ES2721427T3 - Procedimiento para preparar éster alquílico de ácido graso usando destilado de ácido graso - Google Patents
Procedimiento para preparar éster alquílico de ácido graso usando destilado de ácido graso Download PDFInfo
- Publication number
- ES2721427T3 ES2721427T3 ES06757588T ES06757588T ES2721427T3 ES 2721427 T3 ES2721427 T3 ES 2721427T3 ES 06757588 T ES06757588 T ES 06757588T ES 06757588 T ES06757588 T ES 06757588T ES 2721427 T3 ES2721427 T3 ES 2721427T3
- Authority
- ES
- Spain
- Prior art keywords
- fatty acid
- alkyl ester
- acid alkyl
- distillation column
- crude
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10L—FUELS NOT OTHERWISE PROVIDED FOR; NATURAL GAS; SYNTHETIC NATURAL GAS OBTAINED BY PROCESSES NOT COVERED BY SUBCLASSES C10G, C10K; LIQUEFIED PETROLEUM GAS; ADDING MATERIALS TO FUELS OR FIRES TO REDUCE SMOKE OR UNDESIRABLE DEPOSITS OR TO FACILITATE SOOT REMOVAL; FIRELIGHTERS
- C10L1/00—Liquid carbonaceous fuels
- C10L1/02—Liquid carbonaceous fuels essentially based on components consisting of carbon, hydrogen, and oxygen only
- C10L1/026—Liquid carbonaceous fuels essentially based on components consisting of carbon, hydrogen, and oxygen only for compression ignition
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J14/00—Chemical processes in general for reacting liquids with liquids; Apparatus specially adapted therefor
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
- B01J19/006—Baffles
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
- B01J19/1812—Tubular reactors
- B01J19/1818—Tubular reactors in series
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
- B01J19/1868—Stationary reactors having moving elements inside resulting in a loop-type movement
- B01J19/1875—Stationary reactors having moving elements inside resulting in a loop-type movement internally, i.e. the mixture circulating inside the vessel such that the upwards stream is separated physically from the downwards stream(s)
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- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/08—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B3/00—Refining fats or fatty oils
- C11B3/12—Refining fats or fatty oils by distillation
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
- C11C3/00—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom
- C11C3/003—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom by esterification of fatty acids with alcohols
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00002—Chemical plants
- B01J2219/00004—Scale aspects
- B01J2219/00006—Large-scale industrial plants
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00002—Chemical plants
- B01J2219/00027—Process aspects
- B01J2219/0004—Processes in series
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00761—Details of the reactor
- B01J2219/00763—Baffles
- B01J2219/00765—Baffles attached to the reactor wall
- B01J2219/00768—Baffles attached to the reactor wall vertical
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00761—Details of the reactor
- B01J2219/00763—Baffles
- B01J2219/00765—Baffles attached to the reactor wall
- B01J2219/0077—Baffles attached to the reactor wall inclined
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
- C10G2300/10—Feedstock materials
- C10G2300/1011—Biomass
- C10G2300/1014—Biomass of vegetal origin
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
- C10G2300/20—Characteristics of the feedstock or the products
- C10G2300/201—Impurities
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
- C10G2300/40—Characteristics of the process deviating from typical ways of processing
- C10G2300/4006—Temperature
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G2300/00—Aspects relating to hydrocarbon processing covered by groups C10G1/00 - C10G99/00
- C10G2300/40—Characteristics of the process deviating from typical ways of processing
- C10G2300/4012—Pressure
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E50/00—Technologies for the production of fuel of non-fossil origin
- Y02E50/10—Biofuels, e.g. bio-diesel
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P30/00—Technologies relating to oil refining and petrochemical industry
- Y02P30/20—Technologies relating to oil refining and petrochemical industry using bio-feedstock
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Wood Science & Technology (AREA)
- General Chemical & Material Sciences (AREA)
- Microbiology (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Fats And Perfumes (AREA)
- Liquid Carbonaceous Fuels (AREA)
Abstract
Procedimiento para preparar éster alquílico de ácido graso para combustibles biodiesel, que comprende la etapa de esterificar materia prima de ácido graso con alcohol, a una temperatura de 250 a 320 °C y una presión de presión atmosférica a 10 bar, en donde la reacción de esterificación se lleva a cabo sin usar catalizador, en donde la materia prima de ácido graso, que reacciona con el alcohol, es un destilado de ácido graso que se produce como un subproducto durante el proceso de refinación de aceite vegetal crudo para obtener aceite vegetal refinado, y en donde el destilado de ácido graso contiene de 65 a 95% en peso de ácido graso que tiene un número de átomos de carbono de la parte alifática de 14 a 24, que comprende además las etapas de: en primer lugar, refinar un éster alquílico de ácido graso crudo producido en la etapa de esterificación del ácido graso con alcohol, mediante la alimentación del éster alquílico de ácido graso crudo a una columna de destilación y luego la destilación de las impurezas que tienen un punto de ebullición bajo del éster alquílico de ácido graso crudo, manteniendo la temperatura de la parte inferior de la columna de destilación para ser de 150 a 250 °C en condiciones de vacío de 0,133 a 200 mbar (0,1 a 150 torr); y en segundo lugar, refinar el éster alquílico de ácido graso refinado primeramente mediante la alimentación del éster alquílico de ácido graso refinado primeramente a una columna de destilación, manteniendo la temperatura de la parte inferior de la columna de destilación para ser de 200 a 300 °C en condiciones de vacío de 0.133 a 200 mbar (0,1 a 150 torr) para obtener por destilación y eliminación de residuos un ácido graso que tiene un número de átomos de carbono de la parte alifática de 14 a 24.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
PCT/KR2006/001620 WO2007126166A1 (en) | 2006-04-28 | 2006-04-28 | Method and apparatus for preparing fatty acid alkyl ester using fatty acid |
Publications (1)
Publication Number | Publication Date |
---|---|
ES2721427T3 true ES2721427T3 (es) | 2019-07-31 |
Family
ID=38655672
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ES06757588T Active ES2721427T3 (es) | 2006-04-28 | 2006-04-28 | Procedimiento para preparar éster alquílico de ácido graso usando destilado de ácido graso |
Country Status (10)
Country | Link |
---|---|
US (1) | US7951967B2 (es) |
EP (1) | EP2013319B1 (es) |
JP (1) | JP5232139B2 (es) |
CN (1) | CN101198677B (es) |
BR (1) | BRPI0621209B1 (es) |
ES (1) | ES2721427T3 (es) |
IN (1) | IN2012DN00444A (es) |
MX (1) | MX2008011595A (es) |
PL (1) | PL2013319T3 (es) |
WO (1) | WO2007126166A1 (es) |
Families Citing this family (43)
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DE102006047617B4 (de) | 2006-10-09 | 2008-11-27 | Clariant International Limited | Verfahren zur Herstellung basischer (Meth)acrylamide |
JP5380523B2 (ja) * | 2008-04-01 | 2014-01-08 | エスケー ケミカルズ カンパニー リミテッド | 脂肪酸を用いた脂肪酸アルキルエステルの製造方法 |
DE102008017216B4 (de) | 2008-04-04 | 2013-08-14 | Clariant International Ltd. | Kontinuierliches Verfahren zur Herstellung von Fettsäureamiden |
KR101554607B1 (ko) * | 2008-11-07 | 2015-09-22 | 에스케이케미칼주식회사 | 지방산을 이용한 지방산알킬에스테르의 제조방법 및 장치 |
MY156576A (en) | 2008-11-26 | 2016-03-15 | Elevance Renewable Sciences | Methods of producing jet fuel from natural oil feedstocks through metathesis reactions |
WO2010062932A1 (en) | 2008-11-26 | 2010-06-03 | Elevance Renewable Sciences, Inc. | Methods of producing jet fuel from natural oil feedstocks through oxygen-cleaved reactions |
DE102009031053A1 (de) | 2009-06-30 | 2011-01-13 | Clariant International Ltd. | Kontinuierliches Verfahren zur Herstellung von Estern aliphatischer Carbonsäuren |
DE102009031054A1 (de) | 2009-06-30 | 2011-01-13 | Clariant International Ltd. | Kontinuierliches Verfahren zur Herstellung von Estern aromatischer Carbonsäuren |
DE102009031059A1 (de) | 2009-06-30 | 2011-01-05 | Clariant International Ltd. | Vorrichtung zur kontinuierlichen Durchführung chemischer Reaktionen bei hohen Temperaturen |
FI124686B (fi) | 2009-08-14 | 2014-12-15 | Forchem Oy | Menetelmä raakamäntyöljyn jalostamiseksi |
DE102009042522A1 (de) | 2009-09-22 | 2011-04-07 | Clariant International Ltd. | Kontinuierliches Umesterungsverfahren |
DE102009042523B4 (de) | 2009-09-22 | 2012-02-16 | Clariant International Ltd. | Vorrichtung und Verfahren zur kontinuierlichen Durchführung heterogen katalysierter chemischer Reaktionen bei hohen Temperaturen |
US9382502B2 (en) | 2009-10-12 | 2016-07-05 | Elevance Renewable Sciences, Inc. | Methods of refining and producing isomerized fatty acid esters and fatty acids from natural oil feedstocks |
US9000246B2 (en) | 2009-10-12 | 2015-04-07 | Elevance Renewable Sciences, Inc. | Methods of refining and producing dibasic esters and acids from natural oil feedstocks |
US9175231B2 (en) | 2009-10-12 | 2015-11-03 | Elevance Renewable Sciences, Inc. | Methods of refining natural oils and methods of producing fuel compositions |
US9051519B2 (en) | 2009-10-12 | 2015-06-09 | Elevance Renewable Sciences, Inc. | Diene-selective hydrogenation of metathesis derived olefins and unsaturated esters |
EP3170802B1 (en) | 2009-10-12 | 2019-06-19 | Elevance Renewable Sciences, Inc. | Methods of refining and producing fuel from natural oil feedstocks |
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US9365487B2 (en) | 2009-10-12 | 2016-06-14 | Elevance Renewable Sciences, Inc. | Methods of refining and producing dibasic esters and acids from natural oil feedstocks |
US9169447B2 (en) | 2009-10-12 | 2015-10-27 | Elevance Renewable Sciences, Inc. | Methods of refining natural oils, and methods of producing fuel compositions |
FR2966457B1 (fr) | 2010-10-21 | 2012-10-19 | IFP Energies Nouvelles | Procede de production d'esters alkyliques a partir d'huile vegetale ou animale et d'un monoalcool aliphatique avec integration thermique. |
CN102559393B (zh) * | 2010-12-23 | 2015-02-25 | 中国石油化工股份有限公司 | 一种低酸值生物柴油的制备方法 |
DE102010056564A1 (de) | 2010-12-30 | 2012-07-05 | Clariant International Limited | Hydroxylgruppen und Estergruppen tragende Polymere und Verfahren zu ihrer Herstellung |
DE102010056565A1 (de) | 2010-12-30 | 2012-07-05 | Clariant International Ltd. | Verfahren zur Modifizierung Hydroxylgruppen tragender Polymere |
KR20140054291A (ko) * | 2011-08-24 | 2014-05-08 | 바스프 에스이 | 메르캅토알킬 카르복실레이트의 제조 방법 |
US9139493B2 (en) | 2011-12-22 | 2015-09-22 | Elevance Renewable Sciences, Inc. | Methods for suppressing isomerization of olefin metathesis products |
US9133416B2 (en) | 2011-12-22 | 2015-09-15 | Elevance Renewable Sciences, Inc. | Methods for suppressing isomerization of olefin metathesis products |
US9169174B2 (en) | 2011-12-22 | 2015-10-27 | Elevance Renewable Sciences, Inc. | Methods for suppressing isomerization of olefin metathesis products |
GB201210655D0 (en) * | 2012-06-15 | 2012-08-01 | Davy Process Techn Ltd | Process |
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CN103112968B (zh) * | 2013-03-01 | 2014-09-10 | 山东潍坊润丰化工股份有限公司 | 苯氧羧酸类生产废水中高cod成分的处理方法 |
DK3011041T3 (da) * | 2013-06-19 | 2020-05-18 | Argent Energy Uk Ltd | Biodieselsammensætning og dermed forbundet fremgangsmåde og produkter |
KR102327852B1 (ko) * | 2013-07-22 | 2021-11-18 | 에스케이에코프라임 주식회사 | 지방을 이용한 지방산알킬에스테르의 제조방법 |
US9328054B1 (en) | 2013-09-27 | 2016-05-03 | Travis Danner | Method of alcoholisis of fatty acids and fatty acid gyicerides |
CN104496802B (zh) * | 2014-11-28 | 2016-05-04 | 浙江赞宇科技股份有限公司 | 一种生产脂肪酸甘油三酯的酯化反应方法及酯化反应装置 |
CN105112168B (zh) * | 2015-08-21 | 2018-10-26 | 中国石油大学(华东) | 一种生产生物柴油的装置和方法 |
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FR2838433B1 (fr) * | 2002-04-11 | 2005-08-19 | Inst Francais Du Petrole | Procede de production d'esters alkyliques a partir d'une huile vegetale ou animale et d'un monoalcool aliphatique |
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EP1565424A4 (en) | 2002-11-27 | 2006-05-31 | Biodiesel Australia Ltd | METHOD OF MANUFACTURING ALKYLESTER |
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US7473539B2 (en) * | 2004-09-20 | 2009-01-06 | Sunho Biodiesel Corporation | Methods for producing alkyl esters |
KR20050088297A (ko) * | 2005-05-27 | 2005-09-05 | 바이오디젤 오스트레일리아 리미티드. | 알킬 에스테르 제조방법 |
JP2007153943A (ja) * | 2005-12-01 | 2007-06-21 | Japan Energy Corp | エステル交換反応によるエステルの製造方法 |
-
2006
- 2006-04-28 US US12/161,784 patent/US7951967B2/en active Active
- 2006-04-28 CN CN2006800214589A patent/CN101198677B/zh active Active
- 2006-04-28 WO PCT/KR2006/001620 patent/WO2007126166A1/en active Application Filing
- 2006-04-28 ES ES06757588T patent/ES2721427T3/es active Active
- 2006-04-28 IN IN444DEN2012 patent/IN2012DN00444A/en unknown
- 2006-04-28 PL PL06757588T patent/PL2013319T3/pl unknown
- 2006-04-28 JP JP2009507569A patent/JP5232139B2/ja active Active
- 2006-04-28 EP EP06757588.6A patent/EP2013319B1/en active Active
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Publication number | Publication date |
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US20100228042A1 (en) | 2010-09-09 |
PL2013319T3 (pl) | 2019-07-31 |
WO2007126166A1 (en) | 2007-11-08 |
CN101198677B (zh) | 2012-11-14 |
CN101198677A (zh) | 2008-06-11 |
EP2013319A4 (en) | 2012-06-13 |
BRPI0621209B1 (pt) | 2016-03-22 |
US7951967B2 (en) | 2011-05-31 |
JP5232139B2 (ja) | 2013-07-10 |
IN2012DN00444A (es) | 2015-05-15 |
EP2013319A1 (en) | 2009-01-14 |
EP2013319B1 (en) | 2019-01-23 |
MX2008011595A (es) | 2008-09-22 |
JP2009535442A (ja) | 2009-10-01 |
BRPI0621209A2 (pt) | 2011-12-06 |
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