ES2153825T3 - Procedimiento catalitico directo para la produccion de hidroxilamina. - Google Patents
Procedimiento catalitico directo para la produccion de hidroxilamina.Info
- Publication number
- ES2153825T3 ES2153825T3 ES92201955T ES92201955T ES2153825T3 ES 2153825 T3 ES2153825 T3 ES 2153825T3 ES 92201955 T ES92201955 T ES 92201955T ES 92201955 T ES92201955 T ES 92201955T ES 2153825 T3 ES2153825 T3 ES 2153825T3
- Authority
- ES
- Spain
- Prior art keywords
- hydroxylamine
- production
- direct catalytic
- catalytic procedure
- silican
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- AVXURJPOCDRRFD-UHFFFAOYSA-N Hydroxylamine Chemical compound ON AVXURJPOCDRRFD-UHFFFAOYSA-N 0.000 title abstract 2
- 230000003197 catalytic effect Effects 0.000 title abstract 2
- 238000000034 method Methods 0.000 title abstract 2
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 abstract 2
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical group [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 abstract 2
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 abstract 1
- 229910021529 ammonia Inorganic materials 0.000 abstract 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 abstract 1
- 239000003054 catalyst Substances 0.000 abstract 1
- 230000003647 oxidation Effects 0.000 abstract 1
- 238000007254 oxidation reaction Methods 0.000 abstract 1
- 229910052760 oxygen Inorganic materials 0.000 abstract 1
- 239000001301 oxygen Substances 0.000 abstract 1
- 229910052710 silicon Inorganic materials 0.000 abstract 1
- 239000010703 silicon Substances 0.000 abstract 1
- 229910052719 titanium Inorganic materials 0.000 abstract 1
- 239000010936 titanium Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
- C01B21/14—Hydroxylamine; Salts thereof
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
- B01J21/06—Silicon, titanium, zirconium or hafnium; Oxides or hydroxides thereof
- B01J21/063—Titanium; Oxides or hydroxides thereof
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J29/00—Catalysts comprising molecular sieves
- B01J29/89—Silicates, aluminosilicates or borosilicates of titanium, zirconium or hafnium
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
- C01B21/14—Hydroxylamine; Salts thereof
- C01B21/1409—Preparation
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Inorganic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Catalysts (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Silicates, Zeolites, And Molecular Sieves (AREA)
- Crystals, And After-Treatments Of Crystals (AREA)
Abstract
SE PRESENTA UN PROCESO CATALITICO DIRECTO PARA LA PRODUCCION DE HIDROXILAMINO POR MEDIO DE LA OXIDACION DE AMONIACO CON H2O2, EN EL QUE EL CATALIZADOR ESTA COMPUESTO DE SILICIO, TITANIO Y OXIGENO Y TIENE UNA ESTRUCTURA AMORFA O CRISTALINA (COMO EN EL CASO DE SILICATOS DE TITANIO, POR EJEMPLO.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
ITMI911915A IT1252047B (it) | 1991-07-10 | 1991-07-10 | Processo catalitico diretto per la produzione di idrossilammina |
Publications (1)
Publication Number | Publication Date |
---|---|
ES2153825T3 true ES2153825T3 (es) | 2001-03-16 |
Family
ID=11360320
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ES92201955T Expired - Lifetime ES2153825T3 (es) | 1991-07-10 | 1992-07-01 | Procedimiento catalitico directo para la produccion de hidroxilamina. |
Country Status (16)
Country | Link |
---|---|
US (1) | US5320819A (es) |
EP (1) | EP0522634B1 (es) |
JP (1) | JP3374218B2 (es) |
KR (1) | KR930002302A (es) |
AT (1) | ATE198866T1 (es) |
AU (1) | AU1944592A (es) |
CA (1) | CA2073231C (es) |
CZ (1) | CZ285176B6 (es) |
DE (1) | DE69231652T2 (es) |
DK (1) | DK0522634T3 (es) |
ES (1) | ES2153825T3 (es) |
IT (1) | IT1252047B (es) |
PL (1) | PL169232B1 (es) |
RU (1) | RU2099281C1 (es) |
SK (1) | SK217192A3 (es) |
TW (1) | TW232676B (es) |
Families Citing this family (15)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5510097A (en) * | 1994-05-19 | 1996-04-23 | Olin Corporation | Hydroxylammonium nitrate free of ammonium nitrate |
DE4435239A1 (de) * | 1994-10-04 | 1996-04-11 | Basf Ag | Verfahren zur Herstellung von Hydroxylaminen aus Ammoniak oder den entsprechenden Aminen, Wasserstoff und Sauerstoff |
CA2215490A1 (fr) * | 1996-10-11 | 1998-04-11 | Elf Atochem S.A. | Catalyseur a base de titano-silicalites et procede d'obtention d'hydroxylamine n,n-disubstituee |
NL1013899C2 (nl) * | 1999-12-21 | 2001-06-25 | Dsm Nv | Werkwijze voor het bereiden en zuiveren van een hydroxylammoniumzoutoplossing. |
US6281369B1 (en) * | 2000-12-07 | 2001-08-28 | Arco Chemical Technology, L.P. | Epoxidation catalyst and process |
DE10062325A1 (de) * | 2000-12-14 | 2002-06-20 | Basf Ag | Verfahren zur kontinuierlichen Herstellung von Hydroxylammoniumsalzen |
WO2003043937A2 (en) * | 2001-11-15 | 2003-05-30 | Pq Holding, Inc. | Method for controlling synthesis conditions during molecular sieve synthesis using combinations of quaternary ammonium hydroxides and halides |
JP4772326B2 (ja) * | 2002-05-31 | 2011-09-14 | 中國石油化工股▲分▼有限公司 | チタン含有触媒の再生方法 |
CN103193212B (zh) * | 2013-03-15 | 2016-01-20 | 华东师范大学 | 一种游离羟胺的制备方法 |
CN104262196B (zh) * | 2014-09-02 | 2016-07-27 | 河北美邦工程科技有限公司 | 一种氨肟化反应与分离耦合工艺及装置 |
CN105271143B (zh) * | 2015-11-20 | 2017-09-22 | 山东兴辉化工有限公司 | 盐酸羟胺母液的回收处理工艺 |
CN106946235B (zh) * | 2017-03-23 | 2019-03-22 | 北京凯瑞英科技有限公司 | 一种由硝基甲烷和盐酸通过相转移合成盐酸羟胺的方法 |
CN107265420B (zh) * | 2017-06-29 | 2019-06-25 | 河北工业大学 | 一种由环己酮肟水解制备羟胺的方法 |
CN109942457A (zh) * | 2019-04-22 | 2019-06-28 | 河北美邦工程科技股份有限公司 | 一种非均相环己酮肟制备方法 |
CN115215307B (zh) * | 2021-04-15 | 2024-03-29 | 华东师范大学 | 一种羟胺溶液的合成方法 |
Family Cites Families (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
IT1214622B (it) * | 1985-07-10 | 1990-01-18 | Montedipe Spa | Processo catalitico per laproduzione di cicloesanonossima. |
IT1223330B (it) * | 1987-10-29 | 1990-09-19 | Montedipe Spa | Processo per la sintesi di una n n dialchil idrossilammina |
IT1217899B (it) * | 1988-06-23 | 1990-03-30 | Montedipe Spa | Processo catalitico per la produzione di ossime |
-
1991
- 1991-07-10 IT ITMI911915A patent/IT1252047B/it active IP Right Grant
-
1992
- 1992-07-01 DE DE69231652T patent/DE69231652T2/de not_active Expired - Lifetime
- 1992-07-01 DK DK92201955T patent/DK0522634T3/da active
- 1992-07-01 ES ES92201955T patent/ES2153825T3/es not_active Expired - Lifetime
- 1992-07-01 TW TW081105218A patent/TW232676B/zh not_active IP Right Cessation
- 1992-07-01 EP EP92201955A patent/EP0522634B1/en not_active Expired - Lifetime
- 1992-07-01 AT AT92201955T patent/ATE198866T1/de not_active IP Right Cessation
- 1992-07-02 US US07/907,679 patent/US5320819A/en not_active Expired - Lifetime
- 1992-07-03 AU AU19445/92A patent/AU1944592A/en not_active Abandoned
- 1992-07-06 CA CA002073231A patent/CA2073231C/en not_active Expired - Lifetime
- 1992-07-07 KR KR1019920012035A patent/KR930002302A/ko not_active Application Discontinuation
- 1992-07-07 JP JP20188092A patent/JP3374218B2/ja not_active Expired - Lifetime
- 1992-07-09 RU SU925052308A patent/RU2099281C1/ru active
- 1992-07-09 PL PL92295231A patent/PL169232B1/pl unknown
- 1992-07-10 SK SK2171-92A patent/SK217192A3/sk unknown
- 1992-07-10 CZ CS922171A patent/CZ285176B6/cs not_active IP Right Cessation
Also Published As
Publication number | Publication date |
---|---|
CA2073231A1 (en) | 1993-01-11 |
AU1944592A (en) | 1993-01-14 |
CZ217192A3 (en) | 1993-01-13 |
DK0522634T3 (da) | 2001-03-05 |
JPH05201711A (ja) | 1993-08-10 |
PL169232B1 (pl) | 1996-06-28 |
IT1252047B (it) | 1995-05-29 |
CZ285176B6 (cs) | 1999-06-16 |
JP3374218B2 (ja) | 2003-02-04 |
DE69231652T2 (de) | 2001-08-02 |
EP0522634B1 (en) | 2001-01-24 |
ATE198866T1 (de) | 2001-02-15 |
PL295231A1 (en) | 1993-03-22 |
RU2099281C1 (ru) | 1997-12-20 |
DE69231652D1 (de) | 2001-03-01 |
ITMI911915A0 (it) | 1991-07-10 |
EP0522634A1 (en) | 1993-01-13 |
US5320819A (en) | 1994-06-14 |
KR930002302A (ko) | 1993-02-22 |
SK217192A3 (en) | 1994-08-10 |
TW232676B (es) | 1994-10-21 |
CA2073231C (en) | 2002-09-17 |
ITMI911915A1 (it) | 1993-01-10 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
FG2A | Definitive protection |
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