FI122018B - Menetelmä betaiinin kiteyttämiseksi - Google Patents

Menetelmä betaiinin kiteyttämiseksi Download PDF

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Publication number
FI122018B
FI122018B FI20000197A FI20000197A FI122018B FI 122018 B FI122018 B FI 122018B FI 20000197 A FI20000197 A FI 20000197A FI 20000197 A FI20000197 A FI 20000197A FI 122018 B FI122018 B FI 122018B
Authority
FI
Finland
Prior art keywords
crystallization
solution
seeding
crystal
betaine
Prior art date
Application number
FI20000197A
Other languages
English (en)
Finnish (fi)
Swedish (sv)
Other versions
FI20000197A (fi
FI20000197A0 (fi
Inventor
Juha Nurmi
Jouko Virtanen
Kristian Eriksson
Original Assignee
Danisco
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Danisco filed Critical Danisco
Publication of FI20000197A0 publication Critical patent/FI20000197A0/fi
Priority to FI20000197A priority Critical patent/FI122018B/fi
Priority to EP10179998A priority patent/EP2292571A3/fr
Priority to DK01948977.2T priority patent/DK1252127T3/da
Priority to EP01948977A priority patent/EP1252127B1/fr
Priority to CA2398295A priority patent/CA2398295C/fr
Priority to ES01948977T priority patent/ES2365899T3/es
Priority to PCT/FI2001/000036 priority patent/WO2001056956A1/fr
Priority to AT01948977T priority patent/ATE509897T1/de
Priority to JP2001556809A priority patent/JP5024578B2/ja
Priority to AU28538/01A priority patent/AU2853801A/en
Priority to US10/181,280 priority patent/US6821339B2/en
Publication of FI20000197A publication Critical patent/FI20000197A/fi
Application granted granted Critical
Publication of FI122018B publication Critical patent/FI122018B/fi

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D9/00—Crystallisation
    • B01D9/02—Crystallisation from solutions
    • C—CHEMISTRY; METALLURGY
    • C13—SUGAR INDUSTRY
    • C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
    • C13B30/00—Crystallisation; Crystallising apparatus; Separating crystals from mother liquors ; Evaporating or boiling sugar juice
    • C13B30/02—Crystallisation; Crystallising apparatus
    • C13B30/026—Discontinuous processes or apparatus therefor
    • C13B30/027—Discontinuous processes or apparatus therefor combined with measuring instruments for effecting control of the process
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B63/00—Purification; Separation; Stabilisation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C227/00—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton
    • C07C227/38—Separation; Purification; Stabilisation; Use of additives
    • C07C227/40—Separation; Purification
    • C07C227/42—Crystallisation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C229/00—Compounds containing amino and carboxyl groups bound to the same carbon skeleton
    • C07C229/02—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton
    • C07C229/04—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated
    • C07C229/06—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated having only one amino and one carboxyl group bound to the carbon skeleton
    • C07C229/10—Compounds containing amino and carboxyl groups bound to the same carbon skeleton having amino and carboxyl groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being acyclic and saturated having only one amino and one carboxyl group bound to the carbon skeleton the nitrogen atom of the amino group being further bound to acyclic carbon atoms or to carbon atoms of rings other than six-membered aromatic rings
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D201/00—Preparation, separation, purification or stabilisation of unsubstituted lactams
    • C07D201/16—Separation or purification
    • C—CHEMISTRY; METALLURGY
    • C13—SUGAR INDUSTRY
    • C13B—PRODUCTION OF SUCROSE; APPARATUS SPECIALLY ADAPTED THEREFOR
    • C13B30/00—Crystallisation; Crystallising apparatus; Separating crystals from mother liquors ; Evaporating or boiling sugar juice
    • C13B30/02—Crystallisation; Crystallising apparatus
    • C—CHEMISTRY; METALLURGY
    • C30—CRYSTAL GROWTH
    • C30B—SINGLE-CRYSTAL GROWTH; UNIDIRECTIONAL SOLIDIFICATION OF EUTECTIC MATERIAL OR UNIDIRECTIONAL DEMIXING OF EUTECTOID MATERIAL; REFINING BY ZONE-MELTING OF MATERIAL; PRODUCTION OF A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; SINGLE CRYSTALS OR HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; AFTER-TREATMENT OF SINGLE CRYSTALS OR A HOMOGENEOUS POLYCRYSTALLINE MATERIAL WITH DEFINED STRUCTURE; APPARATUS THEREFOR
    • C30B7/00—Single-crystal growth from solutions using solvents which are liquid at normal temperature, e.g. aqueous solutions

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Biochemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Metallurgy (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Saccharide Compounds (AREA)
  • Peptides Or Proteins (AREA)
  • Crystals, And After-Treatments Of Crystals (AREA)
FI20000197A 2000-01-31 2000-01-31 Menetelmä betaiinin kiteyttämiseksi FI122018B (fi)

Priority Applications (11)

Application Number Priority Date Filing Date Title
FI20000197A FI122018B (fi) 2000-01-31 2000-01-31 Menetelmä betaiinin kiteyttämiseksi
PCT/FI2001/000036 WO2001056956A1 (fr) 2000-01-31 2001-01-16 Procede de cristallisation d'autres substances que saccharose
DK01948977.2T DK1252127T3 (da) 2000-01-31 2001-01-16 Fremgangsmåde til krystallisering af betainmonohydrat vandfrit betain
EP01948977A EP1252127B1 (fr) 2000-01-31 2001-01-16 Procédé de cristallisation de monohydrate de bétaine et bétaine anhydre
CA2398295A CA2398295C (fr) 2000-01-31 2001-01-16 Procede de cristallisation d'autres substances que saccharose
ES01948977T ES2365899T3 (es) 2000-01-31 2001-01-16 Procedimiento para la cristalización de monohidrato de betaína y de la betaína anhidra.
EP10179998A EP2292571A3 (fr) 2000-01-31 2001-01-16 Procédé de cristallisation d'autres substances que saccharose
AT01948977T ATE509897T1 (de) 2000-01-31 2001-01-16 Ein verfahren zur kristallisation von betainmonohydrat und wasserfreiem betain
JP2001556809A JP5024578B2 (ja) 2000-01-31 2001-01-16 非スクロース物質の結晶化方法
AU28538/01A AU2853801A (en) 2000-01-31 2001-01-16 A process for the crystallization of non-sucrose substances
US10/181,280 US6821339B2 (en) 2000-01-31 2001-01-16 Process for the crystallization of non-sucrose substances

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FI20000197 2000-01-31
FI20000197A FI122018B (fi) 2000-01-31 2000-01-31 Menetelmä betaiinin kiteyttämiseksi

Publications (3)

Publication Number Publication Date
FI20000197A0 FI20000197A0 (fi) 2000-01-31
FI20000197A FI20000197A (fi) 2001-08-01
FI122018B true FI122018B (fi) 2011-07-29

Family

ID=8557278

Family Applications (1)

Application Number Title Priority Date Filing Date
FI20000197A FI122018B (fi) 2000-01-31 2000-01-31 Menetelmä betaiinin kiteyttämiseksi

Country Status (10)

Country Link
US (1) US6821339B2 (fr)
EP (2) EP2292571A3 (fr)
JP (1) JP5024578B2 (fr)
AT (1) ATE509897T1 (fr)
AU (1) AU2853801A (fr)
CA (1) CA2398295C (fr)
DK (1) DK1252127T3 (fr)
ES (1) ES2365899T3 (fr)
FI (1) FI122018B (fr)
WO (1) WO2001056956A1 (fr)

Families Citing this family (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
ES2279109T3 (es) * 2002-05-31 2007-08-16 Accentus Plc Produccion de materiales cristalinos utilizando un ultrasonido de alta intensidad.
FR2922890B1 (fr) * 2007-10-30 2009-12-18 Roquette Freres Procede d'evapocristallisation du maltitol.
DE102016101217A1 (de) * 2016-01-25 2017-07-27 Bma Braunschweigische Maschinenbauanstalt Ag Verfahren zur Gewinnung von Kristallen aus einer Mutterlösung und dafür geeigneter Kristallisationsapparat
JP6746838B1 (ja) * 2019-12-10 2020-08-26 松谷化学工業株式会社 Ｄ−アロース結晶及びその製造方法
CN111440081B (zh) * 2020-04-09 2023-03-31 天津大学 一种制备粒度超均一的无水甜菜碱晶体的方法
CN111423334B (zh) * 2020-04-09 2022-12-06 天津大学 一种制备立方状无水甜菜碱晶体的方法
CN112321441B (zh) * 2020-10-14 2022-04-15 天津大学 一种增加无水甜菜碱片状晶体厚度的蒸发结晶方法

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1811870A1 (de) 1968-11-29 1970-08-06 Siemens Ag Verfahren zum Eindampfen von Loesungen zwecks Gewinnung der geloesten Substanz in Kristallform
SU425420A1 (ru) 1971-05-12 1982-08-30 Специальное Конструкторское Бюро Ордена Трудового Красного Знамени Института Кристаллографии Ан Ссср Способ выращивани кристаллов дигидрофосфата кали
SU798565A1 (ru) 1978-11-04 1981-01-23 Киевский Технологический Институтпищевой Промышленности Способ и устройство контрол про-цЕССОВ КРиСТАллООбРАзОВАНи B CAXAP-НыХ уТфЕл Х
GR73024B (fr) * 1980-02-29 1984-01-25 Suomen Sokeri Oy
US4359430A (en) 1980-02-29 1982-11-16 Suomen Sokeri Osakeyhtio Betaine recovery process
US4504457A (en) * 1982-09-30 1985-03-12 Olin Corporation Continuous process for producing granular calcium hypochlorite particles
US4476248A (en) * 1983-02-28 1984-10-09 The Upjohn Company Crystallization of ibuprofen
FI952065A0 (fi) * 1995-03-01 1995-04-28 Xyrofin Oy Foerfarande foer tillvaratagande av en kristalliserbar organisk foerening
FI97625C (fi) 1995-03-01 1997-01-27 Xyrofin Oy Menetelmä ksyloosin kiteyttämiseksi vesiliuoksista
DE19535017C1 (de) 1995-09-21 1996-11-28 Braunschweigische Masch Bau Verfahren und Vorrichtung zur kontinuierlichen Herstellung von Impfkristallen
FI101980B (fi) 1997-05-05 1998-09-30 Xyrofin Oy Kiteytysmenetelmä

Also Published As

Publication number Publication date
CA2398295A1 (fr) 2001-08-09
DK1252127T3 (da) 2011-08-15
CA2398295C (fr) 2011-03-29
WO2001056956A1 (fr) 2001-08-09
ES2365899T3 (es) 2011-10-13
US6821339B2 (en) 2004-11-23
JP2003521527A (ja) 2003-07-15
JP5024578B2 (ja) 2012-09-12
EP2292571A3 (fr) 2011-03-16
FI20000197A (fi) 2001-08-01
FI20000197A0 (fi) 2000-01-31
ATE509897T1 (de) 2011-06-15
AU2853801A (en) 2001-08-14
EP2292571A2 (fr) 2011-03-09
EP1252127A1 (fr) 2002-10-30
EP1252127B1 (fr) 2011-05-18
US20030131784A1 (en) 2003-07-17

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