse From Aqueous Reaction Mixture
GB2437442B (en) * 2004-12-10 2010-03-31 Pharmed Medicare Pvt Ltd Improved process for purification of 6 acetyl 4,1',6' trichlorogalactosucrose and 4,1'6' trichlorogalactosucrose by chromatography on silanized silica gel
US20060188629A1 (en) * 2005-01-21 2006-08-24 Greg Liesen Method for the purification of sucralose
US7750146B2 (en) 2005-03-18 2010-07-06 Tate & Lyle Plc Granular sucralose
US20060247180A1 (en) * 2005-04-29 2006-11-02 Bergey James L Purgative composition and uses thereof
AU2006277556A1 (en) * 2005-05-04 2007-02-15 V.B. Medicare Private Limited Generation of Phosphorus Oxychloride as by-product from Phosphorus Pentachloride and DMF and its use for chlorination reaction by converting into Vilsmeier-Haack reagent.
CA2623071A1 (en) * 2005-09-22 2007-05-24 Pharmed Medicare Pvt. Ltd. Novel preparation of 6-o-acyl chlorosucrose from anhydrous chlorinated reaction mass
US20070100139A1 (en) * 2005-10-31 2007-05-03 Healthy Brands, Llc Methods for chlorinating sucrose-6-ester
US7741477B2 (en) * 2006-01-10 2010-06-22 Alembic Limited Process for purification of sucralose
CN100395251C (zh) * 2006-01-12 2008-06-18 上海迪赛诺维生素有限公司 一种三氯蔗糖的合成方法
WO2007096726A2 (en) * 2006-02-20 2007-08-30 Emcure Pharmaceuticals Limited Process for the preparation of a glucose derivative
CN101395167A (zh) * 2006-02-28 2009-03-25 V.B.医疗保险私人有限公司 用于使用氯化亚砜氯化糖的新型氯化试剂以及新方法
CN100418976C (zh) * 2006-04-03 2008-09-17 广州科宏食品添加物有限公司 一种三氯蔗糖的制备方法
JP2009542625A (ja) * 2006-07-06 2009-12-03 アレムビック・リミテッド 高純度スクラロースの改良製造法
CN100567319C (zh) * 2006-07-12 2009-12-09 上海迪赛诺维生素有限公司 一种三氯蔗糖的结晶方法
CN100420697C (zh) * 2006-08-30 2008-09-24 河北苏科瑞科技有限公司 一种制备蔗糖-6-有机酸酯的方法
AU2007328222A1 (en) * 2006-12-05 2008-06-12 Tate & Lyle Technology Ltd. Trityl chloride recovery
CN101012253B (zh) * 2007-02-06 2010-04-14 启东东岳药业有限公司 6-pas的制备方法
JPWO2008099560A1 (ja) * 2007-02-16 2010-05-27 梶原　正宏 アルドース誘導体の製造方法
US20080300392A1 (en) * 2007-06-04 2008-12-04 Polymed Therapeutics, Inc. Novel chlorination process for preparing sucralose
US20080300401A1 (en) * 2007-06-04 2008-12-04 Polymed Therapeutics, Inc. Novel chlorination process for preparing sucralose
CN101245085B (zh) 2007-12-19 2012-02-01 上海同辰生物科技有限公司 一种三氯蔗糖的合成及纯化工艺
AR070082A1 (es) * 2008-01-04 2010-03-10 Tate & Lyle Technology Ltd Metodo para la produccion de sucralosa
CN101977664B (zh) * 2008-03-20 2014-02-26 塔特和莱利技术有限公司 从叔酰胺溶剂中去除酸
US8436157B2 (en) * 2008-03-26 2013-05-07 Tate & Lyle Technology Limited Method for the production of sucralose
CN101981044B (zh) * 2008-04-03 2014-08-06 塔特和莱利技术有限公司 碳水化合物浓度对三氯半乳蔗糖萃取效率的影响
US8497367B2 (en) * 2008-04-03 2013-07-30 Tate & Lyle Technology Limited Sucralose purification process
US20090299055A1 (en) * 2008-04-03 2009-12-03 Tate & Lyle Technology Limited Purification of Sucralose Containing Feed Streams for Sucralose Crystallization
AR071134A1 (es) * 2008-04-03 2010-05-26 Tate & Lyle Technology Ltd Cristalizacion de sucralosa a partir de chorros que contienen sucralosa
WO2009124113A1 (en) * 2008-04-03 2009-10-08 Tate & Lyle Technology Ltd. Extraction of less polar impurities from sucralose containing aqueous feed streams
GB2474310B (en) 2009-10-12 2012-02-29 Tate & Lyle Technology Ltd Process for the production of sucrose-6-ester
GB2474311B (en) * 2009-10-12 2012-10-17 Tate & Lyle Technology Ltd Low temperature, single solvent process for the production of sucrose-6-ester
CN102336787B (zh) * 2011-11-01 2014-06-04 安徽万和制药有限公司 一种高效合成三氯蔗糖的方法
CN102336786A (zh) * 2011-11-01 2012-02-01 安徽万和制药有限公司 一种三氯蔗糖的高效结晶方法
CN102942599B (zh) * 2012-11-28 2015-08-26 湖北益泰药业有限公司 一种蔗糖-6-乙酯的提纯方法

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Publication number Priority date Publication date Assignee Title
US4008218A (en) * 1972-08-25 1977-02-15 Meiji Seiki Kaisha, Ltd. 1-N-((S)-α-substituted-ω-aminoacyl)-neamine or -ribostamycin and the production thereof
US4117224A (en) * 1974-10-15 1978-09-26 Tate & Lyle Limited Preparation of sucrose 6,6'-dichloro hexa-acetate
EP0010409A1 (en) * 1978-10-18 1980-04-30 TATE & LYLE PATENT HOLDINGS LIMITED Bittering agents

Also Published As

Publication number Publication date
PT72208A (en) 1981-01-01
CA1152983A (en) 1983-08-30
AU532217B2 (en) 1983-09-22
GR72482B (ru) 1983-11-14
PH16877A (en) 1984-04-02
AU6554380A (en) 1981-06-25
NO149389B (no) 1984-01-02
PT72208B (en) 1981-10-28
NO803851L (no) 1981-06-22
DK155946C (da) 1989-10-23
IL61763A (en) 1984-10-31
FI803982L (fi) 1981-06-21
FI68403B (fi) 1985-05-31
YU41010B (en) 1986-10-31
NO149389C (no) 1984-04-11
IL61763A0 (en) 1981-01-30
EP0031651B1 (en) 1983-03-23
DE3062467D1 (en) 1983-04-28
NZ195891A (en) 1982-12-07
DK546080A (da) 1981-06-21
EP0031651A1 (en) 1981-07-08
US4362869A (en) 1982-12-07
SU1176844A3 (ru) 1985-08-30
DK155946B (da) 1989-06-05
YU317080A (en) 1983-02-28

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MM Patent lapsed
MM Patent lapsed

Owner name: TATE & LYLE PUBLIC LIMITED COMPANY