ES8207566A1 - Procedimiento para la elaboracion de polieterpolioles - Google Patents

Procedimiento para la elaboracion de polieterpolioles

Info

Publication number
ES8207566A1
ES8207566A1 ES501636A ES501636A ES8207566A1 ES 8207566 A1 ES8207566 A1 ES 8207566A1 ES 501636 A ES501636 A ES 501636A ES 501636 A ES501636 A ES 501636A ES 8207566 A1 ES8207566 A1 ES 8207566A1
Authority
ES
Spain
Prior art keywords
working
organic
polyether polyols
polyether polyol
aqueous phase
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
ES501636A
Other languages
English (en)
Other versions
ES501636A0 (es
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Bayer AG
Original Assignee
Bayer AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Bayer AG filed Critical Bayer AG
Publication of ES8207566A1 publication Critical patent/ES8207566A1/es
Publication of ES501636A0 publication Critical patent/ES501636A0/es
Granted legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/30Post-polymerisation treatment, e.g. recovery, purification, drying
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00Polymeric products of isocyanates or isothiocyanates
    • C08G18/06Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C08G65/2603Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing oxygen
    • C08G65/2606Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing oxygen containing hydroxyl groups
    • C08G65/2609Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing oxygen containing hydroxyl groups containing aliphatic hydroxyl groups
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C08G65/2642Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the catalyst used
    • C08G65/2645Metals or compounds thereof, e.g. salts
    • C08G65/2648Alkali metals or compounds thereof

Landscapes

  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Polyethers (AREA)

Abstract

PROCEDIMIENTO PARA LA PREPARACION DE POLIETERPOLIOLES. CONSTA DE LAS SIGUENTES ETAPAS: 1. ADICION AL POLIMERO ALCALINO DE UN 1 A UN 20 POR 100 EN PESO DE AGUA, ASI COMO DE 0 A UN 30 POR 100 EN PESO DE UN DISOLVENTE ORGANICO INERTE. 2 MANTENIMIENTO DE LA EMULSION FORMADA DURANTE UN TIEMPO DE MEDIA HORA A UNA TEMPERATURA MINIMA DE 70 C CON AGITACION MODERADA O SIN ELLA. 3. SEPARACION DE LA FASE ACUOSA. 4. SEPARACION DE LAS CANTIDADES RESUDULAES DE ALCALI DE LA FASE ORGANICA MEDIANTE DICION DE ACIDOS ABSORBENTES; EL DISOLVENTE ORGANICO Y EL AGUA RESUDUAL SE SEPARAN POR DESTILACION. EN LA TERCERA ETAPA LAS DOS FASES SE SEPARAN PASANDO LA EMULSION A TRAVES DE UNA ESTRUCTURA LAMINAR CONSTITUIDA POR FIBRAS DE METAL O MINERAL CON UN GROSOR ENTRE 1 Y 100 MM.,SIENDO LA VELOCIDAD DE FLUJO DE LA EMULSION A TRAVES DE LA ESTRUCTURA LAMINAR DE 1 A 20 M./H.
ES501636A 1980-04-25 1981-04-24 Procedimiento para la elaboracion de polieterpolioles Granted ES501636A0 (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE19803016113 DE3016113A1 (de) 1980-04-25 1980-04-25 Verfahren zur aufarbeitung von polyetherpolyolen

Publications (2)

Publication Number Publication Date
ES8207566A1 true ES8207566A1 (es) 1982-09-16
ES501636A0 ES501636A0 (es) 1982-09-16

Family

ID=6101003

Family Applications (1)

Application Number Title Priority Date Filing Date
ES501636A Granted ES501636A0 (es) 1980-04-25 1981-04-24 Procedimiento para la elaboracion de polieterpolioles

Country Status (7)

Country Link
US (1) US4482750A (es)
EP (1) EP0038983B1 (es)
JP (1) JPS56167727A (es)
BR (1) BR8102484A (es)
DE (2) DE3016113A1 (es)
ES (1) ES501636A0 (es)
MX (1) MX153635A (es)

Families Citing this family (26)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CS241409B1 (en) * 1983-01-21 1986-03-13 Ladislav Komora Method of water/soluble polyerthers' and/or copolyethers' refining or at least limitation
US4528364A (en) * 1984-04-19 1985-07-09 The Dow Chemical Company Removal of alkaline catalysts from polyether polyols and polyalkylene carbonate polyols
JPS6454026A (en) * 1987-08-24 1989-03-01 Dai Ichi Kogyo Seiyaku Co Ltd Production of modified polyester
JP2568251B2 (ja) * 1988-05-20 1996-12-25 鐘淵化学工業株式会社 粗製ポリエーテルから塩基性アルカリ金属化合物と無機酸との無機塩を除去する方法
DE69324427T2 (de) * 1992-03-24 1999-08-05 Dow Chemical Co Neues endbehandlungsverfahren für hydroxyfunktionelle polythethern
WO1996020972A2 (en) * 1995-01-05 1996-07-11 Bayer Corporation A PROCESS FOR THE REMOVAL OF A pH-BASIC MATERIAL FROM A POLYETHER POLYOL
DE19702787A1 (de) * 1997-01-27 1998-07-30 Bayer Ag Verfahren zur Herstellung von Polyetherpolyolen
AUPO761697A0 (en) * 1997-06-30 1997-07-24 Cardiac Crc Nominees Pty Limited Process for the purification of polyethers
AU741367B2 (en) * 1997-06-30 2001-11-29 Aortech International Plc Process for the purification of polyethers
DE19735795A1 (de) * 1997-08-18 1999-02-25 Bayer Ag Verfahren zur Herstellung von Polyetherpolyolen
US6492565B2 (en) 1998-10-07 2002-12-10 Bayer Aktiengesellschaft Process for the preparation of polyether polyols
US6376625B1 (en) * 1999-08-25 2002-04-23 The Dow Chemical Company Process for purifying polyethers
WO2001044150A2 (en) * 1999-12-17 2001-06-21 E.I. Du Pont De Nemours And Company Continuous process for the preparation of polytrimethylene ether glycol
JP4786847B2 (ja) * 1999-12-17 2011-10-05 イー・アイ・デュポン・ドウ・ヌムール・アンド・カンパニー ポリトリメチレンエーテルグリコールおよびそのコポリマーの生成
DE10121807A1 (de) 2001-05-04 2002-11-07 Bayer Ag Verfahren zur Herstellung von Polyetherpolyolen
US20040249225A1 (en) * 2001-10-24 2004-12-09 Tatsuya Hirata Method an system for recovery of catalysts and process and unit for production of perfluoroalkyl iodide telomers
US6562457B1 (en) 2001-10-31 2003-05-13 E. I. Du Pont De Nemours And Company Polyether ester elastomer comprising polytrimethylene ether ester soft segment and tetramethylene ester hard segment
US6599625B2 (en) 2001-10-31 2003-07-29 E. I. Du Pont De Nemours And Company Polyether ester elastomer comprising polytrimethylene ether ester soft segment and trimethylene ester hard segment
US6852823B2 (en) 2002-08-09 2005-02-08 E. I. Du Pont De Nemours And Company Polyurethane and polyurethane-urea elastomers from polytrimethylene ether glycol
CA2497332A1 (en) * 2004-02-19 2005-08-19 Dai-Ichi Kogyo Seiyaku Co., Ltd. Water soluble nonionic alkylene oxide resin and production process therefor
US7186867B2 (en) * 2004-04-21 2007-03-06 Basf Aktiengesellschaft Process for preparing reactive polyether polyols having an ethylene oxide end block
JP5009620B2 (ja) * 2004-07-13 2012-08-22 株式会社カネカ ポリエーテルの製造方法
JP2006321842A (ja) * 2005-05-17 2006-11-30 Asahi Glass Co Ltd ポリエーテル類の製造方法
US7495063B2 (en) * 2006-02-03 2009-02-24 Dow Global Technologies Inc. Reduced oligomer concentration in high purity polyalkylene glycols
EP2669312A1 (en) 2012-05-29 2013-12-04 Huntsman International Llc Process for the production of polyether polyols
US11572440B2 (en) 2020-02-18 2023-02-07 Covestro Llc Methods for purifying polyols containing oxyalkylene units to reduce 2-methyl-2-pentenal content

Family Cites Families (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE828839C (de) * 1949-02-09 1952-01-21 Anorgana Fa Verfahren zur Abtrennung von Polyglykolen aus Gemischen mit Anlagerungsprodukten von Alkylenoxyden an hydroxyl- oder carboxylhaltige organische Verbindungen
US3299151A (en) * 1963-10-08 1967-01-17 Pittsburgh Plate Glass Co Preparation of polyether polyols
FR1488686A (es) * 1965-08-06 1967-10-25
US3489680A (en) * 1967-10-30 1970-01-13 Mobil Oil Corp Method for breaking a water-in-oil emulsion
US3823145A (en) * 1968-07-26 1974-07-09 Basf Wyandotte Corp Removal of impurities from polyols
US3582491A (en) * 1969-06-12 1971-06-01 Wyandotte Chemicals Corp Removal of inorganic catalysts from polyols
US3715402A (en) * 1969-08-08 1973-02-06 Basf Wyandotte Corp Removal of catalysts from polyols
JPS4733199U (es) * 1971-05-15 1972-12-13
JPS5037036B2 (es) * 1972-06-02 1975-11-29
JPS53123499A (en) * 1977-04-05 1978-10-27 Asahi Denka Kogyo Kk Purification of polyether
US4240908A (en) * 1977-08-05 1980-12-23 Mapco, Inc. Coated metal fiber coalescing cell
US4129718A (en) * 1977-12-01 1978-12-12 Basf Wyandotte Corporation Process for the removal of catalyst from polyether polyol
DE2854541A1 (de) * 1978-12-16 1980-06-26 Bayer Ag Verfahren zur reinigung nichtionischer emulgatoren

Also Published As

Publication number Publication date
JPS56167727A (en) 1981-12-23
JPS643220B2 (es) 1989-01-20
EP0038983A3 (en) 1982-09-22
EP0038983B1 (de) 1984-07-25
MX153635A (es) 1986-12-09
US4482750A (en) 1984-11-13
DE3016113A1 (de) 1981-10-29
DE3165002D1 (en) 1984-08-30
ES501636A0 (es) 1982-09-16
BR8102484A (pt) 1982-01-05
EP0038983A2 (de) 1981-11-04

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