ES8207565A1 - Procedimiento para la elaboracion de polieterpolioles - Google Patents
Procedimiento para la elaboracion de polieterpoliolesInfo
- Publication number
- ES8207565A1 ES8207565A1 ES501639A ES501639A ES8207565A1 ES 8207565 A1 ES8207565 A1 ES 8207565A1 ES 501639 A ES501639 A ES 501639A ES 501639 A ES501639 A ES 501639A ES 8207565 A1 ES8207565 A1 ES 8207565A1
- Authority
- ES
- Spain
- Prior art keywords
- water
- neutralisation
- remainder
- weight
- organic solvent
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
- C08G65/30—Post-polymerisation treatment, e.g. recovery, purification, drying
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D17/00—Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
- B01D17/02—Separation of non-miscible liquids
- B01D17/04—Breaking emulsions
- B01D17/042—Breaking emulsions by changing the temperature
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D17/00—Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
- B01D17/02—Separation of non-miscible liquids
- B01D17/04—Breaking emulsions
- B01D17/045—Breaking emulsions with coalescers
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
- C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
- C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
- C08G65/2603—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing oxygen
- C08G65/2606—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing oxygen containing hydroxyl groups
- C08G65/2609—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing oxygen containing hydroxyl groups containing aliphatic hydroxyl groups
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Polyethers (AREA)
- Processes Of Treating Macromolecular Substances (AREA)
Abstract
PROCEDIMIENTO PARA LA ELABORACION DE POLIETERPOLIOLES. CONSTA DE LAS SIGUENTES ETAPAS 1. ADICION AL POLIMERO ALCALINO DE ACIDOS Y DE UN 1 A UN 30 POR 100 EN PESO DE AGUA, DEMAS DE UN 0 A 30 POR 100 DE UN DISOLVENTE ORGANICO INERTE. 2. LA EMULSION FORMADA DE AGUA EN ACEITE SE CALIENTE A UNA TEMPERATURA DE AL MENOS 70 C.3. LA FASE ACUOSA SE SOMETE A ACOALESCENCIA Y A CONTUNIACION SE SEPARA DE LA FASE ORGANICA. 4. EL AGUA RESIDUAL, ASI COMO EL DISOLVENTE ORGANICO SE SEPARAN POR DESTILACION, SEPARANDO LA SAL RESUDUAL POR FILTRANCION. EL POLIETER EN BRUTO SE NEUTRALIZA A UN PH DE APROXIMADAMENTE 4 A 9. EN LAS EGUNDA ETAPA, LA EMULSION SE CALIENTA AL MENOS A 85. EN LA TERCERA ETAPA LA FASE ACUOSA SE COALIZA CONDUCIENDO LA EMULSION A TRAVES DE UNA ESTRUCTURA LAMINAR.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE19803016112 DE3016112A1 (de) | 1980-04-25 | 1980-04-25 | Verfahren zur aufarbeitung von polyetherpolyolen |
Publications (2)
Publication Number | Publication Date |
---|---|
ES501639A0 ES501639A0 (es) | 1982-09-16 |
ES8207565A1 true ES8207565A1 (es) | 1982-09-16 |
Family
ID=6101002
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ES501639A Expired ES8207565A1 (es) | 1980-04-25 | 1981-04-24 | Procedimiento para la elaboracion de polieterpolioles |
Country Status (5)
Country | Link |
---|---|
EP (1) | EP0038986A3 (es) |
JP (1) | JPS56167726A (es) |
BR (1) | BR8102493A (es) |
DE (1) | DE3016112A1 (es) |
ES (1) | ES8207565A1 (es) |
Families Citing this family (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CS241409B1 (en) * | 1983-01-21 | 1986-03-13 | Ladislav Komora | Method of water/soluble polyerthers' and/or copolyethers' refining or at least limitation |
DE3823455A1 (de) * | 1988-07-11 | 1990-01-18 | Henkel Kgaa | Verfahren zur spaltung von oel-/wasseremulsionen unter verwendung organischer spaltprodukte und die verwendung dieses verfahrens |
DE4444739A1 (de) * | 1994-12-15 | 1996-06-20 | Bayer Ag | Methode zur Aufarbeitung eines tensidhaltigen Reaktionsgemisches |
US6376625B1 (en) * | 1999-08-25 | 2002-04-23 | The Dow Chemical Company | Process for purifying polyethers |
DE102006050381A1 (de) | 2006-10-25 | 2008-05-08 | Bayer Materialscience Ag | Verfahren zur Abtrennung einer organischen von einer elektrolythaltigen wässrigen und organischen Phase |
JP5874285B2 (ja) * | 2011-10-04 | 2016-03-02 | 東ソー株式会社 | ポリアルキレングリコールの製造方法 |
CN109575268A (zh) * | 2018-11-02 | 2019-04-05 | 佳化化学(滨州)有限公司 | 一种聚醚多元醇的精制方法及精制装置 |
US11572440B2 (en) | 2020-02-18 | 2023-02-07 | Covestro Llc | Methods for purifying polyols containing oxyalkylene units to reduce 2-methyl-2-pentenal content |
Family Cites Families (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE828839C (de) * | 1949-02-09 | 1952-01-21 | Anorgana Fa | Verfahren zur Abtrennung von Polyglykolen aus Gemischen mit Anlagerungsprodukten von Alkylenoxyden an hydroxyl- oder carboxylhaltige organische Verbindungen |
GB878460A (en) * | 1958-02-07 | 1961-09-27 | Ici Ltd | Purification of polyethers |
US3582491A (en) * | 1969-06-12 | 1971-06-01 | Wyandotte Chemicals Corp | Removal of inorganic catalysts from polyols |
US3715402A (en) * | 1969-08-08 | 1973-02-06 | Basf Wyandotte Corp | Removal of catalysts from polyols |
US3847821A (en) * | 1973-10-19 | 1974-11-12 | Minnesota Mining & Mfg | Separator for removing a dispersed liquid phase from a continuous liquid phase |
GB1485622A (en) * | 1973-11-05 | 1977-09-14 | Foseco Int | Treatment of droplet dispersions |
DE2554228A1 (de) * | 1974-12-13 | 1976-06-16 | Basf Wyandotte Corp | Verfahren zur reinigung von hydroxylgruppenhaltigen polyaethern |
FR2375890A1 (fr) * | 1977-01-04 | 1978-07-28 | Anvar | Procede et dispositif de separation d'emulsions par coalescence |
US4137398A (en) * | 1978-06-09 | 1979-01-30 | Basf Wyandotte Corporation | Process for the removal of catalyst from polyether polyol |
-
1980
- 1980-04-25 DE DE19803016112 patent/DE3016112A1/de not_active Withdrawn
-
1981
- 1981-04-11 EP EP81102794A patent/EP0038986A3/de not_active Ceased
- 1981-04-23 JP JP6070581A patent/JPS56167726A/ja active Pending
- 1981-04-24 ES ES501639A patent/ES8207565A1/es not_active Expired
- 1981-04-24 BR BR8102493A patent/BR8102493A/pt unknown
Also Published As
Publication number | Publication date |
---|---|
EP0038986A2 (de) | 1981-11-04 |
ES501639A0 (es) | 1982-09-16 |
EP0038986A3 (de) | 1982-03-03 |
DE3016112A1 (de) | 1981-11-05 |
JPS56167726A (en) | 1981-12-23 |
BR8102493A (pt) | 1982-01-05 |
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